Giacovazzoite
Mereiter K, Vollenkle H
Acta Crystallographica B34 (1978) 378-384
Die Kristallstruktur von beta-pentakalium-[mu3-oxo-hexa-mu-sulfato-
triquatriesen(III)]-Heptahydrat - eine monokline Modifikation des
Masschen Salzes
Locality: synthetic
_database_code_amcsd 0019784
CELL PARAMETERS: 9.4910 18.4740 18.1090 90.000 92.380 90.000
SPACE GROUP: P2_1/c
X-RAY WAVELENGTH: 1.541838
Cell Volume: 3172.434
Density (g/cm3): 2.377
MAX. ABS. INTENSITY / VOLUME**2: 10.64532333
RIR: 1.458
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
9.33 100.00 9.4828 1 0 0 2
9.57 4.57 9.2370 0 2 0 2
9.78 36.02 9.0467 0 0 2 2
10.49 2.44 8.4363 1 1 0 4
10.75 64.57 8.2269 0 2 1 4
11.41 1.49 7.7566 -1 1 1 4
11.74 3.16 7.5401 1 1 1 4
13.38 6.22 6.6167 1 2 0 4
14.12 9.03 6.2732 -1 2 1 4
14.39 4.82 6.1570 1 2 1 4
16.37 1.55 5.4160 -1 2 2 4
17.56 1.13 5.0500 0 2 3 4
17.76 1.08 4.9944 -1 1 3 4
18.40 1.10 4.8227 1 1 3 4
18.71 8.59 4.7414 2 0 0 2
19.75 3.41 4.4947 -2 1 1 4
20.14 2.72 4.4093 2 1 1 4
20.61 1.25 4.3088 0 3 3 4
20.79 1.05 4.2732 -2 0 2 2
21.40 1.07 4.1522 1 4 0 4
21.41 10.11 4.1502 -1 0 4 2
21.45 1.22 4.1420 -2 2 1 4
21.81 2.35 4.0748 2 2 1 4
22.05 1.70 4.0311 1 4 1 4
22.12 7.50 4.0183 1 0 4 2
23.41 5.97 3.8000 -1 4 2 4
23.68 9.53 3.7568 2 3 0 4
23.74 6.31 3.7480 1 4 2 4
24.27 6.14 3.6668 0 4 3 4
25.32 3.39 3.5182 -2 2 3 4
25.37 5.65 3.5107 -2 3 2 4
25.83 4.73 3.4495 -1 4 3 4
25.89 15.25 3.4415 -1 3 4 4
26.22 1.41 3.3982 2 2 3 4
26.28 3.95 3.3914 -1 5 1 4
26.28 3.06 3.3914 1 4 3 4
26.45 6.42 3.3693 0 2 5 4
26.49 18.60 3.3652 1 3 4 4
26.67 1.05 3.3429 -2 0 4 2
26.95 1.04 3.3084 2 4 0 4
27.26 1.16 3.2712 -2 4 1 4
27.56 2.90 3.2369 -2 3 3 4
27.58 2.66 3.2338 -1 5 2 4
27.75 4.48 3.2143 -1 2 5 4
27.82 4.30 3.2070 2 0 4 2
27.87 2.10 3.2016 1 5 2 4
28.23 10.74 3.1609 3 0 0 2
28.33 1.03 3.1506 0 5 3 4
28.39 2.84 3.1434 -2 2 4 4
28.40 2.59 3.1427 2 3 3 4
28.45 4.66 3.1369 1 2 5 4
28.46 1.05 3.1366 -2 4 2 4
29.00 2.85 3.0785 2 4 2 4
29.46 1.65 3.0315 1 4 4 4
29.62 8.90 3.0156 0 0 6 2
29.69 21.43 3.0095 -1 5 3 4
