Znamenskyite
Kramer V
Acta Crystallographica C42 (1986) 1089-1091
Lead indium bismuth chalcogenides. III. Structure of Pb4In2Bi4S13
Locality: synthetic
_database_code_amcsd 0020219
CELL PARAMETERS: 21.3440 26.4940 4.0020 90.000 90.000 90.000
SPACE GROUP: Pbam
X-RAY WAVELENGTH: 1.541838
Cell Volume: 2263.083
Density (g/cm3): 6.782
MAX. ABS. INTENSITY / VOLUME**2: 39.05890324
RIR: 1.875
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
6.67 1.18 13.2470 0 2 0 2
7.85 11.58 11.2554 1 2 0 4
8.29 2.01 10.6720 2 0 0 2
10.84 3.75 8.1604 1 3 0 4
12.88 4.99 6.8712 3 1 0 4
13.01 3.57 6.8038 2 3 0 4
14.13 3.20 6.2679 3 2 0 4
15.75 9.43 5.6277 2 4 0 4
16.00 1.32 5.5404 3 3 0 4
16.61 19.18 5.3360 4 0 0 2
16.95 2.16 5.2310 4 1 0 4
17.24 2.97 5.1427 1 5 0 4
17.92 1.70 4.9495 4 2 0 4
18.30 18.79 4.8479 3 4 0 4
21.38 10.54 4.1553 4 4 0 4
21.78 44.88 4.0802 2 6 0 4
21.88 17.76 4.0631 5 2 0 4
22.21 22.68 4.0020 0 0 1 2
23.59 2.41 3.7707 1 2 1 8
23.66 59.06 3.7599 4 5 0 4
23.72 5.72 3.7518 3 6 0 4
23.74 9.27 3.7472 2 0 1 4
23.88 15.39 3.7267 1 7 0 4
23.98 1.03 3.7103 2 1 1 8
24.69 11.75 3.6057 2 2 1 8
24.78 6.68 3.5932 1 3 1 8
24.81 6.84 3.5882 5 4 0 4
24.96 79.01 3.5672 2 7 0 4
25.03 39.17 3.5573 6 0 0 2
25.26 92.10 3.5257 6 1 0 4
25.76 46.12 3.4582 3 1 1 8
25.83 12.14 3.4495 2 3 1 8
25.93 3.49 3.4356 6 2 0 4
26.01 29.49 3.4253 0 4 1 4
26.20 95.64 3.4019 4 6 0 4
26.35 22.89 3.3820 1 4 1 8
26.42 69.38 3.3731 3 2 1 8
26.68 41.16 3.3415 3 7 0 4
26.92 2.50 3.3117 0 8 0 2
27.02 7.63 3.2997 6 3 0 4
27.25 18.68 3.2726 1 8 0 4
27.35 11.06 3.2614 2 4 1 8
27.49 99.51 3.2442 3 3 1 8
27.87 33.29 3.2016 4 0 1 4
28.07 10.53 3.1785 4 1 1 8
28.26 33.30 3.1584 1 5 1 8
28.48 5.18 3.1339 6 4 0 4
28.92 1.48 3.0871 4 7 0 4
28.93 1.90 3.0863 3 4 1 8
29.10 10.59 3.0691 5 6 0 4
29.68 13.18 3.0099 4 3 1 8
30.07 26.05 2.9714 7 2 0 4
30.14 59.03 2.9653 0 6 1 4
30.26 1.35 2.9535 6 5 0 4
30.43 18.52 2.9371 1 6 1 8
30.69 13.21 2.9135 3 5 1 8
31.02 54.32 2.8825 4 4 1 8
31.03 8.97 2.8822 7 3 0 4
31.53 1.02 2.8378 2 9 0 4
31.59 11.52 2.8320 5 7 0 4
31.80 2.59 2.8139 4 8 0 4
32.29 7.45 2.7721 5 3 1 8
