Garrelsite
Ghose S, Wan C, Ulbrich H H
Acta Crystallographica B32 (1976) 824-832
Structural chemistry of borosilicates. I. Garrelsite, NaBa3Si2B7O16(OH)4, a
silicoborate with the pentaborate [B5O12]9- polyanion
Locality: South Ouray, Utah
_database_code_amcsd 0009552
CELL PARAMETERS: 14.6390 8.4660 13.4380 90.000 114.210 90.000
SPACE GROUP: C2/c
X-RAY WAVELENGTH: 1.541838
Cell Volume: 1518.946
Density (g/cm3): 3.877
MAX. ABS. INTENSITY / VOLUME**2: 17.51983839
RIR: 1.471
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
12.38 5.92 7.1498 1 1 0 4
12.89 1.54 6.8669 -1 1 1 4
13.26 6.80 6.6757 2 0 0 2
14.45 37.13 6.1281 0 0 2 2
15.09 6.62 5.8702 -2 0 2 2
15.66 38.23 5.6585 1 1 1 4
16.86 17.46 5.2583 -1 1 2 4
20.99 23.88 4.2330 0 2 0 2
21.03 3.79 4.2235 -3 1 1 4
21.06 14.11 4.2177 1 1 2 4
21.95 12.10 4.0490 -3 1 2 4
22.57 48.09 3.9393 3 1 0 4
24.36 40.27 3.6544 -2 2 1 4
24.59 71.43 3.6205 -4 0 2 2
24.91 2.45 3.5749 2 2 0 4
25.07 3.81 3.5523 -3 1 3 4
25.58 31.18 3.4829 0 2 2 4
25.95 5.88 3.4334 -2 2 2 4
26.71 6.73 3.3379 4 0 0 2
27.42 24.36 3.2528 1 1 3 4
27.48 34.17 3.2456 2 2 1 4
29.08 68.28 3.0710 -1 1 4 4
29.14 24.23 3.0640 0 0 4 2
29.36 100.00 3.0416 -2 2 3 4
30.46 24.02 2.9351 -4 0 4 2
31.13 62.41 2.8731 3 1 2 4
32.37 1.39 2.7660 -5 1 2 4
32.43 7.77 2.7610 1 3 0 4
32.54 54.19 2.7514 -4 2 2 4
32.55 1.48 2.7506 -4 2 1 4
33.01 41.58 2.7137 -5 1 1 4
33.40 1.09 2.6829 -5 1 3 4
33.88 38.43 2.6458 1 3 1 4
34.10 6.37 2.6291 -2 2 4 4
34.18 1.91 2.6231 -4 2 3 4
34.21 3.38 2.6210 4 2 0 4
34.28 7.34 2.6160 1 1 4 4
34.48 1.24 2.6013 -1 3 2 4
35.24 7.94 2.5466 5 1 0 4
35.42 3.54 2.5344 -3 1 5 4
35.51 12.51 2.5280 4 0 2 2
35.98 4.49 2.4963 -5 1 4 4
36.19 5.15 2.4820 0 2 4 4
36.80 4.67 2.4421 -3 3 1 4
36.82 1.05 2.4410 1 3 2 4
36.87 2.11 2.4380 2 2 3 4
36.96 6.49 2.4321 2 0 4 2
37.01 4.00 2.4292 3 1 3 4
37.28 4.96 2.4120 -4 2 4 4
37.32 2.24 2.4093 4 2 1 4
37.75 1.50 2.3833 3 3 0 4
38.83 9.71 2.3192 5 1 1 4
39.36 7.72 2.2890 -3 3 3 4
39.76 22.13 2.2671 -2 2 5 4
40.10 2.83 2.2487 3 3 1 4
40.54 1.34 2.2252 -2 0 6 2
40.98 19.48 2.2026 1 3 3 4
41.29 8.18 2.1867 -4 0 6 2
41.48 1.67 2.1767 1 1 5 4
41.56 2.60 2.1731 -4 2 5 4
41.77 2.24 2.1623 -3 1 6 4
42.62 13.68 2.1212 0 2 5 4
42.72 8.85 2.1165 0 4 0 2
42.82 1.82 2.1117 -6 2 2 4
42.88 3.86 2.1088 2 2 4 4
43.14 12.94 2.0968 -6 2 3 4
43.31 15.50 2.0890 -1 1 6 4
43.39 5.75 2.0856 0 4 1 4
43.51 20.34 2.0802 3 1 4 4
43.83 5.02 2.0657 -6 2 1 4
44.35 1.08 2.0427 0 0 6 2
44.60 26.70 2.0315 -2 4 1 4
44.72 2.77 2.0266 -7 1 3 4
44.72 22.69 2.0265 -5 1 6 4
