Gladite
Kohatsu I, Wuensch B J
Acta Crystallographica B32 (1976) 2401-2409
The crystal structure of gladite, PbCuBi5S9, a superstructure intermediate in
the series Bi2S3-PbCuBiS3 (bismuthinite-aikinite)
_database_code_amcsd 0009571
CELL PARAMETERS: 33.5310 11.4860 4.0030 90.000 90.000 90.000
SPACE GROUP: Pbnm
X-RAY WAVELENGTH: 1.541838
Cell Volume: 1541.703
Density (g/cm3): 6.911
MAX. ABS. INTENSITY / VOLUME**2: 80.06158578
RIR: 3.772
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
5.27 3.71 16.7655 2 0 0 2
11.05 3.20 8.0103 3 1 0 4
15.43 18.21 5.7430 0 2 0 2
15.86 3.10 5.5885 6 0 0 2
16.31 2.85 5.4331 2 2 0 4
17.36 19.59 5.1081 3 2 0 4
21.20 4.54 4.1914 8 0 0 2
22.20 53.25 4.0052 6 2 0 4
22.58 5.73 3.9374 8 1 0 4
23.61 28.80 3.7686 3 0 1 4
23.84 4.57 3.7326 2 3 0 4
24.19 2.49 3.6785 7 2 0 4
24.58 100.00 3.6221 3 3 0 4
24.87 56.42 3.5808 3 1 1 8
25.13 85.05 3.5439 9 1 0 4
25.58 1.20 3.4826 4 3 0 4
26.58 5.71 3.3531 10 0 0 2
26.81 1.94 3.3249 5 3 0 4
27.15 19.42 3.2840 0 2 1 4
27.29 4.06 3.2683 1 2 1 8
27.68 1.52 3.2227 2 2 1 8
28.25 8.36 3.1585 6 3 0 4
28.33 56.56 3.1508 3 2 1 8
28.51 94.79 3.1310 6 1 1 8
28.56 7.76 3.1256 9 2 0 4
29.21 3.18 3.0577 4 2 1 8
29.88 1.92 2.9907 7 3 0 4
30.12 3.54 2.9674 7 1 1 8
31.15 2.89 2.8715 0 4 0 2
31.60 97.30 2.8313 6 2 1 8
31.61 1.15 2.8303 2 4 0 4
32.03 4.05 2.7942 12 0 0 2
32.84 22.97 2.7272 9 0 1 4
32.99 3.77 2.7151 12 1 0 4
33.56 1.15 2.6701 9 3 0 4
33.78 35.39 2.6535 9 1 1 8
33.96 3.86 2.6397 5 4 0 4
35.14 45.83 2.5541 6 4 0 4
35.74 15.86 2.5126 12 2 0 4
35.80 1.11 2.5084 10 1 1 8
36.23 19.85 2.4796 6 3 1 8
36.47 1.57 2.4636 9 2 1 8
36.48 2.58 2.4629 7 4 0 4
37.07 1.09 2.4252 11 0 1 4
38.59 23.96 2.3333 0 4 1 4
38.68 5.34 2.3276 1 4 1 8
39.45 32.55 2.2840 3 4 1 8
39.63 3.09 2.2744 9 4 0 4
39.94 3.32 2.2571 12 3 0 4
40.13 21.57 2.2470 12 1 1 8
40.37 6.30 2.2341 11 2 1 8
40.61 5.54 2.2213 9 3 1 8
40.73 1.07 2.2155 4 5 0 4
41.14 3.90 2.1942 15 1 0 4
41.55 1.02 2.1732 5 5 0 4
41.96 9.17 2.1531 6 4 1 8
42.25 3.06 2.1392 13 3 0 4
42.43 2.53 2.1306 13 1 1 8
42.48 15.97 2.1281 12 2 1 8
42.55 8.90 2.1247 6 5 0 4
43.29 1.73 2.0902 11 4 0 4
43.44 5.17 2.0832 15 2 0 4
44.21 1.66 2.0487 11 3 1 8
44.67 1.42 2.0284 13 2 1 8
