Robinsonite
Skowron A, Brown I D
Acta Crystallographica C46 (1990) 527-531
Refinement of the structure of robinsonite, Pb4Sb6S13
Locality: synthetic
_database_code_amcsd 0010117
CELL PARAMETERS: 23.6980 3.9800 24.4660 90.000 93.900 90.000
SPACE GROUP: I2/m
X-RAY WAVELENGTH: 1.541838
Cell Volume: 2302.241
Density (g/cm3): 5.959
MAX. ABS. INTENSITY / VOLUME**2: 26.23307823
RIR: 1.433
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
5.38 2.62 16.4332 1 0 1 2
7.48 2.69 11.8216 2 0 0 2
10.77 4.41 8.2166 2 0 2 2
11.26 1.22 7.8599 -1 0 3 2
11.74 13.12 7.5375 1 0 3 2
12.03 11.85 7.3550 3 0 1 2
14.52 14.04 6.1023 0 0 4 2
15.11 1.48 5.8637 -3 0 3 2
15.88 2.06 5.5794 -2 0 4 2
16.18 11.60 5.4777 3 0 3 2
16.21 5.43 5.4676 -4 0 2 2
16.80 2.74 5.2781 2 0 4 2
17.11 1.66 5.1832 4 0 2 2
20.19 20.36 4.3978 -4 0 4 2
20.74 3.03 4.2826 -3 0 5 2
21.63 5.02 4.1083 4 0 4 2
21.85 67.13 4.0682 0 0 6 2
22.38 62.59 3.9726 5 0 3 2
22.56 19.57 3.9405 6 0 0 2
22.63 25.73 3.9299 -2 0 6 2
22.64 1.63 3.9281 0 1 1 4
22.66 20.01 3.9248 1 1 0 4
23.24 68.66 3.8268 -6 0 2 2
23.61 6.56 3.7687 2 0 6 2
23.74 30.28 3.7487 -1 1 2 4
23.79 9.45 3.7400 -2 1 1 4
23.89 10.83 3.7241 1 1 2 4
23.95 100.00 3.7156 2 1 1 4
24.20 52.26 3.6775 6 0 2 2
24.90 17.52 3.5752 0 1 3 4
25.31 41.67 3.5182 -5 0 5 2
25.57 2.60 3.4841 -1 0 7 2
25.73 33.70 3.4630 -4 0 6 2
25.82 2.26 3.4508 -2 1 3 4
26.07 10.46 3.4180 -6 0 4 2
26.08 91.12 3.4164 1 0 7 2
26.26 28.26 3.3941 2 1 3 4
26.34 16.70 3.3834 3 1 2 4
26.39 3.38 3.3770 -7 0 1 2
26.87 12.27 3.3181 -1 1 4 4
26.89 3.00 3.3152 7 0 1 2
27.12 1.14 3.2882 -4 1 1 4
27.15 2.61 3.2842 1 1 4 4
27.25 1.76 3.2723 -3 0 7 2
27.40 32.28 3.2552 4 1 1 4
27.45 1.55 3.2495 4 0 6 2
27.77 45.10 3.2123 6 0 4 2
27.90 21.08 3.1974 -7 0 3 2
28.69 8.98 3.1120 -3 1 4 4
28.80 1.17 3.1004 -4 1 3 4
28.94 11.11 3.0848 0 1 5 4
29.27 14.65 3.0512 0 0 8 2
29.31 25.18 3.0470 7 0 3 2
29.33 76.80 3.0450 5 1 0 4
29.59 15.74 3.0194 4 1 3 4
29.61 44.81 3.0167 -2 1 5 4
29.93 27.43 2.9853 -5 1 2 4
30.26 10.53 2.9540 2 1 5 4
30.49 4.63 2.9318 -6 0 6 2
30.57 23.06 2.9245 5 1 2 4
30.64 1.86 2.9181 -8 0 2 2
30.76 17.44 2.9069 2 0 8 2
30.81 3.20 2.9024 -5 0 7 2
31.49 85.39 2.8407 -1 1 6 4
31.86 16.55 2.8088 1 1 6 4
32.08 4.09 2.7897 -4 0 8 2
32.15 94.42 2.7843 -4 1 5 4
32.28 93.31 2.7736 -5 1 4 4
32.36 57.77 2.7669 6 1 1 4
