Giacovazzoite
Biagioni C, Bindi L, Mauro D, Pasero M
Physics and Chemistry of Minerals 47 (2020) 7
Crystal-chemistry of sulfates from the Apuan Alps (Tuscany, Italy).
IV. Giacovazzoite, K5Fe3+3O(SO4)6(H2O)9*H2O, the natural analogue of the �-Maus's salt
and its dehydration product
Note: T = 100 K
Locality: the Monte Arsiccio mine, Apuan Alps, Tuscany, Italy
_database_code_amcsd 0020910
CELL PARAMETERS: 9.4480 18.3183 17.9825 90.000 92.274 90.000
SPACE GROUP: P2_1/c
X-RAY WAVELENGTH: 1.541838
Cell Volume: 3109.804
Density (g/cm3): 2.419
MAX. ABS. INTENSITY / VOLUME**2: 10.93837398
RIR: 1.473
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
9.37 100.00 9.4406 1 0 0 2
9.66 4.10 9.1592 0 2 0 2
9.85 34.31 8.9842 0 0 2 2
10.54 2.57 8.3917 1 1 0 4
10.84 61.27 8.1602 0 2 1 4
11.48 1.57 7.7083 -1 1 1 4
11.80 3.30 7.5026 1 1 1 4
13.47 5.82 6.5737 1 2 0 4
14.22 8.64 6.2293 -1 2 1 4
14.48 4.61 6.1192 1 2 1 4
16.49 1.45 5.3765 -1 2 2 4
17.69 1.02 5.0128 0 2 3 4
18.80 9.14 4.7203 2 0 0 2
19.86 3.50 4.4711 -2 1 1 4
20.23 2.86 4.3898 2 1 1 4
20.77 1.38 4.2758 0 3 3 4
20.91 1.09 4.2486 -2 0 2 2
21.57 1.11 4.1204 1 4 0 4
21.57 10.56 4.1202 -1 0 4 2
21.58 1.22 4.1182 -2 2 1 4
21.92 2.48 4.0544 2 2 1 4
22.22 1.77 4.0011 1 4 1 4
22.25 7.79 3.9953 1 0 4 2
23.60 6.20 3.7701 -1 4 2 4
23.83 9.33 3.7345 2 3 0 4
23.91 6.69 3.7209 1 4 2 4
24.47 6.91 3.6380 0 4 3 4
25.49 3.39 3.4949 -2 2 3 4
25.54 6.07 3.4875 -2 3 2 4
26.04 4.63 3.4224 -1 4 3 4
26.09 15.75 3.4154 -1 3 4 4
26.36 1.36 3.3809 2 2 3 4
26.47 2.83 3.3675 1 4 3 4
26.49 4.27 3.3643 -1 5 1 4
26.65 6.86 3.3454 0 2 5 4
26.66 18.74 3.3432 1 3 4 4
27.75 3.14 3.2146 -2 3 3 4
27.81 2.84 3.2079 -1 5 2 4
27.96 4.04 3.1914 2 0 4 2
27.96 4.65 3.1906 -1 2 5 4
28.08 2.22 3.1774 1 5 2 4
28.36 10.49 3.1469 3 0 0 2
28.56 1.29 3.1253 0 5 3 4
28.56 2.70 3.1252 2 3 3 4
28.59 3.14 3.1217 -2 2 4 4
28.64 4.13 3.1172 1 2 5 4
28.66 1.12 3.1147 -2 4 2 4
29.19 3.18 3.0596 2 4 2 4
29.25 1.05 3.0531 0 6 0 2
29.67 1.68 3.0106 1 4 4 4
29.83 8.83 2.9947 0 0 6 2
29.93 20.53 2.9855 -1 5 3 4
30.03 2.34 2.9761 3 2 0 4
30.31 26.96 2.9488 1 5 3 4
30.47 9.15 2.9338 3 0 2 2
30.63 2.20 2.9185 3 2 1 4
30.65 5.67 2.9171 -2 3 4 4
30.66 1.15 2.9157 -2 4 3 4
30.97 4.95 2.8878 -1 0 6 2
31.06 1.13 2.8794 -2 1 5 4
31.13 2.21 2.8732 -1 6 1 4
