Ponomarevite
de Boer J J, Bright D, Helle J N
Acta Crystallographica B28 (1972) 3436-3437
The structure of the potassium salt of mu4-oxo-hexa-mu-chloro-
tetra[chlorocuprate(II)], K4Cu4OCl10
Locality: synthetic
_database_code_amcsd 0009464
CELL PARAMETERS: 14.7000 14.8800 8.9500 90.000 104.740 90.000
SPACE GROUP: C2/c
X-RAY WAVELENGTH: 1.541838
Cell Volume: 1893.260
Density (g/cm3): 2.740
MAX. ABS. INTENSITY / VOLUME**2: 7.620049953
RIR: 0.906
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
8.60 8.95 10.2790 1 1 0 4
11.90 65.33 7.4400 0 2 0 2
12.10 100.00 7.3172 -1 1 1 4
12.45 67.79 7.1081 2 0 0 2
14.54 86.55 6.0917 1 1 1 4
15.71 5.67 5.6421 0 2 1 4
17.25 41.12 5.1395 2 2 0 4
18.38 33.06 4.8261 -2 2 1 4
18.95 4.45 4.6831 1 3 0 4
19.66 4.59 4.5153 3 1 0 4
19.85 10.23 4.4726 -3 1 1 4
20.75 27.45 4.2802 -1 1 2 4
21.67 46.86 4.1004 2 2 1 4
22.33 23.42 3.9816 1 3 1 4
23.73 13.61 3.7496 1 1 2 4
23.79 2.18 3.7409 0 2 2 4
23.92 8.60 3.7200 0 4 0 2
24.33 43.35 3.6586 -2 2 2 4
24.34 3.73 3.6563 3 1 1 4
24.81 42.64 3.5891 -3 1 2 4
25.06 11.59 3.5541 4 0 0 2
26.01 19.21 3.4263 3 3 0 4
26.15 25.94 3.4076 -3 3 1 4
26.70 4.04 3.3384 2 0 2 2
26.85 15.51 3.3201 -1 3 2 4
27.05 5.35 3.2959 2 4 0 4
27.35 3.43 3.2609 -4 2 1 4
29.25 12.76 3.0534 1 3 2 4
29.32 7.03 3.0458 2 2 2 4
29.76 18.38 3.0024 3 3 1 4
30.13 29.19 2.9660 2 4 1 4
30.14 1.70 2.9649 -3 3 2 4
30.65 21.88 2.9168 -4 2 2 4
31.10 2.25 2.8761 -5 1 1 4
31.72 6.79 2.8210 0 4 2 4
31.90 3.03 2.8053 -1 5 1 4
31.91 39.90 2.8047 4 2 1 4
31.92 17.31 2.8033 3 1 2 4
32.05 7.76 2.7927 5 1 0 4
32.14 44.30 2.7853 -2 4 2 4
32.68 18.73 2.7402 -2 2 3 4
32.95 10.15 2.7182 1 5 1 4
33.56 6.67 2.6702 -5 1 2 4
33.78 1.72 2.6537 1 1 3 4
34.53 39.97 2.5973 -4 4 1 4
34.91 33.91 2.5698 4 4 0 4
35.14 6.87 2.5539 -1 3 3 4
36.15 28.94 2.4846 2 4 2 4
36.22 1.59 2.4800 0 6 0 2
36.31 35.89 2.4740 3 3 2 4
36.57 9.25 2.4570 4 0 2 2
36.81 36.92 2.4416 -4 2 3 4
36.85 9.29 2.4391 -3 3 3 4
37.26 15.14 2.4130 -4 4 2 4
37.78 3.64 2.3811 -5 3 2 4
38.13 2.95 2.3602 1 5 2 4
38.33 6.12 2.3484 4 4 1 4
38.39 1.11 2.3447 -6 0 2 2
