Katayamalite
Andrade M B, Doell D, Downs R T, Yang H
Acta Crystallographica E69 (2013) i41-i41
Redetermination of katayamalite, KLi3Ca7Ti2(SiO3)12(OH)2
Locality: Iwagi Island, Inland Sea, Ehime Prefecture, Japan
_database_code_amcsd 0019864
CELL PARAMETERS: 16.9093 9.7287 20.9019 90.000 112.396 90.000
SPACE GROUP: C2/c
X-RAY WAVELENGTH: 1.541838
Cell Volume: 3179.122
Density (g/cm3): 2.897
MAX. ABS. INTENSITY / VOLUME**2: 3.263100899
RIR: 0.367
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
10.71 21.99 8.2600 1 1 0 4
10.77 4.57 8.2165 -1 1 1 4
11.32 6.82 7.8169 2 0 0 2
11.53 8.01 7.6725 -2 0 2 2
12.47 1.20 7.0966 1 1 1 4
12.62 5.85 7.0146 -1 1 2 4
15.45 1.37 5.7343 1 1 2 4
17.52 1.08 5.0618 -2 0 4 2
18.24 2.49 4.8643 0 2 0 2
18.29 1.84 4.8508 -3 1 1 4
18.39 2.02 4.8244 -3 1 2 4
19.10 1.03 4.6463 1 1 3 4
19.32 9.99 4.5938 3 1 0 4
19.33 3.18 4.5927 -1 1 4 4
19.61 1.67 4.5274 -3 1 3 4
20.44 12.46 4.3449 0 2 2 4
21.02 43.42 4.2260 -4 0 2 2
21.07 51.89 4.2160 -2 2 1 4
21.33 10.82 4.1655 3 1 1 4
21.52 16.57 4.1300 2 2 0 4
21.63 14.61 4.1083 -2 2 2 4
21.76 56.16 4.0837 -3 1 4 4
22.91 47.70 3.8819 0 2 3 4
23.12 16.84 3.8465 1 1 4 4
23.36 2.83 3.8073 -1 1 5 4
24.08 74.67 3.6953 3 1 2 4
24.62 19.35 3.6156 -3 1 5 4
25.09 7.65 3.5492 2 0 4 2
25.10 4.39 3.5483 2 2 2 4
25.39 5.47 3.5073 -2 2 4 4
25.59 10.46 3.4817 -2 0 6 2
25.99 33.10 3.4279 0 2 4 4
27.37 12.67 3.2584 3 1 3 4
27.37 1.87 3.2580 1 1 5 4
27.63 7.66 3.2289 -1 1 6 4
27.69 8.20 3.2216 4 0 2 2
27.70 92.20 3.2209 0 0 6 2
27.91 19.09 3.1967 2 2 3 4
27.97 4.72 3.1902 -4 2 2 4
27.98 3.61 3.1889 -5 1 2 4
27.99 65.84 3.1882 -3 1 6 4
28.09 3.90 3.1764 -5 1 3 4
28.10 2.73 3.1753 1 3 0 4
28.12 2.67 3.1728 -1 3 1 4
28.27 6.28 3.1573 -4 2 1 4
28.27 9.71 3.1568 -2 2 5 4
28.41 16.42 3.1415 -4 0 6 2
28.44 1.57 3.1380 -4 2 3 4
28.64 6.87 3.1172 -5 1 1 4
28.84 37.06 3.0952 1 3 1 4
28.91 8.01 3.0883 -1 3 2 4
28.97 49.34 3.0824 -5 1 4 4
29.31 76.53 3.0468 4 2 0 4
29.52 40.85 3.0261 0 2 5 4
29.66 6.58 3.0122 -4 2 4 4
30.02 1.53 2.9768 5 1 0 4
30.30 84.66 2.9497 1 3 2 4
30.54 75.07 2.9268 -5 1 5 4
31.04 61.75 2.8809 4 2 1 4
31.04 38.25 2.8808 3 1 4 4
31.20 6.49 2.8672 2 2 4 4
31.53 8.42 2.8373 -4 2 5 4
31.60 5.66 2.8312 -2 2 6 4
31.71 5.78 2.8214 -3 1 7 4
31.90 4.38 2.8058 -3 3 1 4
31.99 2.64 2.7980 -6 0 2 2