32.70 6.40 2.7389 6 0 6 2
32.96 6.06 2.7175 -3 1 6 4
33.27 29.47 2.6932 7 0 5 2
33.33 35.29 2.6881 -6 1 3 4
33.34 1.02 2.6878 4 1 5 4
33.46 3.21 2.6782 5 1 4 4
33.51 30.51 2.6740 1 0 9 2
33.97 1.87 2.6391 4 0 8 2
34.08 1.43 2.6310 -9 0 1 2
34.37 3.53 2.6093 6 1 3 4
34.61 17.79 2.5916 8 0 4 2
34.65 11.67 2.5887 -2 1 7 4
34.84 7.95 2.5752 7 1 0 4
35.18 6.79 2.5512 -9 0 3 2
35.24 9.14 2.5466 -7 1 2 4
35.43 14.77 2.5333 2 1 7 4
35.74 1.02 2.5125 3 0 9 2
35.98 2.51 2.4961 -6 0 8 2
36.01 4.72 2.4938 7 1 2 4
36.77 14.46 2.4442 -4 1 7 4
37.07 9.99 2.4249 -5 0 9 2
37.12 1.73 2.4222 -1 1 8 4
37.54 8.62 2.3958 1 1 8 4
37.67 5.04 2.3881 5 1 6 4
37.80 14.20 2.3799 6 1 5 4
37.90 15.10 2.3741 -8 1 1 4
38.15 2.52 2.3589 2 0 10 2
38.25 3.57 2.3532 4 1 7 4
38.28 16.79 2.3512 -10 0 2 2
38.29 2.38 2.3506 -3 1 8 4
38.31 1.95 2.3493 8 1 1 4
38.34 2.16 2.3476 7 0 7 2
38.53 2.95 2.3368 6 0 8 2
38.65 3.53 2.3297 7 1 4 4
38.95 23.23 2.3121 -8 1 3 4
39.41 2.87 2.2865 5 0 9 2
39.52 54.02 2.2804 3 1 8 4
40.07 1.10 2.2504 9 0 5 2
40.16 7.61 2.2452 8 1 3 4
40.24 4.32 2.2412 0 1 9 4
40.32 7.74 2.2368 -6 1 7 4
40.54 2.05 2.2250 -2 1 9 4
40.95 16.32 2.2041 -5 1 8 4
40.95 1.37 2.2039 4 0 10 2
41.05 2.51 2.1989 -8 0 8 2
41.11 5.56 2.1955 1 0 11 2
41.17 1.38 2.1925 9 1 0 4
41.25 1.22 2.1887 -7 0 9 2
41.39 1.15 2.1814 -8 1 5 4
41.43 3.95 2.1797 2 1 9 4
41.43 13.44 2.1796 -9 1 2 4
41.61 1.07 2.1704 -9 0 7 2
41.91 1.93 2.1558 10 0 4 2
42.20 17.59 2.1413 -6 0 10 2
42.32 1.14 2.1358 -4 1 9 4
42.47 8.68 2.1285 11 0 1 2
42.51 17.98 2.1267 7 1 6 4
42.78 11.99 2.1139 -11 0 3 2
42.87 23.12 2.1096 5 1 8 4
43.04 1.31 2.1017 -9 1 4 4
43.30 8.84 2.0897 8 1 5 4
43.87 19.09 2.0635 -5 0 11 2
43.90 4.23 2.0623 1 1 10 4
44.23 2.49 2.0478 7 0 9 2
44.32 2.23 2.0440 11 0 3 2
44.38 2.82 2.0413 -3 1 10 4
44.57 2.98 2.0328 9 0 7 2
44.69 2.38 2.0278 -2 0 12 2
44.71 10.47 2.0271 9 1 4 4
44.86 2.61 2.0203 -7 1 8 4
45.00 3.86 2.0146 6 0 10 2
45.02 3.57 2.0135 -8 1 7 4
45.59 80.03 1.9900 0 2 0 2
45.67 2.14 1.9863 10 0 6 2
45.74 6.22 1.9836 3 1 10 4
45.77 3.39 1.9822 2 0 12 2
45.89 5.86 1.9775 -9 1 6 4
46.07 4.63 1.9703 12 0 0 2
46.17 5.53 1.9662 -12 0 2 2
46.46 1.08 1.9546 -9 0 9 2
46.62 5.55 1.9482 -8 0 10 2
46.66 2.23 1.9466 -5 1 10 4
46.69 6.37 1.9455 10 1 3 4
46.99 5.54 1.9337 -10 0 8 2
47.36 5.81 1.9196 11 0 5 2
47.36 11.93 1.9195 7 1 8 4