29.88 2.25 2.9907 3 2 0 4
30.08 26.43 2.9707 1 5 3 4
30.34 8.32 2.9462 3 0 2 2
30.43 5.77 2.9379 -2 3 4 4
30.44 1.10 2.9367 -2 4 3 4
30.49 2.03 2.9322 3 2 1 4
30.74 4.36 2.9089 -1 0 6 2
30.84 1.08 2.8996 -2 1 5 4
30.87 1.97 2.8967 -1 6 1 4
30.95 16.25 2.8889 -2 5 1 4
31.21 3.50 2.8659 2 5 1 4
31.45 9.40 2.8444 2 3 4 4
31.78 1.03 2.8155 -3 1 3 4
31.82 6.17 2.8121 3 3 0 4
31.88 1.20 2.8069 1 1 6 4
31.88 3.03 2.8069 3 2 2 4
32.10 1.99 2.7884 2 1 5 4
32.25 1.13 2.7757 1 6 2 4
32.44 1.43 2.7596 -1 5 4 4
32.90 2.99 2.7223 -3 2 3 4
33.01 3.95 2.7139 -3 3 2 4
33.92 3.75 2.6430 -3 0 4 2
34.09 6.40 2.6302 -1 3 6 4
34.52 1.68 2.5982 2 5 3 4
34.79 2.06 2.5789 1 3 6 4
35.72 1.63 2.5139 1 7 1 4
35.72 1.05 2.5134 3 3 3 4
35.95 1.22 2.4980 2 0 6 2
35.96 3.16 2.4973 -1 1 7 4
36.74 1.37 2.4462 1 1 7 4
37.63 1.88 2.3904 -2 3 6 4
37.94 1.29 2.3713 3 5 1 4
38.28 4.09 2.3514 4 1 0 4
38.31 1.17 2.3496 3 3 4 4
38.91 1.94 2.3147 3 1 5 4
39.19 2.43 2.2990 -4 1 2 4
39.23 1.19 2.2963 4 2 0 4
39.30 4.32 2.2923 -2 1 7 4
39.33 1.99 2.2907 0 8 1 4
39.85 1.23 2.2623 1 6 5 4
39.87 1.29 2.2613 -3 3 5 4
39.96 1.00 2.2561 -3 5 3 4
40.31 1.82 2.2375 0 8 2 4
40.56 1.04 2.2240 1 8 1 4
40.60 1.35 2.2220 -4 1 3 4
40.74 2.35 2.2148 2 1 7 4
40.79 2.16 2.2124 4 3 0 4
40.92 2.41 2.2056 3 6 0 4
41.43 1.50 2.1796 1 0 8 2
41.89 1.51 2.1566 0 8 3 4
42.27 1.63 2.1380 3 0 6 2
42.77 1.86 2.1145 -1 6 6 4
43.44 1.34 2.0829 3 2 6 4
43.46 1.44 2.0822 -1 5 7 4
43.62 1.53 2.0751 -2 0 8 2
43.85 1.60 2.0648 4 0 4 2
44.13 3.57 2.0522 1 5 7 4
44.46 1.62 2.0378 2 7 4 4
44.62 1.42 2.0309 -3 5 5 4
44.89 1.10 2.0192 -3 7 1 4
46.01 1.15 1.9727 3 5 5 4
47.16 1.06 1.9271 2 7 5 4
47.49 1.01 1.9144 -4 5 3 4
47.81 2.26 1.9025 -4 0 6 2
49.26 1.31 1.8499 -2 7 6 4
49.33 4.32 1.8474 0 10 0 2
49.60 1.28 1.8378 0 10 1 4
50.44 1.58 1.8093 0 0 10 2
54.36 1.18 1.6877 -1 10 4 4
58.17 1.30 1.5859 2 9 6 4
59.23 1.31 1.5599 0 6 10 4
59.67 1.29 1.5495 0 4 11 4
62.87 1.20 1.4782 -5 4 7 4
64.49 1.15 1.4450 -5 6 6 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.