32.68 59.51 2.7402 4 5 1 8
32.72 3.72 2.7371 3 6 1 8
32.84 100.00 2.7273 1 7 1 8
33.54 33.55 2.6716 5 4 1 8
33.59 8.07 2.6680 8 0 0 2
33.66 10.06 2.6629 2 7 1 8
33.71 6.78 2.6588 6 0 1 4
33.77 15.56 2.6546 8 1 0 4
33.83 3.67 2.6494 0 10 0 2
33.88 13.00 2.6455 6 1 1 8
34.10 1.65 2.6292 1 10 0 4
34.27 6.93 2.6166 5 8 0 4
34.40 1.04 2.6068 6 2 1 8
34.60 6.15 2.5921 6 7 0 4
34.81 1.71 2.5776 4 9 0 4
34.98 9.73 2.5649 3 7 1 8
35.09 5.12 2.5571 5 5 1 8
35.17 4.25 2.5514 0 8 1 4
35.25 4.55 2.5459 6 3 1 8
35.43 1.43 2.5334 1 8 1 8
35.79 2.47 2.5091 7 6 0 4
36.18 1.27 2.4828 3 10 0 4
36.41 17.74 2.4674 6 4 1 8
36.77 1.44 2.4444 4 7 1 8
36.91 1.29 2.4354 5 6 1 8
37.09 1.77 2.4239 6 8 0 4
37.45 1.38 2.4017 3 8 1 8
37.86 26.13 2.3764 6 5 1 8
37.92 4.85 2.3730 4 10 0 4
38.10 3.86 2.3621 9 1 0 4
38.19 24.65 2.3568 1 9 1 8
38.49 1.31 2.3388 7 3 1 8
38.91 1.05 2.3149 2 9 1 8
38.96 6.33 2.3117 5 7 1 8
39.13 1.44 2.3018 4 8 1 8
39.34 1.38 2.2904 9 3 0 4
39.57 1.30 2.2778 6 6 1 8
39.57 25.83 2.2775 7 4 1 8
40.08 1.57 2.2497 3 9 1 8
40.20 10.88 2.2432 7 8 0 4
40.64 6.07 2.2199 8 0 1 4
40.79 14.40 2.2122 8 1 1 8
40.85 4.34 2.2092 0 10 1 4
40.87 12.08 2.2078 0 12 0 2
40.92 14.39 2.2053 7 5 1 8
41.08 4.36 2.1974 1 10 1 8
41.10 4.61 2.1961 1 12 0 4
41.23 2.09 2.1894 8 2 1 8
41.41 7.01 2.1807 8 7 0 4
41.51 5.98 2.1756 6 7 1 8
41.73 1.17 2.1646 9 5 0 4
41.75 1.97 2.1633 2 10 1 8
41.78 5.21 2.1621 2 12 0 4
41.96 4.93 2.1529 8 3 1 8
42.49 1.14 2.1275 10 1 0 4
42.53 5.64 2.1258 7 6 1 8
42.69 5.84 2.1178 7 9 0 4
42.86 5.35 2.1098 3 10 1 8
43.12 3.23 2.0977 5 11 0 4
43.31 5.44 2.0893 9 6 0 4
43.56 10.72 2.0777 8 8 0 4
43.66 7.60 2.0733 6 8 1 8
44.09 2.50 2.0541 1 11 1 8
44.24 2.13 2.0475 8 5 1 8
44.36 7.80 2.0421 7 7 1 8
44.38 4.20 2.0411 4 10 1 8
44.54 4.03 2.0342 9 1 1 8
44.67 8.82 2.0288 1 13 0 4
44.73 22.45 2.0261 2 11 1 8
44.95 40.80 2.0165 9 2 1 8
45.12 1.17 2.0096 9 7 0 4
45.30 6.31 2.0018 2 13 0 4
45.32 71.23 2.0010 0 0 2 2
45.35 1.82 1.9999 7 10 0 4
45.48 15.50 1.9944 6 11 0 4
45.64 1.08 1.9879 9 3 1 8
45.75 10.87 1.9834 8 6 1 8
45.83 28.55 1.9798 10 5 0 4
45.90 4.34 1.9769 8 9 0 4