32.04 12.49 2.7936 5 1 1 4
32.23 3.30 2.7778 -6 0 4 2
32.38 32.50 2.7645 1 3 3 4
32.52 16.02 2.7531 -1 3 4 4
32.70 7.87 2.7388 -3 3 3 4
32.73 27.43 2.7361 -5 1 6 4
33.36 19.04 2.6860 4 2 2 4
33.36 9.19 2.6855 0 2 6 4
33.80 5.34 2.6523 3 3 1 4
33.97 13.82 2.6390 -4 2 6 4
34.42 3.40 2.6056 6 0 0 2
34.58 3.76 2.5936 4 0 4 2
34.60 12.00 2.5925 5 1 2 4
34.84 1.00 2.5752 2 2 5 4
35.00 6.02 2.5640 1 3 4 4
35.00 3.75 2.5636 3 1 5 4
35.09 1.92 2.5575 -6 0 6 2
35.16 10.73 2.5523 -1 3 5 4
35.28 3.21 2.5439 -2 2 7 4
35.43 5.73 2.5337 -5 1 7 4
35.71 7.01 2.5140 -3 1 8 4
36.04 1.84 2.4921 -3 3 5 4
36.16 6.01 2.4838 4 2 3 4
36.59 2.45 2.4555 -1 1 8 4
36.87 8.08 2.4379 -6 2 3 4
36.88 7.68 2.4375 -4 2 7 4
37.07 3.56 2.4254 -6 2 2 4
37.22 16.15 2.4157 0 0 8 2
37.26 9.86 2.4131 0 4 1 4
37.28 3.01 2.4122 -6 2 4 4
37.46 1.47 2.4010 0 2 7 4
37.60 7.24 2.3920 5 1 3 4
37.86 2.61 2.3763 -6 2 1 4
38.04 2.01 2.3655 3 3 3 4
38.04 10.28 2.3654 1 3 5 4
38.23 4.66 2.3541 -1 3 6 4
38.27 2.02 2.3516 -6 2 5 4
38.52 2.67 2.3373 -2 4 1 4
38.54 2.28 2.3359 -7 1 4 4
38.55 8.95 2.3355 -5 1 8 4
38.58 1.50 2.3335 -5 3 3 4
38.99 1.38 2.3098 -5 3 1 4
39.08 2.27 2.3047 6 0 2 2
39.37 8.33 2.2886 4 2 4 4
39.61 1.33 2.2754 0 4 3 4
39.74 1.05 2.2682 -2 4 3 4
39.93 1.14 2.2578 -3 1 9 4
40.16 1.84 2.2452 -4 2 8 4
40.98 2.19 2.2025 5 1 4 4
41.39 5.89 2.1814 -3 3 7 4
41.45 6.94 2.1785 1 3 6 4
41.66 2.42 2.1681 -1 3 7 4
42.01 6.95 2.1505 -5 1 9 4
42.20 1.68 2.1413 -5 3 6 4
42.26 2.34 2.1385 -7 1 7 4
42.64 1.49 2.1205 4 0 6 2
42.91 6.58 2.1077 4 2 5 4
43.11 4.39 2.0983 -2 4 5 4
43.41 1.86 2.0846 -2 2 9 4
43.45 1.12 2.0828 6 2 2 4
43.53 10.33 2.0789 7 1 1 4
43.72 4.25 2.0703 5 3 2 4
43.77 4.11 2.0681 -4 2 9 4
44.06 1.40 2.0555 3 3 5 4
44.36 1.01 2.0419 -6 2 8 4
44.41 6.88 2.0400 -5 3 7 4
44.49 5.01 2.0363 -7 1 8 4
44.66 4.68 2.0293 5 1 5 4
45.16 9.01 2.0079 1 3 7 4
45.19 5.27 2.0063 2 4 4 4
45.38 3.97 1.9985 -1 3 8 4
45.41 2.70 1.9974 6 0 4 2
45.44 1.41 1.9960 -4 4 5 4
45.49 4.32 1.9939 -2 4 6 4
45.77 9.71 1.9822 -5 1 10 4
46.23 2.37 1.9638 5 3 3 4
46.64 1.89 1.9473 -6 0 10 2
46.73 9.42 1.9439 4 2 6 4
46.88 2.16 1.9380 -8 2 4 4
46.92 3.79 1.9364 -7 3 3 4
47.01 1.59 1.9328 -8 2 3 4
47.02 8.34 1.9325 0 0 10 2
47.03 3.18 1.9322 -5 3 8 4
47.06 2.24 1.9308 1 5 0 4
47.08 2.46 1.9303 -1 5 1 4
47.25 1.62 1.9236 -6 2 9 4