38.53 4.97 2.3364 3 5 1 4
38.59 9.54 2.3331 4 2 2 4
38.87 4.38 2.3167 -5 1 3 4
38.99 21.76 2.3102 -2 4 3 4
39.00 7.10 2.3096 -2 6 1 4
39.53 6.64 2.2798 0 4 3 4
39.93 6.64 2.2577 6 2 0 4
40.16 1.80 2.2452 5 3 1 4
40.33 9.50 2.2363 -6 2 2 4
40.36 5.77 2.2345 -2 0 4 2
40.75 6.66 2.2140 2 6 1 4
41.00 2.95 2.2011 3 1 3 4
41.74 6.61 2.1639 0 0 4 2
42.23 8.33 2.1401 -2 2 4 4
42.32 4.61 2.1357 -2 6 2 4
42.59 3.18 2.1227 -4 4 3 4
42.96 2.71 2.1055 -1 5 3 4
43.02 13.63 2.1023 1 7 0 4
43.06 6.39 2.1009 -4 0 4 2
43.53 11.37 2.0790 -7 1 1 4
43.56 5.45 2.0778 0 2 4 4
43.83 3.68 2.0657 6 2 1 4
43.94 3.95 2.0608 -1 7 1 4
44.05 2.59 2.0558 5 5 0 4
44.09 1.63 2.0541 2 4 3 4
44.17 1.82 2.0502 4 4 2 4
44.34 2.58 2.0430 1 1 4 4
44.56 9.70 2.0333 -6 2 3 4
44.63 11.71 2.0306 3 3 3 4
44.63 4.28 2.0302 -1 3 4 4
45.05 4.00 2.0122 7 1 0 4
45.21 22.64 2.0054 -5 5 2 4
45.26 4.14 2.0035 -3 3 4 4
45.38 8.21 1.9984 1 5 3 4
45.57 9.15 1.9908 2 6 2 4
46.21 1.53 1.9647 -5 1 4 4
46.95 1.46 1.9353 4 2 3 4
47.29 8.72 1.9222 5 5 1 4
47.36 4.09 1.9196 -1 7 2 4
47.94 5.69 1.8976 -2 6 3 4
48.25 9.54 1.8860 6 0 2 2
48.40 15.71 1.8807 0 6 3 4
48.56 3.71 1.8748 2 2 4 4
48.68 1.54 1.8704 0 4 4 4
48.93 1.28 1.8616 6 4 1 4
48.99 1.71 1.8593 7 1 1 4
49.28 9.73 1.8492 -6 0 4 2
49.48 2.72 1.8421 -5 5 3 4
49.53 2.60 1.8405 -5 3 4 4
49.88 4.63 1.8281 6 2 2 4
50.17 2.40 1.8185 0 8 1 4
50.87 11.86 1.7949 5 1 3 4
51.04 2.40 1.7895 -4 6 3 4
51.18 3.92 1.7848 -2 8 1 4
51.27 4.22 1.7821 -1 5 4 4
51.28 2.00 1.7817 -8 2 1 4
51.77 3.34 1.7658 -3 1 5 4
51.88 2.44 1.7624 -8 2 2 4
51.93 4.11 1.7609 -1 1 5 4
52.51 29.52 1.7427 -6 6 1 4
52.61 5.43 1.7396 2 8 1 4
52.91 1.55 1.7304 -1 7 3 4
52.98 8.18 1.7284 8 2 0 4
53.32 1.94 1.7183 2 4 4 4
53.41 3.79 1.7156 -7 5 1 4
53.85 6.99 1.7025 5 7 0 4
53.91 6.50 1.7008 -2 8 2 4
54.10 8.60 1.6952 1 5 4 4
54.12 2.96 1.6946 -4 2 5 4
54.72 3.64 1.6775 7 5 0 4
54.74 6.66 1.6769 -8 2 3 4
54.96 1.64 1.6707 7 1 2 4
54.98 2.06 1.6701 -5 1 5 4
54.99 1.20 1.6699 -1 3 5 4
55.01 2.76 1.6692 4 0 4 2
55.72 1.23 1.6496 -5 5 4 4
55.78 1.86 1.6480 4 8 0 4
56.43 1.02 1.6305 -8 4 2 4