44.77 1.83 2.0245 -6 2 4 4
44.89 14.04 2.0191 -7 1 2 4
44.93 2.05 2.0175 2 4 0 4
45.10 29.22 2.0104 -5 3 1 4
45.40 5.93 1.9978 -5 3 3 4
45.82 17.12 1.9803 -7 1 4 4
46.08 1.74 1.9697 1 3 4 4
46.08 1.12 1.9697 6 2 0 4
46.40 1.32 1.9567 -6 0 6 2
46.52 8.40 1.9523 2 4 1 4
46.76 8.77 1.9428 -4 2 6 4
46.82 3.33 1.9403 4 2 3 4
46.84 2.31 1.9396 5 3 0 4
46.98 11.23 1.9342 -3 3 5 4
47.42 1.30 1.9171 -5 3 4 4
47.47 5.90 1.9155 -1 3 5 4
47.58 13.12 1.9110 -6 2 5 4
47.74 12.93 1.9051 -2 4 3 4
47.83 2.02 1.9019 4 0 4 2
48.25 1.69 1.8862 3 3 3 4
48.64 4.58 1.8719 -3 1 7 4
48.94 8.17 1.8611 6 0 2 2
48.95 14.88 1.8607 7 1 0 4
48.99 4.62 1.8592 5 1 3 4
48.99 1.90 1.8592 1 1 6 4
49.73 16.25 1.8333 5 3 1 4
49.91 3.56 1.8272 -4 4 2 4
49.92 2.45 1.8270 -4 4 1 4
50.39 1.49 1.8108 -5 1 7 4
50.41 7.13 1.8103 -8 0 4 2
50.44 1.57 1.8094 -8 0 2 2
51.02 1.79 1.7900 -2 4 4 4
51.08 1.54 1.7881 -4 4 3 4
51.45 3.02 1.7762 -6 2 6 4
51.90 5.86 1.7616 2 0 6 2
51.94 16.66 1.7604 1 3 5 4
52.19 1.01 1.7528 -3 3 6 4
52.70 2.07 1.7370 -4 2 7 4
52.77 2.30 1.7348 4 2 4 4
53.06 3.41 1.7260 2 4 3 4
53.64 3.50 1.7086 5 3 2 4
54.72 1.07 1.6773 -4 0 8 2
54.95 2.95 1.6711 -8 0 6 2
55.18 3.66 1.6644 -8 2 4 4
55.27 2.33 1.6621 -2 4 5 4
55.61 2.00 1.6528 1 5 1 4
55.79 4.28 1.6478 -2 0 8 2
55.88 1.14 1.6452 -7 1 7 4
55.95 1.70 1.6435 -3 1 8 4
56.21 3.26 1.6364 -6 2 7 4
56.59 1.11 1.6264 2 2 6 4
56.73 2.61 1.6228 4 4 2 4
56.73 5.28 1.6227 -5 1 8 4
56.86 1.06 1.6193 -8 2 1 4
56.91 3.17 1.6179 0 2 7 4
57.21 3.22 1.6103 7 1 2 4
57.53 1.88 1.6020 0 4 5 4
57.63 1.20 1.5994 -3 5 1 4
57.79 1.56 1.5953 -9 1 3 4
57.91 5.98 1.5925 3 1 6 4
57.95 4.06 1.5913 -6 4 3 4
58.03 3.48 1.5894 -3 5 2 4
58.12 6.58 1.5871 -3 3 7 4
58.31 1.94 1.5825 3 5 0 4
58.31 1.73 1.5825 -1 5 3 4
58.43 9.16 1.5793 5 3 3 4
58.50 1.15 1.5777 -6 4 1 4
58.74 2.54 1.5718 -9 1 2 4
58.80 7.68 1.5703 -1 1 8 4
59.34 4.29 1.5575 4 2 5 4
59.47 2.87 1.5543 -8 2 6 4
60.03 1.33 1.5412 3 5 1 4
60.64 2.49 1.5272 6 0 4 2
60.68 2.76 1.5261 1 5 3 4
60.92 2.14 1.5208 -4 4 6 4
60.97 3.75 1.5196 4 4 3 4
61.58 3.68 1.5060 -1 5 4 4
61.61 10.48 1.5054 -6 4 5 4
62.74 6.51 1.4809 3 5 2 4
63.17 3.93 1.4719 8 2 1 4
63.38 5.72 1.4676 -8 0 8 2
63.49 1.98 1.4651 8 0 2 2
63.86 2.34 1.4576 -5 5 1 4
64.65 2.52 1.4418 -7 3 7 4
64.70 1.05 1.4406 -3 3 8 4
64.91 4.14 1.4366 6 2 4 4
65.12 3.14 1.4324 -10 0 2 2
65.36 2.01 1.4278 -3 5 5 4
65.50 1.94 1.4250 1 3 7 4
65.75 2.93 1.4202 -1 5 5 4
66.24 2.92 1.4110 0 6 0 2
66.39 1.55 1.4081 3 5 3 4
66.39 1.66 1.4081 -4 2 9 4
66.40 9.46 1.4078 -9 3 3 4