47.65 1.56 1.9083 -4 2 10 4
47.78 2.19 1.9037 -2 2 10 4
47.93 1.96 1.8981 2 4 5 4
48.21 2.81 1.8875 -3 3 9 4
48.27 3.07 1.8854 -2 4 7 4
48.60 1.01 1.8735 5 1 6 4
48.89 4.52 1.8631 7 1 3 4
49.12 3.32 1.8549 5 3 4 4
49.12 5.93 1.8546 1 3 8 4
49.32 2.17 1.8477 6 2 4 4
49.42 19.01 1.8442 -9 1 4 4
49.51 16.18 1.8410 -6 4 3 4
49.54 19.92 1.8399 -9 1 5 4
49.60 20.46 1.8378 -3 5 1 4
49.64 20.89 1.8364 -3 5 2 4
49.67 20.97 1.8356 -6 4 2 4
49.77 13.15 1.8320 -9 1 3 4
49.79 4.04 1.8315 -5 1 11 4
49.83 17.91 1.8299 -6 4 4 4
49.98 5.40 1.8250 0 4 7 4
50.02 1.53 1.8234 -5 3 9 4
50.04 9.58 1.8228 3 5 0 4
50.15 3.15 1.8192 -9 1 6 4
50.15 3.28 1.8189 -7 1 10 4
50.16 4.78 1.8186 -3 5 3 4
50.24 1.47 1.8161 -7 3 7 4
50.30 1.33 1.8140 -6 4 1 4
50.48 1.99 1.8078 -6 2 10 4
50.63 1.01 1.8029 1 1 10 4
50.80 3.90 1.7974 4 2 7 4
51.02 3.02 1.7901 2 4 6 4
51.37 6.93 1.7787 3 3 7 4
51.40 1.68 1.7777 -2 4 8 4
51.50 1.41 1.7746 4 0 8 2
51.77 3.14 1.7657 -4 2 11 4
51.79 5.02 1.7653 2 2 9 4
51.88 1.37 1.7624 -9 1 1 4
51.93 1.21 1.7607 -1 5 5 4
52.30 1.83 1.7493 3 5 2 4
52.31 1.43 1.7488 8 2 1 4
52.33 1.76 1.7484 -2 2 11 4
52.57 3.92 1.7408 -4 0 12 2
52.58 4.51 1.7406 -3 5 5 4
52.72 5.76 1.7362 -9 1 8 4
52.76 7.37 1.7351 6 2 5 4
52.77 3.00 1.7347 5 1 7 4
52.93 6.86 1.7299 6 4 1 4
52.96 3.21 1.7291 6 0 6 2
53.32 3.43 1.7181 1 3 9 4
53.34 1.02 1.7174 -5 3 10 4
53.50 1.35 1.7129 -7 1 11 4
53.55 1.12 1.7114 -2 0 12 2
53.56 9.26 1.7109 -6 4 7 4
53.57 3.57 1.7107 -1 3 10 4
53.59 7.81 1.7101 9 1 0 4
54.02 7.43 1.6974 -6 2 11 4
54.03 3.59 1.6974 -5 1 12 4
54.08 5.67 1.6957 3 5 3 4
54.38 3.05 1.6873 -6 0 12 2
54.43 4.39 1.6856 -3 5 6 4
54.65 3.17 1.6794 -9 1 9 4
54.88 1.28 1.6729 6 4 2 4
55.09 3.41 1.6671 4 2 8 4
56.11 1.20 1.6390 -4 2 12 4
56.15 7.46 1.6381 -3 3 11 4
56.48 6.54 1.6292 6 2 6 4
57.16 1.13 1.6114 5 1 8 4
57.20 2.31 1.6104 0 0 12 2
57.23 11.59 1.6097 0 4 9 4
57.73 2.10 1.5969 1 3 10 4
57.83 1.53 1.5944 -10 2 4 4
57.84 7.43 1.5941 -6 2 12 4
58.00 1.21 1.5903 -1 3 11 4
58.12 2.08 1.5872 -8 4 5 4
58.15 2.02 1.5864 -2 6 2 4
58.27 1.49 1.5835 -9 3 7 4
58.35 2.10 1.5815 -10 2 3 4
58.48 2.28 1.5783 -5 1 13 4
58.82 1.82 1.5700 -2 6 3 4
58.86 2.08 1.5690 -8 4 6 4
58.88 3.56 1.5685 -9 3 1 4
59.29 2.43 1.5586 -10 2 2 4
59.30 2.15 1.5583 -3 5 8 4
59.59 2.30 1.5515 4 2 9 4
59.65 3.33 1.5499 -9 1 11 4