46.00 2.61 1.9731 6 9 1 8
46.27 3.81 1.9620 5 10 1 8
46.30 2.59 1.9611 5 12 0 4
46.34 7.66 1.9592 3 13 0 4
46.40 49.12 1.9568 7 8 1 8
46.95 7.66 1.9352 11 1 0 4
47.21 25.95 1.9253 1 12 1 8
47.22 1.89 1.9247 4 11 1 8
48.01 2.36 1.8952 11 3 0 4
48.28 3.67 1.8850 1 14 0 4
48.46 15.59 1.8786 10 1 1 8
48.51 3.03 1.8767 6 10 1 8
48.59 2.15 1.8736 4 0 2 4
48.64 8.71 1.8719 7 9 1 8
49.00 10.05 1.8592 10 7 0 4
49.03 2.98 1.8579 5 11 1 8
49.26 2.43 1.8496 3 4 2 8
49.86 1.09 1.8288 3 14 0 4
50.19 15.98 1.8176 4 12 1 8
50.37 8.81 1.8115 10 4 1 8
50.43 1.30 1.8095 1 13 1 8
50.63 1.56 1.8029 4 4 2 8
50.82 7.47 1.7966 2 6 2 8
50.84 1.54 1.7959 9 7 1 8
50.87 2.88 1.7951 5 2 2 8
50.90 1.01 1.7941 10 8 0 4
51.07 3.97 1.7883 7 12 0 4
51.09 1.47 1.7878 8 11 0 4
51.17 9.37 1.7850 6 11 1 8
51.22 2.95 1.7836 4 14 0 4
51.49 2.69 1.7747 12 1 0 4
51.50 3.36 1.7745 10 5 1 8
51.69 2.70 1.7684 6 13 0 4
51.75 11.52 1.7664 4 5 2 8
51.78 1.13 1.7656 3 6 2 8
51.86 3.26 1.7629 1 7 2 8
51.87 2.64 1.7628 12 2 0 4
51.92 12.25 1.7610 5 12 1 8
51.97 9.68 1.7597 3 13 1 8
52.35 1.49 1.7476 5 4 2 8
52.43 17.71 1.7452 2 7 2 8
52.47 8.66 1.7440 6 0 2 4
52.51 6.05 1.7426 2 15 0 4
52.59 19.94 1.7403 6 1 2 8
52.69 2.07 1.7371 9 8 1 8
52.85 13.07 1.7323 10 6 1 8
52.89 1.49 1.7310 11 2 1 8
53.10 22.54 1.7248 4 6 2 8
53.33 2.31 1.7178 12 4 0 4
53.37 10.02 1.7167 3 7 2 8
53.45 2.52 1.7142 3 15 0 4
53.56 2.04 1.7110 6 3 2 8
53.69 4.72 1.7072 1 8 2 8
53.90 4.34 1.7010 8 12 0 4
54.13 5.02 1.6944 7 13 0 4
54.28 1.79 1.6899 9 11 0 4
54.31 3.77 1.6892 2 14 1 8
54.40 1.40 1.6865 6 4 2 8
54.74 1.87 1.6769 9 9 1 8
54.76 2.85 1.6762 5 6 2 8
54.84 4.23 1.6742 11 8 0 4
54.96 1.53 1.6707 6 14 0 4
55.22 5.89 1.6634 3 14 1 8
55.35 7.04 1.6597 7 2 2 8
55.41 1.03 1.6583 11 5 1 8
55.49 1.52 1.6559 0 16 0 2
55.94 2.77 1.6437 7 3 2 8
56.13 6.10 1.6387 13 1 0 4
56.29 2.86 1.6342 5 7 2 8
56.36 1.11 1.6323 8 11 1 8
57.11 2.78 1.6128 3 16 0 4
57.17 2.56 1.6113 1 15 1 8
57.58 2.84 1.6008 8 0 2 4
57.67 1.19 1.5985 12 3 1 8
57.69 4.88 1.5979 8 1 2 8
57.74 1.06 1.5968 0 10 2 4
58.03 2.43 1.5895 5 8 2 8
58.19 1.58 1.5854 11 7 1 8
58.25 2.22 1.5840 6 7 2 8
