Borax
Gainsford G J, Kemmitt T, Higham C
Acta Crystallographica E64 (2008) i24-i25
Redetermination of the borax structure from laboratory X-ray data at 145 K
Note T = 145 K
Locality: synthetic
_database_code_amcsd 0019359
CELL PARAMETERS: 11.8843 10.6026 12.2111 90.000 106.790 90.000
SPACE GROUP: C2/c
X-RAY WAVELENGTH: 1.541838
Cell Volume: 1473.060
Density (g/cm3): 1.719
MAX. ABS. INTENSITY / VOLUME**2: 3.040832017
RIR: 0.576
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
11.41 5.85 7.7567 1 1 0 4
12.39 20.12 7.1440 -1 1 1 4
14.90 14.41 5.9464 1 1 1 4
15.16 4.19 5.8453 0 0 2 2
15.58 41.60 5.6888 2 0 0 2
16.72 3.85 5.3013 0 2 0 2
17.10 17.40 5.1847 -1 1 2 4
18.38 82.32 4.8281 0 2 1 4
22.64 25.02 3.9268 0 2 2 4
22.69 16.13 3.9189 -2 2 1 4
22.93 1.07 3.8784 2 2 0 4
24.79 4.52 3.5911 2 0 2 2
24.93 4.81 3.5710 3 1 0 4
25.45 1.46 3.5001 -3 1 2 4
25.58 2.70 3.4819 2 2 1 4
26.41 2.11 3.3751 1 3 0 4
26.86 4.51 3.3194 -1 3 1 4
28.04 5.15 3.1820 3 1 1 4
28.14 1.79 3.1711 1 3 1 4
29.11 8.75 3.0675 -2 2 3 4
30.06 15.84 2.9732 2 2 2 4
30.07 28.48 2.9719 -2 0 4 2
30.49 1.71 2.9321 -1 1 4 4
30.59 7.21 2.9226 0 0 4 2
31.45 26.08 2.8444 4 0 0 2
31.73 59.70 2.8201 1 3 2 4
32.75 1.28 2.7344 3 1 2 4
33.82 5.19 2.6507 0 4 0 2
33.94 3.20 2.6410 -3 1 4 4
34.00 2.07 2.6364 -3 3 1 4
34.69 1.57 2.5856 3 3 0 4
34.70 3.01 2.5850 0 4 1 4
34.87 35.70 2.5729 1 1 4 4
35.08 100.00 2.5583 -3 3 2 4
35.18 17.42 2.5507 -4 2 2 4
35.74 1.52 2.5126 2 2 3 4
36.69 12.80 2.4495 1 3 3 4
37.78 7.66 2.3813 -3 3 3 4
38.48 20.34 2.3394 2 0 4 2
38.55 2.01 2.3353 3 1 3 4
38.61 1.43 2.3321 4 2 1 4
38.74 15.11 2.3242 -2 4 2 4
39.01 1.17 2.3087 -5 1 1 4
39.04 2.80 2.3072 -5 1 2 4
40.85 6.98 2.2091 3 3 2 4
41.04 4.60 2.1992 -4 2 4 4
41.19 4.06 2.1917 0 4 3 4
41.69 1.24 2.1666 -2 4 3 4
41.84 4.42 2.1590 -3 3 4 4
42.22 9.33 2.1403 2 2 4 4
42.38 2.36 2.1326 2 4 2 4
43.41 1.05 2.0846 1 5 0 4
43.62 7.02 2.0752 -5 1 4 4
43.70 4.10 2.0713 -1 5 1 4
44.55 6.28 2.0337 1 5 1 4
44.59 3.52 2.0320 -2 0 6 2
45.12 8.78 2.0096 3 1 4 4
45.25 1.16 2.0040 -1 3 5 4
45.78 1.51 1.9821 3 3 3 4
45.90 1.43 1.9769 -4 4 1 4
46.18 2.47 1.9658 -5 3 1 4
46.20 2.14 1.9649 -5 3 2 4
46.34 1.01 1.9595 -4 4 2 4
46.61 3.59 1.9484 0 0 6 2
46.64 2.14 1.9475 -3 1 6 4
46.78 4.94 1.9420 2 4 3 4
46.98 1.40 1.9340 -3 3 5 4
47.05 2.08 1.9314 1 5 2 4
47.59 7.33 1.9108 -5 3 3 4
47.82 2.35 1.9022 -5 1 5 4
47.95 3.30 1.8974 -2 2 6 4
47.98 5.87 1.8963 6 0 0 2
48.12 4.56 1.8910 -4 4 3 4
48.40 1.88 1.8806 -4 0 6 2
49.13 5.61 1.8543 -6 2 2 4
49.14 8.29 1.8540 -6 0 4 2
49.28 3.25 1.8492 1 3 5 4
49.52 1.54 1.8408 -3 5 2 4
49.86 1.30 1.8288 0 2 6 4
51.14 2.92 1.7860 -4 4 4 4
51.57 2.11 1.7723 -4 2 6 4
51.60 2.83 1.7712 3 3 4 4
51.73 1.75 1.7671 0 6 0 2
52.15 1.07 1.7540 2 4 4 4
52.15 10.20 1.7538 -1 3 6 4
52.16 2.48 1.7534 0 4 5 4
52.57 4.56 1.7409 4 4 2 4
52.98 5.25 1.7282 -3 3 6 4
53.92 12.12 1.7003 5 3 2 4
54.02 2.87 1.6975 6 2 1 4
54.04 2.47 1.6970 3 5 2 4
54.23 3.15 1.6915 0 6 2 4
55.45 2.25 1.6570 -2 2 7 4
56.98 1.87 1.6161 -7 1 4 4
57.12 1.99 1.6127 -2 4 6 4
58.33 1.15 1.5820 2 4 5 4
58.45 1.57 1.5789 -5 5 1 4
58.82 3.11 1.5699 0 4 6 4
59.95 1.31 1.5430 3 1 6 4
59.98 1.05 1.5423 6 4 0 4
60.50 1.51 1.5303 -7 3 2 4
60.99 1.16 1.5192 -6 4 4 4
61.30 4.46 1.5122 0 6 4 4
61.75 1.06 1.5024 2 6 3 4
61.79 6.68 1.5014 1 7 0 4
61.86 1.10 1.4998 5 5 1 4
62.50 3.50 1.4859 -4 0 8 2
65.41 1.29 1.4267 4 0 6 2
65.65 2.87 1.4222 8 0 0 2
66.20 1.74 1.4117 6 4 2 4
66.29 3.99 1.4100 2 6 4 4
70.34 1.38 1.3384 -1 5 7 4
70.41 1.96 1.3372 -3 5 7 4
71.09 1.16 1.3261 2 0 8 2
74.12 2.72 1.2791 -6 6 4 4
75.78 1.10 1.2553 9 1 0 4
76.06 1.79 1.2513 7 5 1 4
77.80 1.33 1.2277 -9 1 6 4
78.57 1.07 1.2175 3 7 4 4
82.46 1.28 1.1697 4 0 8 2
82.63 1.17 1.1677 6 2 6 4
82.72 1.44 1.1667 -9 3 6 4
84.95 1.50 1.1416 0 2 10 4
88.17 1.53 1.1081 7 7 0 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.