Gratonite
Ribar B, Nowacki W
Zeitschrift fur Kristallographie 128 (1969) 321-338
Neubestimmung der kristallstruktur von gratonit, Pb9As4S15
Locality: Wiesloch, Germany
_database_code_amcsd 0010673
CELL PARAMETERS: 17.7580 17.7580 7.8070 90.000 90.000 120.000
SPACE GROUP: R3m
X-RAY WAVELENGTH: 1.541838
Cell Volume: 2132.077
Density (g/cm3): 6.180
MAX. ABS. INTENSITY / VOLUME**2: 129.9391124
RIR: 6.846
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
9.96 9.42 8.8790 1 1 0 6
16.18 17.42 5.4783 0 2 1 3
17.30 1.66 5.1263 3 0 0 3
19.04 12.63 4.6623 2 1 1 6
20.00 6.25 4.4395 2 2 0 6
23.51 37.08 3.7835 0 1 2 3
23.77 47.57 3.7431 1 3 1 6
25.59 1.15 3.4807 2 0 2 3
25.83 100.00 3.4491 4 0 1 3
26.56 20.92 3.3559 4 1 0 6
27.52 29.15 3.2406 1 2 2 6
27.75 3.99 3.2151 3 2 1 6
31.06 11.31 2.8796 3 1 2 6
31.26 50.44 2.8617 0 5 1 3
32.69 40.52 2.7392 0 4 2 3
32.88 18.65 2.7237 2 4 1 6
34.26 2.45 2.6174 2 3 2 6
34.44 1.41 2.6040 5 1 1 6
34.46 2.69 2.6023 0 0 3 1
35.01 8.75 2.5631 6 0 0 3
35.96 8.89 2.4973 1 1 3 6
37.22 9.12 2.4159 5 0 2 3
37.39 9.65 2.4053 4 3 1 6
38.62 7.13 2.3312 4 2 2 6
38.81 10.34 2.3205 0 3 3 3
38.81 5.49 2.3205 3 0 3 3
39.99 1.17 2.2547 1 5 2 6
40.15 6.09 2.2461 1 6 1 6
40.17 2.02 2.2451 2 2 3 6
40.64 35.02 2.2197 4 4 0 6
42.60 2.30 2.1220 3 4 2 6
42.76 1.96 2.1148 3 5 1 6
44.01 4.60 2.0573 6 2 1 6
44.03 19.22 2.0565 4 1 3 6
44.03 9.95 2.0565 1 4 3 6
44.48 4.04 2.0370 7 1 0 6
45.10 8.26 2.0103 6 1 2 6
46.47 10.00 1.9543 3 3 3 6
46.93 7.65 1.9362 1 0 4 3
47.49 10.36 1.9146 5 3 2 6
47.49 8.72 1.9146 0 7 2 3
47.63 3.08 1.9093 5 4 1 6
48.79 8.13 1.8666 0 8 1 3
49.25 4.81 1.8502 2 1 4 6
51.06 8.16 1.7887 5 2 3 6
51.06 1.58 1.7887 2 5 3 6
51.46 1.49 1.7758 5 5 0 6
52.02 12.71 1.7581 4 5 2 6
52.15 12.18 1.7539 8 1 1 6
52.59 1.57 1.7403 4 0 4 3
53.11 4.33 1.7246 8 0 2 3
53.23 8.11 1.7207 4 6 1 6
53.64 1.16 1.7088 9 0 0 3
53.67 3.77 1.7078 3 2 4 6
54.18 2.68 1.6929 7 2 2 6
54.31 1.56 1.6893 7 3 1 6
54.70 4.50 1.6780 8 2 0 6
55.78 2.98 1.6480 0 5 4 3
56.28 1.38 1.6346 1 8 2 6
56.82 2.16 1.6203 2 4 4 6
57.45 1.29 1.6040 1 7 3 6
57.45 1.30 1.6040 7 1 3 6
57.82 4.06 1.5947 7 4 0 6
58.33 2.10 1.5818 3 7 2 6
59.87 2.55 1.5450 4 3 4 6
61.45 1.11 1.5089 10 0 1 3
61.49 1.81 1.5079 1 2 5 6
61.84 5.41 1.5002 1 6 4 6
62.31 3.54 1.4901 5 6 2 6
62.43 1.34 1.4876 9 2 1 6
63.44 2.06 1.4662 3 1 5 6
63.79 3.00 1.4591 3 5 4 6
64.25 3.74 1.4498 8 3 2 6
64.36 3.85 1.4475 5 7 1 6
64.40 4.58 1.4467 0 4 5 3
65.20 2.16 1.4308 0 10 2 3
65.32 4.15 1.4286 8 4 1 6
65.33 3.58 1.4284 0 9 3 3
65.33 1.61 1.4284 9 0 3 3
65.67 3.08 1.4218 9 3 0 6
66.15 1.88 1.4126 2 9 2 6
67.24 2.96 1.3923 5 0 5 3
67.58 5.80 1.3862 5 4 4 6
68.14 2.69 1.3762 0 11 1 3
68.18 2.43 1.3755 4 2 5 6
69.08 5.27 1.3597 4 7 3 6
69.08 3.85 1.3597 7 4 3 6
69.41 1.18 1.3540 8 5 0 6
70.94 1.18 1.3285 3 4 5 6
71.82 1.23 1.3145 11 1 1 6
71.82 3.81 1.3145 4 9 1 6
72.67 1.90 1.3012 0 0 6 1
73.09 1.91 1.2947 7 3 4 6
73.96 1.04 1.2816 12 0 0 3
74.54 2.75 1.2731 1 10 3 6
74.54 1.76 1.2731 10 1 3 6
75.31 1.17 1.2619 9 4 2 6
76.25 1.32 1.2486 2 2 6 6
76.67 1.60 1.2430 6 5 4 6
77.53 2.22 1.2313 10 4 0 6
78.44 1.04 1.2193 3 8 4 6
78.91 1.23 1.2132 1 4 6 6
79.00 1.22 1.2120 8 0 5 3
79.74 1.72 1.2026 8 6 2 6
79.85 1.49 1.2012 8 5 3 6
80.19 2.54 1.1969 9 2 4 6
81.63 1.32 1.1795 1 8 5 6
82.36 1.25 1.1709 12 1 2 6
82.50 1.06 1.1692 6 4 5 6
83.33 1.82 1.1596 12 2 1 6
83.37 1.15 1.1592 3 7 5 6
84.10 1.01 1.1510 11 3 2 6
85.08 1.10 1.1402 7 7 3 6
86.75 3.08 1.1225 4 4 6 6
89.29 1.22 1.0970 4 11 2 6
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.