Nickelboussingaultite
Montgomery H, Lingafelter E C
Acta Crystallographica 17 (1964) 1478-1479
The crystal structure of Tutton's salts. II.
Magnesium ammonium sulfate hexahydrate and nickel ammonium sulfate hexahydrate
Locality: synthetic
_database_code_amcsd 0020239
CELL PARAMETERS: 9.2410 12.5540 6.2430 90.000 106.970 90.000
SPACE GROUP: P2_1/a
X-RAY WAVELENGTH: 1.541838
Cell Volume: 692.724
Density (g/cm3): 1.893
MAX. ABS. INTENSITY / VOLUME**2: 5.593223764
RIR: 0.962
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
12.25 11.45 7.2271 1 1 0 4
14.11 28.97 6.2770 0 2 0 2
14.84 27.04 5.9712 0 0 1 2
16.44 43.50 5.3923 0 1 1 4
16.85 12.29 5.2608 -1 1 1 4
17.33 22.54 5.1177 1 2 0 4
20.09 29.83 4.4193 2 0 0 2
20.53 25.73 4.3263 0 2 1 4
20.86 32.13 4.2576 -1 2 1 4
21.24 79.27 4.1838 -2 0 1 2
21.31 26.62 4.1686 2 1 0 4
21.45 61.09 4.1432 1 1 1 4
22.40 6.83 3.9692 -2 1 1 4
23.52 100.00 3.7822 1 3 0 4
24.64 9.59 3.6136 2 2 0 4
24.75 10.78 3.5970 1 2 1 4
25.59 4.00 3.4814 -2 2 1 4
26.00 12.29 3.4269 0 3 1 4
26.27 24.72 3.3924 -1 3 1 4
28.42 8.09 3.1408 2 0 1 2
28.44 10.95 3.1385 0 4 0 2
29.31 16.99 3.0469 2 1 1 4
29.39 1.10 3.0386 2 3 0 4
29.52 55.23 3.0260 -1 1 2 4
30.21 3.71 2.9587 -2 3 1 4
30.50 1.44 2.9309 -3 1 1 4
30.78 2.70 2.9046 0 1 2 4
30.87 4.46 2.8971 -2 0 2 2
31.18 8.91 2.8683 3 1 0 4
31.70 1.96 2.8229 -2 1 2 4
31.86 25.63 2.8088 2 2 1 4
32.05 21.61 2.7924 -1 2 2 4
32.44 2.95 2.7597 -1 4 1 4
32.97 9.12 2.7171 -3 2 1 4
33.60 1.03 2.6670 3 2 0 4
34.08 2.61 2.6304 -2 2 2 4
35.07 8.03 2.5589 2 4 0 4
35.15 4.93 2.5530 1 4 1 4
35.15 1.83 2.5528 1 1 2 4
35.74 8.04 2.5120 2 3 1 4
36.75 35.71 2.4458 -3 3 1 4
36.77 1.46 2.4443 -3 1 2 4
36.99 2.25 2.4304 0 3 2 4
37.33 3.32 2.4090 3 3 0 4
37.77 1.79 2.3819 -2 3 2 4
38.91 2.22 2.3145 0 5 1 4
40.64 18.39 2.2201 2 4 1 4
40.78 1.57 2.2129 1 3 2 4
40.79 1.53 2.2119 -1 4 2 4
41.43 3.28 2.1794 1 5 1 4
41.49 2.12 2.1762 4 1 0 4
41.54 1.28 2.1740 -3 4 1 4
41.76 13.44 2.1632 0 4 2 4
41.97 3.12 2.1529 -2 5 1 4
42.06 6.79 2.1480 3 4 0 4
42.21 1.83 2.1411 -3 3 2 4
42.46 8.10 2.1288 -2 4 2 4
43.42 15.30 2.0843 4 2 0 4
44.11 1.90 2.0530 -2 0 3 2
44.22 1.64 2.0481 -1 1 3 4
44.73 2.59 2.0261 -2 1 3 4
44.93 1.14 2.0173 -4 3 1 4
45.58 6.47 1.9904 0 0 3 2
45.72 3.32 1.9846 -4 2 2 4
45.96 3.95 1.9746 0 6 1 4
46.29 2.13 1.9612 2 5 1 4
46.74 1.34 1.9435 2 3 2 4
47.11 6.54 1.9292 -3 5 1 4
47.30 2.46 1.9216 0 5 2 4
47.58 7.84 1.9110 3 5 0 4
47.64 10.86 1.9089 -3 1 3 4
47.95 1.64 1.8973 0 2 3 4