45.28 3.76 2.0026 12 4 0 4
45.31 40.83 2.0015 0 0 2 2
45.87 1.33 1.9785 2 5 1 8
45.89 1.57 1.9775 9 4 1 8
46.17 41.32 1.9661 12 3 1 8
46.29 9.49 1.9615 3 5 1 8
46.44 11.25 1.9554 9 5 0 4
46.53 18.57 1.9517 15 0 1 4
46.87 1.73 1.9384 4 5 1 8
47.07 23.07 1.9304 15 3 0 4
47.24 3.22 1.9241 15 1 1 8
47.47 1.67 1.9152 10 4 1 8
47.50 10.20 1.9143 0 6 0 2
47.58 1.60 1.9112 1 6 0 4
47.61 1.93 1.9099 5 5 1 8
48.01 1.37 1.8951 10 5 0 4
48.14 1.92 1.8900 0 2 2 4
48.23 1.16 1.8869 3 6 0 4
48.24 1.63 1.8867 13 3 1 8
48.51 9.29 1.8767 6 5 1 8
48.82 1.21 1.8655 17 2 0 4
48.87 2.36 1.8636 3 2 2 8
48.89 8.09 1.8628 18 0 0 2
49.31 1.55 1.8479 15 2 1 8
49.52 1.73 1.8408 5 6 0 4
49.56 1.87 1.8393 14 4 0 4
49.57 1.52 1.8388 18 1 0 4
50.39 1.19 1.8110 6 6 0 4
50.39 3.05 1.8109 14 3 1 8
50.73 2.61 1.7995 8 5 1 8
50.99 1.15 1.7910 12 4 1 8
51.01 11.12 1.7904 6 2 2 8
51.20 1.26 1.7842 8 1 2 8
51.58 3.08 1.7719 18 2 0 4
51.66 2.23 1.7693 17 0 1 4
51.75 2.96 1.7666 16 2 1 8
51.83 1.27 1.7639 15 4 0 4
51.83 1.02 1.7639 2 3 2 8
52.05 13.66 1.7570 9 5 1 8
52.22 24.08 1.7518 3 3 2 8
52.46 1.87 1.7443 19 1 0 4
52.51 21.98 1.7428 9 1 2 8
52.64 4.01 1.7388 15 3 1 8
53.02 12.09 1.7270 0 6 1 4
53.30 1.46 1.7186 10 0 2 4
53.70 4.86 1.7068 3 6 1 8
53.84 2.29 1.7027 9 6 0 4
54.23 1.93 1.6915 4 6 1 8
54.26 2.05 1.6906 6 3 2 8
54.44 2.23 1.6855 9 2 2 8
54.95 3.69 1.6709 18 1 1 8
55.38 1.93 1.6590 20 1 0 4
55.71 1.60 1.6500 6 6 1 8
56.00 1.03 1.6420 0 4 2 4
56.56 1.46 1.6271 12 0 2 4
56.75 4.48 1.6223 12 5 1 8
57.18 1.62 1.6111 12 1 2 8
57.64 2.69 1.5991 19 1 1 8
57.81 1.44 1.5949 5 4 2 8
58.60 18.17 1.5754 6 4 2 8
58.64 1.09 1.5744 6 7 0 4
58.95 2.05 1.5669 9 6 1 8
59.00 6.41 1.5655 12 2 2 8
59.12 2.76 1.5628 18 4 0 4
59.27 1.06 1.5591 16 4 1 8
59.51 1.15 1.5533 7 4 2 8
60.15 4.51 1.5384 21 2 0 4
60.44 1.50 1.5317 14 5 1 8
60.60 1.21 1.5279 8 7 0 4
61.31 2.22 1.5121 2 7 1 8
61.65 7.23 1.5044 3 7 1 8
61.74 1.49 1.5025 9 4 2 8
61.78 6.60 1.5017 9 7 0 4
61.97 1.63 1.4975 12 3 2 8
62.13 1.34 1.4940 4 7 1 8
62.84 2.01 1.4787 15 1 2 8
63.22 1.99 1.4709 21 1 1 8
63.49 4.05 1.4651 6 7 1 8
63.67 1.60 1.4615 13 3 2 8
63.90 4.72 1.4569 6 5 2 8
63.95 4.72 1.4558 18 4 1 8
64.04 2.46 1.4540 15 6 0 4