47.43 9.14 1.9167 -10 1 5 4
48.02 11.66 1.8947 2 1 11 4
48.11 42.77 1.8912 11 1 0 4
48.20 1.33 1.8880 -11 0 7 2
48.25 2.72 1.8861 -11 1 2 4
48.26 12.05 1.8858 9 1 6 4
48.37 2.72 1.8819 -1 0 13 2
48.56 45.51 1.8749 -4 1 11 4
48.68 1.24 1.8704 3 2 3 4
48.83 7.91 1.8651 5 1 10 4
48.92 9.95 1.8618 1 0 13 2
48.98 1.68 1.8598 -6 0 12 2
49.11 6.64 1.8552 -3 0 13 2
49.19 1.49 1.8522 11 1 2 4
49.58 1.78 1.8388 10 1 5 4
49.60 1.03 1.8378 -11 1 4 4
49.65 4.61 1.8362 -8 1 9 4
49.82 2.33 1.8304 -9 1 8 4
49.95 1.02 1.8259 9 0 9 2
50.04 3.90 1.8229 -13 0 1 2
50.05 8.08 1.8225 -12 0 6 2
50.06 2.04 1.8221 8 0 10 2
50.29 1.87 1.8144 -1 1 12 4
50.33 2.88 1.8130 -4 2 4 4
50.58 7.75 1.8046 13 0 1 2
50.64 17.90 1.8026 -10 1 7 4
50.74 17.68 1.7993 7 0 11 2
51.05 1.17 1.7891 -3 1 12 4
51.10 11.20 1.7876 0 2 6 4
51.10 4.50 1.7873 -5 0 13 2
51.35 11.27 1.7793 5 2 3 4
51.43 1.96 1.7766 11 1 4 4
51.44 2.12 1.7765 11 0 7 2
51.44 3.37 1.7763 6 2 0 4
51.47 4.54 1.7754 -2 2 6 4
51.67 4.81 1.7689 -12 1 1 4
51.78 12.73 1.7655 -6 2 2 4
51.96 1.14 1.7597 2 2 6 4
51.98 3.64 1.7591 -10 0 10 2
52.10 5.87 1.7556 -11 1 6 4
52.11 5.05 1.7551 -9 0 11 2
52.27 10.37 1.7502 6 2 2 4
52.35 1.25 1.7478 -12 1 3 4
52.48 5.65 1.7435 -13 0 5 2
52.62 1.86 1.7394 8 1 9 4
52.86 9.29 1.7321 -5 2 5 4
53.00 7.24 1.7277 12 0 6 2
53.01 5.97 1.7274 7 1 10 4
53.03 6.32 1.7267 -5 1 12 4
53.08 7.82 1.7254 -4 2 6 4
53.27 2.36 1.7198 -6 2 4 4
53.27 20.29 1.7195 1 2 7 4
53.63 2.82 1.7090 -12 0 8 2
53.66 4.65 1.7082 2 0 14 2
53.79 1.36 1.7042 12 1 3 4
53.80 1.95 1.7040 -4 0 14 2
53.95 6.57 1.6996 6 1 11 4
54.00 3.24 1.6982 0 1 13 4
54.22 10.73 1.6917 6 2 4 4
54.30 5.46 1.6895 -7 2 3 4
54.73 7.17 1.6770 11 1 6 4
54.83 3.53 1.6742 -10 1 9 4
55.10 3.75 1.6668 0 2 8 4
55.11 6.98 1.6665 2 1 13 4
55.12 6.06 1.6661 7 2 3 4
55.36 4.23 1.6595 -13 0 7 2
55.84 1.25 1.6465 -6 2 6 4
56.00 4.77 1.6421 2 2 8 4
56.40 1.48 1.6314 11 0 9 2
56.49 1.10 1.6290 12 1 5 4
56.61 1.32 1.6259 13 1 2 4
56.83 1.12 1.6201 -4 2 8 4
57.22 2.18 1.6099 6 2 6 4
57.37 2.39 1.6061 12 0 8 2
57.59 9.27 1.6005 7 2 5 4
57.61 1.75 1.6001 -1 1 14 4
57.64 1.06 1.5992 -11 0 11 2
57.74 1.16 1.5966 -10 0 12 2
57.75 10.00 1.5964 1 2 9 4
58.14 9.14 1.5867 1 1 14 4
58.47 5.74 1.5784 8 2 4 4
58.74 1.70 1.5720 -5 0 15 2
58.85 2.42 1.5691 -9 2 3 4
58.98 1.04 1.5661 15 0 1 2