48.12 1.91 1.8911 2 6 0 4
48.18 1.61 1.8887 1 6 1 4
48.66 6.15 1.8714 -2 6 1 4
48.98 5.60 1.8597 -1 3 3 4
49.07 3.77 1.8565 -4 4 1 4
49.45 6.35 1.8431 -2 3 3 4
49.87 3.63 1.8285 -5 1 1 4
50.17 3.79 1.8182 4 2 1 4
50.37 4.62 1.8115 1 1 3 4
50.51 7.46 1.8068 4 4 0 4
50.76 4.65 1.7985 2 4 2 4
50.80 3.82 1.7974 0 3 3 4
51.64 1.15 1.7702 3 2 2 4
51.68 3.75 1.7687 -3 5 2 4
52.04 1.05 1.7574 1 2 3 4
52.26 8.31 1.7505 5 1 0 4
52.68 2.67 1.7374 -1 6 2 4
52.93 1.71 1.7298 4 3 1 4
53.01 6.83 1.7276 3 5 1 4
53.32 5.83 1.7181 -2 4 3 4
53.48 2.34 1.7135 0 6 2 4
54.04 1.10 1.6970 -4 5 1 4
54.06 3.73 1.6962 -2 6 2 4
54.26 1.03 1.6906 -5 3 1 4
54.26 2.68 1.6906 -4 2 3 4
54.34 2.49 1.6882 3 3 2 4
54.73 3.60 1.6772 1 3 3 4
55.34 3.03 1.6602 1 7 1 4
55.39 1.30 1.6588 4 5 0 4
55.77 1.01 1.6484 -2 7 1 4
56.64 2.47 1.6252 4 4 1 4
56.64 3.00 1.6250 -5 3 2 4
56.88 1.43 1.6188 -4 3 3 4
57.99 1.73 1.5904 2 2 3 4
59.14 1.52 1.5623 5 1 1 4
59.24 1.07 1.5597 0 5 3 4
59.27 2.26 1.5590 -2 0 4 2
59.39 1.71 1.5563 -5 1 3 4
59.46 2.43 1.5546 -1 7 2 4
59.72 3.71 1.5485 -4 6 1 4
60.42 4.03 1.5321 -4 4 3 4
60.63 1.29 1.5272 5 2 1 4
61.05 1.28 1.5177 0 8 1 4
61.20 1.29 1.5144 2 6 2 4
61.27 1.86 1.5130 -2 2 4 4
62.47 1.18 1.4868 3 5 2 4
62.79 2.26 1.4799 -3 2 4 4
62.81 2.83 1.4794 -4 6 2 4
62.90 4.01 1.4776 1 7 2 4
63.29 1.48 1.4693 -2 8 1 4
64.08 1.77 1.4532 3 1 3 4
64.14 3.22 1.4519 -1 3 4 4
64.58 2.38 1.4430 -5 5 2 4
64.63 1.38 1.4421 0 6 3 4
65.03 2.24 1.4341 6 2 0 4
65.12 4.42 1.4325 3 7 1 4
65.19 1.63 1.4310 -3 3 4 4
65.87 1.04 1.4179 -6 3 2 4
66.21 1.20 1.4114 -4 2 4 4
66.97 1.13 1.3974 1 1 4 4
67.71 2.16 1.3839 3 6 2 4
67.84 1.10 1.3814 -6 4 1 4
68.05 1.96 1.3777 1 6 3 4
68.97 1.14 1.3616 -4 7 2 4
68.98 1.70 1.3614 -6 2 3 4
69.29 2.83 1.3561 -1 9 1 4
70.02 2.65 1.3436 -5 1 4 4
70.12 1.62 1.3420 6 0 1 2
70.58 1.77 1.3344 6 1 1 4
71.19 1.16 1.3244 -2 5 4 4
71.61 1.94 1.3177 -1 5 4 4
71.83 1.60 1.3142 -3 7 3 4
72.21 2.26 1.3083 -7 1 1 4
72.95 2.73 1.2967 -4 8 1 4
73.85 1.26 1.2832 1 4 4 4
74.31 1.03 1.2764 2 2 4 4
74.42 1.31 1.2748 4 2 3 4
75.52 1.29 1.2590 5 7 0 4
75.71 2.28 1.2563 7 1 0 4
75.78 1.01 1.2553 -4 8 2 4
77.73 1.53 1.2285 0 10 1 4
78.16 1.42 1.2229 -6 6 2 4
80.43 1.08 1.1940 5 5 2 4
80.85 1.25 1.1888 -3 3 5 4
81.53 1.44 1.1806 -5 7 3 4
83.47 1.53 1.1581 -6 4 4 4
83.54 1.22 1.1573 0 10 2 4
84.02 1.18 1.1519 -2 10 2 4
84.71 1.32 1.1443 5 2 3 4
85.55 1.59 1.1351 2 8 3 4
87.97 1.59 1.1100 4 8 2 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.