59.37 1.79 1.5568 9 11 1 8
59.92 2.63 1.5438 5 16 0 4
59.93 1.42 1.5436 8 14 0 4
60.13 1.27 1.5389 13 6 0 4
60.31 1.78 1.5346 10 12 0 4
60.52 2.03 1.5297 4 10 2 8
60.65 1.69 1.5268 9 1 2 8
60.86 3.94 1.5221 14 1 0 4
61.19 1.20 1.5146 14 2 0 4
61.34 1.03 1.5112 5 15 1 8
61.99 6.07 1.4970 13 3 1 8
62.17 4.71 1.4932 7 8 2 8
62.22 1.46 1.4920 7 14 1 8
62.61 4.53 1.4836 10 11 1 8
62.66 5.33 1.4827 0 12 2 4
62.76 1.17 1.4805 13 4 1 8
62.83 2.02 1.4791 1 12 2 8
62.94 1.22 1.4767 12 10 0 4
63.05 3.26 1.4744 8 7 2 8
63.13 5.54 1.4728 8 15 0 4
63.33 2.38 1.4686 2 12 2 8
63.55 1.01 1.4640 5 17 0 4
63.85 3.87 1.4579 11 10 1 8
64.02 2.82 1.4545 7 9 2 8
64.29 1.14 1.4489 1 17 1 8
64.34 1.56 1.4479 5 11 2 8
64.48 2.67 1.4451 9 6 2 8
64.67 5.00 1.4413 8 8 2 8
64.73 3.57 1.4402 8 14 1 8
64.79 2.08 1.4390 2 17 1 8
65.52 6.01 1.4247 14 0 1 4
65.52 4.43 1.4246 1 13 2 8
65.82 3.20 1.4189 4 18 0 4
65.97 2.77 1.4160 10 14 0 4
66.01 3.00 1.4152 2 13 2 8
66.05 1.04 1.4145 7 10 2 8
66.10 1.22 1.4136 11 11 1 8
66.15 7.71 1.4126 6 11 2 8
66.31 3.95 1.4097 13 7 1 8
66.43 14.39 1.4074 10 5 2 8
66.48 2.24 1.4063 8 9 2 8
66.79 1.31 1.4006 5 12 2 8
66.83 4.04 1.3999 3 13 2 8
67.31 4.01 1.3911 11 1 2 8
67.51 2.48 1.3875 9 14 1 8
67.64 1.72 1.3851 12 12 0 4
67.65 1.44 1.3849 14 8 0 4
67.77 1.97 1.3827 2 19 0 4
67.80 1.09 1.3822 8 15 1 8
67.84 2.59 1.3814 0 18 1 4
67.89 5.33 1.3807 13 8 1 8
68.15 1.25 1.3760 11 3 2 8
68.16 6.59 1.3758 14 5 1 8
68.21 2.23 1.3749 5 17 1 8
68.37 2.16 1.3721 1 14 2 8
68.52 3.57 1.3695 11 12 1 8
68.95 5.54 1.3620 10 7 2 8
69.30 1.20 1.3559 14 6 1 8
69.39 1.95 1.3544 15 6 0 4
69.81 3.22 1.3473 12 11 1 8
69.97 2.92 1.3445 6 17 1 8
70.40 3.16 1.3373 4 18 1 8
70.64 2.28 1.3334 7 12 2 8
70.65 1.34 1.3334 14 7 1 8
70.76 1.79 1.3314 4 14 2 8
70.99 1.55 1.3277 12 1 2 8
71.10 2.63 1.3259 11 13 1 8
71.15 1.60 1.3251 6 13 2 8
71.30 1.62 1.3227 12 2 2 8
71.63 1.75 1.3175 13 12 0 4
71.81 1.16 1.3146 2 20 0 4
71.83 1.21 1.3143 1 19 1 8
71.84 3.57 1.3141 2 15 2 8
72.13 1.51 1.3095 3 1 3 8
72.17 5.42 1.3089 12 12 1 8
72.24 1.03 1.3077 0 4 3 4
72.30 6.93 1.3069 2 19 1 8