56.50 1.69 1.6287 4 2 4 4
56.65 8.55 1.6248 2 8 2 4
56.67 1.17 1.6243 5 7 1 4
56.84 5.74 1.6197 8 2 1 4
57.11 2.86 1.6129 -2 4 5 4
57.27 2.07 1.6087 -6 6 3 4
57.47 2.68 1.6035 8 4 0 4
58.19 1.73 1.5853 -8 0 4 2
58.21 1.02 1.5849 4 8 1 4
58.36 1.31 1.5812 1 3 5 4
58.84 4.62 1.5695 0 4 5 4
59.09 2.40 1.5633 0 8 3 4
59.26 1.04 1.5593 -3 9 1 4
59.63 3.04 1.5505 -8 2 4 4
60.21 8.82 1.5370 -1 7 4 4
60.66 1.06 1.5266 -3 5 5 4
60.82 1.26 1.5229 4 4 4 4
61.19 5.83 1.5146 -7 1 5 4
61.21 1.12 1.5143 3 9 1 4
62.59 5.16 1.4842 7 1 3 4
62.68 1.80 1.4823 -3 1 6 4
62.72 3.62 1.4813 -6 8 1 4
62.77 2.83 1.4803 1 7 4 4
63.01 3.47 1.4752 -8 6 1 4
63.08 3.16 1.4737 -4 0 6 2
63.59 1.17 1.4632 2 4 5 4
63.97 2.84 1.4555 -7 3 5 4
64.30 1.49 1.4487 -2 10 1 4
64.64 2.26 1.4420 3 3 5 4
64.83 2.00 1.4381 -10 2 2 4
64.93 1.12 1.4361 -10 2 1 4
65.32 1.39 1.4285 7 3 3 4
65.41 3.02 1.4267 -3 3 6 4
65.47 2.00 1.4257 9 3 1 4
65.56 1.29 1.4238 -3 9 3 4
66.68 2.27 1.4026 -2 10 2 4
66.73 3.78 1.4017 -10 2 3 4
66.74 1.24 1.4016 6 2 4 4
67.08 1.05 1.3953 4 2 5 4
67.08 2.03 1.3952 9 5 0 4
67.16 4.41 1.3937 1 1 6 4
67.71 3.18 1.3839 -9 5 3 4
67.77 1.04 1.3828 -2 4 6 4
67.81 4.41 1.3820 5 9 1 4
68.11 3.79 1.3767 -4 10 1 4
68.21 3.01 1.3749 3 7 4 4
68.85 2.06 1.3637 -10 4 2 4
68.95 1.06 1.3620 -10 4 1 4
69.23 1.35 1.3571 -10 0 4 2
69.57 1.33 1.3513 -5 9 3 4
69.77 1.69 1.3480 -6 6 5 4
69.81 2.41 1.3472 1 3 6 4
69.85 1.52 1.3466 1 11 0 4
69.95 1.02 1.3448 -9 1 5 4
70.28 2.02 1.3394 2 6 5 4
70.77 1.17 1.3312 9 5 1 4
71.11 3.44 1.3258 1 11 1 4
71.13 1.12 1.3254 9 3 2 4
71.27 1.73 1.3233 -11 1 1 4
71.50 2.16 1.3196 -3 9 4 4
72.33 1.06 1.3063 -8 8 1 4
74.56 2.16 1.2728 4 10 2 4
74.87 2.53 1.2682 10 4 1 4
76.25 1.48 1.2487 5 7 4 4
76.68 2.04 1.2427 -8 6 5 4
76.88 1.32 1.2400 0 12 0 2
77.68 2.12 1.2293 6 8 3 4
78.02 1.66 1.2248 -12 0 2 2
78.73 2.24 1.2155 -6 8 5 4
80.24 1.82 1.1964 8 6 3 4
83.49 3.03 1.1578 -5 5 7 4
85.41 1.27 1.1367 -8 8 5 4
85.49 1.99 1.1359 -9 9 3 4
88.36 1.40 1.1062 9 9 1 4
88.90 1.18 1.1009 8 8 3 4
89.99 1.42 1.0903 5 5 6 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.