31.18 15.91 2.8683 -2 5 1 4
31.43 3.67 2.8465 2 5 1 4
31.63 9.78 2.8284 2 3 4 4
31.97 1.22 2.7992 -3 1 3 4
32.00 6.27 2.7972 3 3 0 4
32.03 3.18 2.7940 3 2 2 4
32.09 1.43 2.7895 1 1 6 4
32.21 1.00 2.7789 -3 3 1 4
32.26 1.17 2.7746 -2 5 2 4
32.27 2.37 2.7738 2 1 5 4
32.51 1.24 2.7542 1 6 2 4
32.51 1.09 2.7541 -1 2 6 4
32.71 1.39 2.7378 -1 5 4 4
33.11 3.22 2.7060 -3 2 3 4
33.21 3.99 2.6979 -3 3 2 4
34.13 3.71 2.6268 -3 0 4 2
34.35 6.21 2.6105 -1 3 6 4
34.75 1.38 2.5814 2 5 3 4
35.02 2.06 2.5620 1 3 6 4
35.91 1.19 2.5009 3 3 3 4
36.02 1.88 2.4937 1 7 1 4
36.15 1.58 2.4845 2 0 6 2
36.23 3.62 2.4792 -1 1 7 4
36.98 1.26 2.4308 1 1 7 4
37.92 1.92 2.3730 -2 3 6 4
38.03 1.04 2.3663 0 3 7 4
38.18 1.32 2.3571 3 5 1 4
38.46 4.31 2.3408 4 1 0 4
38.51 1.21 2.3378 3 3 4 4
39.10 1.87 2.3038 3 1 5 4
39.39 2.97 2.2872 -4 1 2 4
39.43 1.54 2.2855 4 2 0 4
39.60 4.53 2.2758 -2 1 7 4
39.66 1.11 2.2727 -1 6 5 4
39.68 1.92 2.2714 0 8 1 4
40.15 1.49 2.2461 -3 3 5 4
40.15 1.51 2.2458 1 6 5 4
40.25 1.23 2.2408 -3 5 3 4
40.54 1.05 2.2253 1 8 0 4
40.66 2.23 2.2189 0 8 2 4
40.83 1.46 2.2099 -4 1 3 4
40.91 1.24 2.2059 1 8 1 4
40.98 2.13 2.2023 2 1 7 4
41.00 2.15 2.2014 4 3 0 4
41.20 2.85 2.1912 3 6 0 4
41.70 2.02 2.1658 1 0 8 2
42.16 1.33 2.1436 -1 2 8 4
42.25 1.64 2.1388 0 8 3 4
42.49 2.18 2.1276 3 0 6 2
43.12 2.31 2.0980 -1 6 6 4
43.68 1.68 2.0724 3 2 6 4
43.81 1.39 2.0663 -1 5 7 4
43.95 1.54 2.0601 -2 0 8 2
44.04 1.81 2.0560 4 0 4 2
44.45 4.02 2.0380 1 5 7 4
44.70 1.05 2.0272 4 4 2 4
44.79 1.53 2.0236 2 7 4 4
44.95 1.51 2.0166 -3 5 5 4
45.22 1.35 2.0052 -3 7 1 4
46.20 1.05 1.9650 4 5 1 4
46.29 1.18 1.9614 3 5 5 4
46.53 1.06 1.9517 2 2 8 4
46.62 1.10 1.9483 3 6 4 4
47.51 1.29 1.9138 2 7 5 4
47.56 1.04 1.9120 1 6 7 4
47.64 1.03 1.9089 -4 3 5 4
48.13 2.46 1.8905 -4 0 6 2
49.22 1.22 1.8513 4 6 1 4
49.67 1.57 1.8356 -2 7 6 4
49.78 4.70 1.8318 0 10 0 2
50.05 1.28 1.8224 0 10 1 4
50.66 1.10 1.8018 2 7 6 4
50.81 1.66 1.7968 0 0 10 2
54.85 1.44 1.6739 -1 10 4 4
54.89 1.15 1.6727 0 4 10 4
57.32 1.18 1.6073 -4 6 6 4
58.63 1.43 1.5745 2 9 6 4
59.71 1.45 1.5485 0 6 10 4
60.14 1.47 1.5385 0 4 11 4
60.45 1.15 1.5315 -6 1 3 4
62.03 1.02 1.4962 5 6 4 4
63.32 1.33 1.4687 -5 4 7 4
64.96 1.36 1.4355 -5 6 6 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.