72.43 2.73 1.3048 3 2 3 8
72.52 1.52 1.3034 12 4 2 8
72.62 1.67 1.3018 3 15 2 8
72.94 4.11 1.2969 3 3 3 8
73.00 2.74 1.2960 8 12 2 8
73.08 4.49 1.2948 3 19 1 8
73.12 1.51 1.2942 4 0 3 4
73.20 3.28 1.2931 7 13 2 8
73.31 1.55 1.2913 1 5 3 8
73.33 1.13 1.2911 9 11 2 8
73.51 1.34 1.2883 10 15 1 8
73.80 2.88 1.2840 11 8 2 8
73.85 1.23 1.2832 11 14 1 8
74.17 1.07 1.2784 4 19 1 8
74.27 3.18 1.2770 16 6 0 4
74.27 2.55 1.2770 0 6 3 4
74.36 1.01 1.2757 0 16 2 4
74.70 2.99 1.2707 12 13 1 8
74.74 2.59 1.2702 4 4 3 8
74.90 4.27 1.2678 13 1 2 8
75.08 1.39 1.2652 5 20 0 4
75.18 1.19 1.2638 15 7 1 8
75.54 2.02 1.2587 10 17 0 4
75.56 1.42 1.2583 7 18 1 8
75.62 1.81 1.2576 0 20 1 4
75.64 2.98 1.2572 4 5 3 8
75.73 5.23 1.2560 1 7 3 8
75.75 1.96 1.2557 3 16 2 8
75.86 1.58 1.2541 17 1 0 4
75.96 1.00 1.2527 16 3 1 8
76.13 1.97 1.2504 5 4 3 8
76.16 1.28 1.2499 17 2 0 4
76.99 2.13 1.2385 9 17 1 8
77.82 1.24 1.2274 6 4 3 8
77.87 6.16 1.2267 8 18 1 8
78.21 2.00 1.2223 5 16 2 8
78.56 1.37 1.2177 10 12 2 8
78.65 4.57 1.2166 16 6 1 8
78.71 1.82 1.2157 6 5 3 8
78.91 1.77 1.2131 1 9 3 8
79.04 2.87 1.2114 14 1 2 8
79.61 1.61 1.2043 0 22 0 2
79.80 2.06 1.2019 7 4 3 8
80.21 2.05 1.1967 17 1 1 8
80.25 1.58 1.1963 15 10 1 8
80.60 1.19 1.1920 8 1 3 8
80.68 1.38 1.1909 7 5 3 8
81.07 4.33 1.1861 8 15 2 8
81.11 3.78 1.1857 6 20 1 8
81.68 1.08 1.1788 17 4 1 8
82.67 1.09 1.1672 18 4 0 4
83.30 2.47 1.1600 2 11 3 8
83.46 4.22 1.1582 9 2 3 8
83.53 2.72 1.1574 4 18 2 8
83.67 2.39 1.1559 10 14 2 8
84.02 1.22 1.1519 8 6 3 8
84.50 5.33 1.1466 7 8 3 8
84.92 1.01 1.1420 16 10 1 8
85.09 2.97 1.1401 1 12 3 8
85.21 1.42 1.1389 12 12 2 8
85.22 1.26 1.1387 14 8 2 8
85.33 1.61 1.1375 2 19 2 8
86.02 1.75 1.1302 10 1 3 8
86.16 1.09 1.1287 7 9 3 8
86.84 1.74 1.1216 15 6 2 8
87.34 2.21 1.1165 4 12 3 8
87.47 1.31 1.1151 10 4 3 8
87.87 1.54 1.1110 9 20 1 8
88.02 1.21 1.1096 17 9 1 8
88.10 1.27 1.1088 6 11 3 8
88.68 1.71 1.1030 5 12 3 8
88.72 1.26 1.1027 3 13 3 8
88.88 1.34 1.1010 18 6 1 8
88.95 1.59 1.1004 13 12 2 8
89.12 1.05 1.0987 2 20 2 8
89.42 1.98 1.0958 10 6 3 8
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.