66.73 1.69 1.4017 0 6 1 4
66.98 2.41 1.3971 -7 1 9 4
67.56 2.16 1.3866 9 1 1 4
67.60 1.52 1.3857 5 5 1 4
67.61 2.30 1.3856 -9 3 5 4
67.65 1.19 1.3850 -2 6 1 4
68.01 1.50 1.3784 -6 2 9 4
68.19 1.63 1.3753 2 0 8 2
68.20 2.49 1.3750 0 6 2 4
68.47 2.86 1.3702 -10 2 5 4
68.54 3.40 1.3691 -9 1 8 4
69.08 2.95 1.3597 -6 4 7 4
69.12 3.14 1.3589 -9 3 1 4
69.32 1.35 1.3555 5 1 6 4
69.44 2.60 1.3534 1 5 5 4
69.66 1.07 1.3499 -8 4 1 4
69.70 3.74 1.3491 0 4 7 4
70.54 1.78 1.3351 10 0 0 2
70.76 1.65 1.3316 -1 5 6 4
70.90 1.79 1.3293 3 5 4 4
71.14 4.55 1.3253 -5 1 10 4
71.79 5.07 1.3149 -5 5 6 4
71.80 6.55 1.3147 -4 6 2 4
71.81 1.50 1.3146 -4 6 1 4
71.81 2.22 1.3145 -11 1 4 4
71.88 2.85 1.3134 4 4 5 4
71.90 3.13 1.3131 -3 3 9 4
71.92 1.33 1.3129 -7 5 2 4
72.23 3.24 1.3080 2 2 8 4
72.34 1.10 1.3062 -10 0 8 2
72.47 4.21 1.3042 -2 0 10 2
72.61 2.58 1.3020 -7 5 4 4
72.65 1.07 1.3014 -9 3 7 4
72.75 1.59 1.2999 -4 6 3 4
72.77 1.46 1.2996 4 6 0 4
72.77 5.00 1.2995 -10 2 7 4
72.98 3.22 1.2964 8 2 3 4
72.98 4.87 1.2964 0 2 9 4
72.99 1.67 1.2961 -7 5 1 4
73.45 3.65 1.2893 -11 1 6 4
73.60 1.72 1.2870 -7 1 10 4
73.96 2.64 1.2816 0 6 4 4
73.98 4.86 1.2813 -11 1 2 4
74.19 5.85 1.2782 4 2 7 4
74.52 1.95 1.2733 10 2 0 4
74.63 1.45 1.2717 -4 6 4 4
74.77 2.38 1.2698 -3 5 7 4
74.89 2.07 1.2679 6 0 6 2
75.01 3.16 1.2662 7 5 0 4
75.03 5.95 1.2660 -7 3 9 4
75.04 2.38 1.2658 5 5 3 4
75.38 2.89 1.2609 8 4 1 4
75.57 4.04 1.2582 9 3 1 4
76.42 1.53 1.2464 -2 2 10 4
76.54 1.12 1.2446 -1 5 7 4
79.15 1.44 1.2100 -9 1 10 4
79.40 1.24 1.2068 -12 0 6 2
79.49 3.51 1.2057 10 0 2 2
80.33 1.31 1.1952 -10 4 5 4
80.63 1.21 1.1916 -7 5 7 4
80.67 1.04 1.1910 -10 2 9 4
81.12 2.23 1.1856 -4 6 6 4
81.34 1.12 1.1829 -5 5 8 4
82.25 1.76 1.1722 -9 5 3 4
82.34 1.40 1.1711 3 5 6 4
82.44 2.29 1.1700 -4 2 11 4
82.68 1.30 1.1671 3 7 0 4
83.11 1.74 1.1622 -1 5 8 4
83.17 1.27 1.1615 2 6 5 4
83.33 1.01 1.1596 10 2 2 4
83.95 1.33 1.1526 -12 0 8 2
84.13 1.05 1.1506 9 1 4 4
84.42 3.98 1.1474 -10 4 7 4
84.62 2.73 1.1452 8 4 3 4
84.62 3.44 1.1452 0 4 9 4
84.78 2.03 1.1435 -9 5 1 4
85.53 3.48 1.1354 -1 7 4 4
85.79 2.98 1.1326 4 4 7 4
85.87 1.39 1.1317 5 1 8 4
85.94 2.78 1.1310 8 2 5 4
86.40 2.30 1.1262 2 0 10 2
86.56 2.60 1.1245 3 7 2 4
87.37 1.34 1.1161 -5 5 9 4
87.69 1.47 1.1129 -8 -6 4 4
87.88 1.30 1.1110 -12 -2 1 4
88.29 1.02 1.1069 -3 3 11 4
88.55 2.67 1.1043 -7 3 11 4
88.86 1.13 1.1013 2 6 6 4
================================================================================
XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.