59.34 1.43 1.5574 7 1 12 4
59.40 1.03 1.5560 -6 2 8 4
59.80 3.36 1.5466 3 1 14 4
60.15 3.67 1.5383 -5 2 9 4
60.17 3.50 1.5380 12 1 7 4
60.48 4.47 1.5307 -15 0 5 2
60.70 1.48 1.5258 6 1 13 4
60.80 1.15 1.5235 14 0 6 2
60.86 1.07 1.5221 -14 0 8 2
60.91 1.01 1.5211 2 2 10 4
61.00 6.80 1.5190 -10 2 2 4
61.17 1.20 1.5151 6 2 8 4
61.26 1.65 1.5132 -8 1 13 4
61.45 2.37 1.5089 -14 1 5 4
61.80 1.15 1.5011 5 2 9 4
61.85 3.96 1.5001 2 0 16 2
62.89 1.53 1.4777 16 0 0 2
63.00 1.12 1.4755 -8 2 8 4
63.05 2.35 1.4744 1 2 11 4
63.45 3.27 1.4660 -15 1 2 4
63.46 1.97 1.4659 -12 0 12 2
63.50 1.10 1.4651 13 0 9 2
63.54 1.97 1.4643 -11 0 13 2
63.86 7.61 1.4577 -6 2 10 4
63.89 4.08 1.4571 10 1 11 4
63.92 1.09 1.4564 -6 0 16 2
64.06 4.16 1.4536 11 2 1 4
64.20 5.24 1.4507 9 1 12 4
64.29 5.25 1.4490 -11 2 3 4
64.44 2.71 1.4459 -15 1 4 4
64.52 3.35 1.4442 15 1 2 4
64.73 1.67 1.4402 12 1 9 4
64.83 2.29 1.4381 4 1 15 4
64.86 1.67 1.4375 -6 1 15 4
64.90 4.55 1.4367 14 0 8 2
65.00 2.69 1.4348 8 1 13 4
65.12 9.06 1.4324 -5 2 11 4
65.38 1.44 1.4273 1 0 17 2
65.39 1.17 1.4272 7 2 9 4
65.66 1.51 1.4220 9 2 7 4
65.69 11.48 1.4213 -10 1 13 4
65.75 1.12 1.4203 -2 2 12 4
65.87 2.25 1.4179 13 1 8 4
65.98 1.94 1.4158 6 2 10 4
66.06 1.33 1.4144 16 0 4 2
66.28 2.65 1.4102 7 1 14 4
66.43 3.29 1.4074 -15 1 6 4
66.51 1.10 1.4058 10 2 6 4
66.59 1.73 1.4044 2 2 12 4
66.77 1.34 1.4010 15 0 7 2
66.79 1.31 1.4006 -5 0 17 2
66.82 2.36 1.4001 12 2 0 4
66.90 2.82 1.3987 -12 2 2 4
67.04 2.28 1.3959 3 0 17 2
67.10 1.45 1.3948 -8 0 16 2
67.25 2.84 1.3921 -8 2 10 4
67.55 3.08 1.3868 -10 2 8 4
67.56 1.60 1.3865 3 1 16 4
67.84 3.21 1.3816 11 2 5 4
67.91 1.50 1.3803 -16 1 3 4
68.02 1.70 1.3783 6 1 15 4
68.64 1.46 1.3673 -1 2 13 4
69.09 5.47 1.3595 1 2 13 4
69.24 3.79 1.3570 -3 2 13 4
69.31 2.13 1.3557 17 0 3 2
69.32 3.41 1.3556 -16 1 5 4
69.36 1.08 1.3549 -15 1 8 4
69.52 1.00 1.3521 -12 0 14 2
69.55 1.76 1.3517 -2 1 17 4
69.56 5.08 1.3515 16 1 3 4
69.99 2.28 1.3442 -13 2 1 4
70.00 4.44 1.3440 -12 2 6 4
70.01 1.15 1.3439 8 2 10 4
70.04 3.13 1.3435 -7 1 16 4
70.10 2.18 1.3424 12 1 11 4
70.20 1.53 1.3407 10 1 13 4
70.44 4.31 1.3368 13 2 1 4
70.52 1.59 1.3354 -4 1 17 4
70.57 10.10 1.3346 7 2 11 4
70.87 2.52 1.3297 -5 2 13 4
71.14 1.19 1.3253 11 2 7 4
71.59 2.06 1.3180 -10 2 10 4
71.70 3.14 1.3163 -9 2 11 4
71.72 2.79 1.3159 2 3 1 4
71.82 7.15 1.3144 -17 1 2 4