59.70 2.03 1.5488 3 3 9 4
59.90 3.28 1.5442 -2 6 4 4
59.93 5.35 1.5436 6 4 4 4
60.02 3.71 1.5415 -8 4 7 4
60.20 5.10 1.5372 0 6 4 4
60.47 6.08 1.5309 6 2 7 4
60.64 5.25 1.5270 -10 2 1 4
60.66 3.92 1.5266 -4 2 13 4
60.86 1.40 1.5221 -5 3 12 4
60.95 4.62 1.5201 -6 4 10 4
61.05 2.10 1.5179 -7 1 13 4
61.06 4.80 1.5177 9 1 3 4
61.39 4.74 1.5102 -2 6 5 4
61.44 6.03 1.5091 -9 3 9 4
61.58 4.07 1.5061 -8 4 8 4
61.71 1.24 1.5031 -11 1 7 4
61.72 5.45 1.5029 3 5 6 4
61.76 6.00 1.5021 5 1 9 4
61.92 4.63 1.4985 -6 2 13 4
62.01 2.75 1.4966 -11 1 3 4
62.07 2.39 1.4952 0 6 5 4
62.25 1.33 1.4913 -7 5 1 4
62.26 3.91 1.4911 -3 5 9 4
62.34 2.11 1.4894 7 3 5 4
62.35 1.78 1.4892 1 3 11 4
62.39 1.45 1.4884 10 2 0 4
62.43 5.38 1.4876 9 3 1 4
62.57 1.73 1.4845 8 4 1 4
62.63 5.13 1.4833 -1 3 12 4
62.67 1.22 1.4824 -11 1 8 4
62.67 2.51 1.4824 -7 5 6 4
62.68 2.68 1.4823 -9 1 12 4
62.97 1.83 1.4761 6 4 5 4
63.03 1.64 1.4748 2 6 4 4
63.13 1.24 1.4726 -5 1 14 4
63.23 2.92 1.4707 -4 6 5 4
63.49 2.90 1.4652 7 1 7 4
63.53 3.54 1.4645 -3 1 14 4
63.58 1.04 1.4634 -10 2 10 4
63.78 1.72 1.4592 5 3 8 4
64.32 1.48 1.4484 4 6 2 4
64.32 2.50 1.4483 0 6 6 4
64.51 1.71 1.4444 10 2 1 4
64.94 1.06 1.4360 7 5 1 4
65.42 3.63 1.4267 -4 2 14 4
65.51 2.17 1.4248 -2 6 7 4
65.55 1.74 1.4242 0 4 11 4
65.64 1.68 1.4223 -8 2 13 4
65.68 3.95 1.4217 0 2 13 4
65.83 2.93 1.4186 -8 4 10 4
66.12 1.42 1.4131 -9 3 11 4
66.34 1.64 1.4091 2 4 10 4
66.57 3.01 1.4048 5 1 10 4
66.65 1.85 1.4033 1 5 9 4
66.84 2.76 1.3997 -2 4 12 4
66.86 1.03 1.3994 7 5 2 4
66.87 1.24 1.3992 -1 5 10 4
66.88 1.12 1.3990 -12 0 4 2
67.00 1.80 1.3968 10 2 2 4
67.22 1.24 1.3928 8 4 3 4
67.43 1.78 1.3889 -12 0 8 2
67.44 1.70 1.3887 -7 3 13 4
67.47 2.83 1.3882 -1 3 13 4
67.66 1.07 1.3847 8 2 6 4
67.70 1.03 1.3841 -11 3 4 4
67.74 1.34 1.3833 -7 5 9 4
67.79 1.01 1.3824 -10 4 6 4
67.80 1.63 1.3823 2 6 6 4
67.82 5.18 1.3818 3 1 12 4
67.87 1.08 1.3809 -11 1 11 4
67.90 6.18 1.3804 0 0 14 2
68.06 1.07 1.3775 1 7 1 4
68.11 3.14 1.3767 6 6 0 4
68.52 3.22 1.3694 -6 6 6 4
68.60 1.41 1.3680 -10 2 12 4
68.90 1.06 1.3628 -10 4 2 4
68.95 2.24 1.3619 3 3 11 4
68.97 1.79 1.3617 -12 0 2 2
68.98 1.22 1.3614 -11 3 8 4
69.42 1.65 1.3538 -5 3 14 4
69.47 2.28 1.3531 -12 2 6 4
69.53 4.39 1.3521 -12 2 5 4
69.57 1.08 1.3514 -9 5 4 4
69.67 1.53 1.3497 -9 5 5 4