64.39 1.66 1.4469 18 5 0 4
64.57 2.68 1.4433 15 2 2 8
64.94 8.24 1.4360 21 2 1 8
65.05 2.44 1.4339 20 3 1 8
65.55 1.89 1.4240 3 8 0 4
65.99 2.16 1.4157 12 4 2 8
66.03 3.07 1.4149 12 7 0 4
66.90 6.80 1.3987 9 5 2 8
66.98 1.26 1.3971 24 0 0 2
67.40 13.88 1.3895 15 3 2 8
67.73 6.34 1.3834 0 6 2 4
67.78 2.26 1.3825 22 2 1 8
68.19 1.49 1.3753 7 8 0 4
68.68 5.13 1.3667 15 6 1 8
68.85 5.18 1.3636 18 0 2 4
69.21 1.66 1.3575 24 2 0 4
69.36 1.10 1.3549 5 6 2 8
69.40 1.18 1.3543 14 4 2 8
70.14 1.17 1.3417 3 8 1 8
70.54 2.87 1.3351 18 6 0 4
71.05 2.14 1.3267 18 2 2 8
71.16 1.13 1.3249 3 0 3 4
71.17 1.17 1.3248 5 8 1 8
71.40 2.59 1.3211 19 5 1 8
71.61 12.66 1.3177 21 4 1 8
71.71 2.55 1.3162 3 1 3 8
71.78 1.34 1.3150 19 1 2 8
71.87 3.88 1.3136 6 8 1 8
72.07 2.92 1.3105 24 1 1 8
72.20 1.27 1.3084 13 7 1 8
72.70 1.32 1.3007 7 8 1 8
72.79 2.40 1.2993 17 6 1 8
72.94 1.60 1.2969 9 6 2 8
73.33 3.40 1.2910 3 2 3 8
73.42 5.12 1.2896 6 1 3 8
74.25 1.45 1.2773 20 1 2 8
74.57 1.26 1.2725 2 9 0 4
74.89 2.05 1.2680 3 9 0 4
75.03 6.12 1.2659 6 2 3 8
75.04 1.38 1.2658 25 3 0 4
75.71 1.49 1.2562 9 0 3 4
75.73 4.50 1.2560 15 7 1 8
76.25 2.52 1.2488 9 1 3 8
77.22 2.06 1.2355 11 8 1 8
77.27 1.51 1.2347 27 1 0 4
77.49 2.26 1.2318 18 4 2 8
77.69 1.67 1.2292 6 3 3 8
78.34 1.39 1.2206 26 1 1 8
78.40 3.68 1.2197 21 2 2 8
78.64 2.34 1.2166 12 8 1 8
78.80 1.02 1.2145 8 7 2 8
79.15 2.37 1.2101 0 4 3 4
79.70 3.33 1.2030 3 4 3 8
79.85 5.60 1.2012 9 7 2 8
80.15 2.32 1.1975 12 1 3 8
80.46 1.01 1.1937 24 5 0 4
81.08 2.90 1.1861 27 0 1 4
81.36 1.01 1.1827 6 4 3 8
81.71 1.83 1.1785 12 2 3 8
81.85 2.48 1.1769 18 7 1 8
81.89 2.21 1.1764 15 6 2 8
82.21 1.48 1.1726 18 5 2 8
83.22 2.11 1.1609 12 9 0 4
83.27 1.76 1.1603 3 8 2 8
83.61 1.89 1.1565 15 8 1 8
83.66 1.49 1.1559 9 9 1 8
83.71 2.89 1.1554 12 7 2 8
84.31 5.81 1.1486 12 3 3 8
84.40 1.27 1.1477 3 5 3 8
84.58 2.64 1.1457 15 0 3 4
84.59 1.20 1.1456 24 0 2 4
85.71 1.49 1.1335 7 8 2 8
86.04 1.47 1.1300 6 5 3 8
86.66 1.67 1.1235 24 2 2 8
87.49 1.90 1.1149 12 9 1 8
87.91 2.94 1.1106 18 6 2 8
88.58 2.19 1.1040 0 10 1 4
88.64 1.71 1.1035 1 10 1 8
88.77 2.49 1.1022 9 5 3 8
89.54 2.22 1.0947 0 6 3 4
89.77 1.03 1.0925 27 5 0 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.