72.01 3.43 1.3114 -13 2 5 4
72.04 1.86 1.3109 16 1 5 4
72.21 1.64 1.3082 -10 1 15 4
72.44 4.44 1.3046 12 2 6 4
72.69 1.50 1.3008 -17 1 4 4
72.82 1.10 1.2988 4 1 17 4
72.97 1.25 1.2966 17 1 2 4
72.97 1.79 1.2965 -12 2 8 4
72.99 2.80 1.2962 2 2 14 4
73.11 1.18 1.2943 -4 2 14 4
73.20 3.00 1.2930 -15 1 10 4
73.29 1.17 1.2916 4 3 1 4
73.43 1.37 1.2896 15 1 8 4
73.56 1.26 1.2876 -1 0 19 2
73.60 6.04 1.2870 -9 1 16 4
73.94 2.03 1.2819 -3 0 19 2
74.06 6.28 1.2801 -3 1 18 4
74.19 1.07 1.2781 1 0 19 2
74.25 3.30 1.2773 5 3 0 4
74.39 1.95 1.2752 -2 3 5 4
74.44 2.67 1.2745 -13 2 7 4
74.55 1.36 1.2728 -5 3 2 4
74.89 1.11 1.2680 5 3 2 4
74.96 1.57 1.2669 17 1 4 4
74.97 1.60 1.2668 -16 1 9 4
75.18 4.19 1.2637 12 0 14 2
75.38 3.91 1.2609 -1 3 6 4
75.74 4.71 1.2559 -4 3 5 4
75.81 4.41 1.2549 -5 3 4 4
75.85 2.69 1.2543 6 3 1 4
75.92 2.72 1.2533 6 1 17 4
76.17 1.67 1.2498 12 2 8 4
76.24 1.50 1.2489 12 1 13 4
76.40 2.06 1.2467 -6 3 3 4
76.43 2.05 1.2462 13 1 12 4
76.68 1.73 1.2428 -19 0 3 2
77.17 3.36 1.2361 -14 1 13 4
77.36 1.26 1.2335 -5 2 15 4
77.87 2.17 1.2267 17 1 6 4
78.90 3.23 1.2133 -15 2 5 4
78.93 1.76 1.2129 -4 1 19 4
79.06 1.03 1.2113 6 3 5 4
79.12 1.02 1.2105 -8 3 1 4
79.13 5.40 1.2103 -16 1 11 4
79.30 2.30 1.2081 2 1 19 4
79.71 3.82 1.2030 16 1 9 4
79.79 1.77 1.2020 -8 3 3 4
79.79 2.15 1.2019 8 0 18 2
80.12 3.03 1.1979 2 2 16 4
80.15 4.12 1.1975 3 3 8 4
80.68 1.04 1.1910 -18 0 10 2
80.74 1.50 1.1902 18 1 5 4
80.88 1.05 1.1885 -17 1 10 4
81.05 1.20 1.1864 16 2 0 4
81.05 1.16 1.1864 -9 0 19 2
81.08 1.34 1.1860 -5 3 8 4
81.22 2.11 1.1844 -20 0 2 2
81.40 1.09 1.1822 -9 3 2 4
81.56 1.48 1.1803 -12 2 12 4
81.64 1.47 1.1794 -11 2 13 4
82.13 1.87 1.1735 7 3 6 4
82.38 2.20 1.1706 5 3 8 4
82.84 1.75 1.1653 -3 1 20 4
82.88 3.59 1.1649 14 2 8 4
83.18 1.40 1.1613 -19 0 9 2
83.31 1.12 1.1598 1 2 17 4
83.66 1.03 1.1559 9 3 4 4
83.94 1.11 1.1528 16 2 4 4
84.09 1.38 1.1511 18 1 7 4
84.54 1.05 1.1461 20 0 4 2
84.59 1.09 1.1456 15 2 7 4
84.84 1.93 1.1428 3 2 17 4
84.90 1.16 1.1422 -8 2 16 4
85.39 1.12 1.1369 -17 1 12 4
85.58 1.16 1.1349 7 3 8 4
86.07 1.38 1.1297 2 3 11 4
86.14 4.87 1.1289 11 3 0 4
86.25 1.36 1.1278 9 3 6 4
86.47 5.30 1.1254 -4 3 11 4
86.96 1.86 1.1204 17 2 3 4
88.06 2.24 1.1092 -10 3 7 4
89.70 1.98 1.0931 -9 1 20 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.