69.75 4.19 1.3483 -3 7 2 4
69.83 1.16 1.3470 10 2 3 4
69.85 4.83 1.3465 -9 5 3 4
70.05 1.96 1.3432 -12 0 10 2
70.07 2.88 1.3429 3 7 0 4
70.16 4.24 1.3414 -9 5 6 4
70.17 2.52 1.3412 -3 7 3 4
70.38 3.64 1.3377 -4 2 15 4
70.51 4.24 1.3355 -12 2 8 4
70.81 1.95 1.3307 -12 2 3 4
70.81 2.88 1.3306 3 7 1 4
70.98 1.59 1.3279 0 2 14 4
71.06 1.37 1.3266 -2 6 9 4
71.09 2.48 1.3261 6 6 2 4
71.50 1.61 1.3195 -8 4 12 4
71.58 1.02 1.3182 -9 5 1 4
71.59 4.11 1.3181 5 1 11 4
71.76 2.21 1.3154 -6 6 8 4
72.17 1.45 1.3090 -3 7 5 4
72.53 4.10 1.3033 -1 3 14 4
72.99 1.70 1.2963 10 2 4 4
73.43 1.01 1.2895 1 7 5 4
73.45 1.53 1.2892 -13 1 6 4
73.64 1.16 1.2864 -8 6 4 4
73.72 1.55 1.2851 -5 7 2 4
74.17 1.41 1.2785 -3 1 16 4
74.33 1.33 1.2761 -2 6 10 4
74.81 1.77 1.2691 -3 3 15 4
74.83 1.13 1.2689 -8 4 13 4
75.58 1.42 1.2581 -4 2 16 4
75.83 1.83 1.2546 -1 7 7 4
76.11 1.53 1.2506 10 4 2 4
76.35 1.69 1.2473 -11 3 12 4
77.30 1.22 1.2343 11 3 2 4
77.63 1.49 1.2299 -10 4 12 4
78.30 1.54 1.2211 1 7 7 4
79.33 3.28 1.2078 0 0 16 2
79.39 1.65 1.2070 -14 0 6 2
79.67 3.24 1.2035 -7 7 4 4
79.67 1.01 1.2034 -12 2 13 4
79.76 2.65 1.2023 -6 4 15 4
79.98 3.03 1.1996 9 1 8 4
80.51 1.47 1.1930 12 2 2 4
80.56 1.18 1.1924 8 4 7 4
80.90 3.29 1.1883 3 5 11 4
81.36 1.06 1.1827 2 6 10 4
81.47 1.45 1.1813 -14 0 10 2
81.59 2.92 1.1800 7 7 0 4
81.70 2.67 1.1786 -3 5 14 4
82.15 2.39 1.1733 -11 5 9 4
82.34 1.77 1.1711 9 5 4 4
82.39 3.65 1.1705 -9 1 17 4
82.44 1.85 1.1699 -12 4 1 4
82.51 2.56 1.1691 -13 3 2 4
82.69 2.50 1.1670 -2 8 5 4
82.77 3.61 1.1661 6 4 10 4
83.12 1.19 1.1621 1 1 16 4
83.54 2.39 1.1573 -3 7 10 4
83.72 1.84 1.1553 -12 4 11 4
83.76 1.15 1.1548 -13 3 11 4
83.97 2.21 1.1524 -9 5 13 4
84.15 1.21 1.1504 2 8 4 4
84.71 1.08 1.1443 8 4 8 4
84.71 2.36 1.1443 -14 0 12 2
84.74 4.79 1.1439 7 7 2 4
85.31 1.15 1.1377 0 8 6 4
85.40 1.26 1.1368 4 2 14 4
85.55 1.05 1.1352 9 5 5 4
85.81 1.82 1.1324 -12 2 15 4
86.26 2.38 1.1276 3 7 8 4
86.27 1.68 1.1276 13 3 0 4
86.40 1.22 1.1262 -2 8 7 4
87.83 1.43 1.1115 -7 7 10 4
87.99 1.56 1.1098 -11 5 12 4
88.17 1.78 1.1081 -9 3 17 4
88.68 1.07 1.1030 13 3 1 4
88.79 1.30 1.1019 -2 8 8 4
89.19 1.33 1.0981 8 4 9 4
89.34 2.52 1.0966 7 7 4 4
89.39 1.25 1.0961 -14 0 14 2
89.41 1.21 1.0959 -12 2 16 4
89.94 1.13 1.0908 7 5 9 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.