Plagionite
Cho S A, Wuensch B J
Zeitschrift fur Kristallographie 139 (1974) 351-378
The crystal structure of plagionite, Pb5Sb8S17,
the second member in the homologous series Pb3+2nSb8S15+2n
Locality: Wolfsberg, Harz, Germany
_database_code_amcsd 0010763
CELL PARAMETERS: 13.4857 11.8656 19.9834 90.000 107.168 90.000
SPACE GROUP: C2/c
X-RAY WAVELENGTH: 1.541838
Cell Volume: 3055.185
Density (g/cm3): 5.554
MAX. ABS. INTENSITY / VOLUME**2: 29.96054874
RIR: 1.756
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
9.26 14.63 9.5465 0 0 2 2
10.13 3.67 8.7284 1 1 0 4
10.27 3.04 8.6164 -1 1 1 4
11.96 14.75 7.3985 1 1 1 4
13.75 3.60 6.4424 2 0 0 2
14.13 13.02 6.2662 -2 0 2 2
14.93 1.44 5.9328 0 2 0 2
15.06 34.64 5.8825 1 1 2 4
15.64 10.16 5.6656 0 2 1 4
17.60 2.57 5.0390 0 2 2 4
18.75 2.04 4.7317 2 0 2 2
19.33 12.66 4.5923 -1 1 4 4
19.94 2.58 4.4522 -2 2 1 4
20.35 1.54 4.3642 2 2 0 4
20.47 39.68 4.3397 0 2 3 4
21.19 14.66 4.1938 -3 1 1 4
21.38 3.50 4.1563 -3 1 2 4
21.78 3.65 4.0809 2 2 1 4
22.28 5.96 3.9906 -2 2 3 4
22.56 25.70 3.9404 -3 1 3 4
22.95 100.00 3.8745 1 1 4 4
23.49 2.31 3.7876 -1 1 5 4
23.53 47.61 3.7811 1 3 0 4
23.59 60.37 3.7718 -1 3 1 4
23.93 3.51 3.7190 0 2 4 4
24.39 10.93 3.6493 1 3 1 4
24.56 14.02 3.6245 -1 3 2 4
24.61 38.89 3.6177 -3 1 4 4
24.74 25.28 3.5991 -2 2 4 4
26.09 14.87 3.4155 1 3 2 4
26.24 6.41 3.3965 3 1 2 4
26.31 5.86 3.3868 2 0 4 2
26.46 16.31 3.3681 -4 0 2 2
26.98 63.55 3.3043 2 2 3 4
27.30 48.02 3.2668 1 1 5 4
27.33 68.52 3.2634 -3 1 5 4
27.35 1.55 3.2608 -2 0 6 2
27.69 71.44 3.2212 4 0 0 2
27.80 98.03 3.2094 -2 2 5 4
28.48 2.34 3.1337 1 3 3 4
29.30 1.66 3.0486 3 1 3 4
30.13 9.48 2.9664 0 4 0 2
30.13 27.79 2.9659 -3 3 1 4
30.27 9.45 2.9526 -3 3 2 4
30.39 52.48 2.9413 2 2 4 4
30.50 3.22 2.9312 0 4 1 4
30.52 1.23 2.9290 -4 2 2 4
30.56 42.23 2.9251 -3 1 6 4
30.70 13.49 2.9120 -4 2 1 4
30.73 77.28 2.9095 3 3 0 4
31.07 28.08 2.8786 -4 2 3 4
31.14 3.71 2.8721 -3 3 3 4
31.43 2.85 2.8463 1 3 4 4
31.58 2.59 2.8328 0 4 2 4
31.61 1.58 2.8309 4 2 0 4
31.80 2.23 2.8141 1 1 6 4
31.83 4.21 2.8111 4 0 2 2
32.03 50.41 2.7942 3 3 1 4
32.31 21.76 2.7705 -4 2 4 4
32.37 1.88 2.7656 -1 1 7 4
32.78 2.22 2.7318 3 1 4 4
32.99 8.10 2.7148 -2 4 1 4
33.25 16.66 2.6945 2 4 0 4
33.32 1.26 2.6887 0 4 3 4
33.42 4.43 2.6811 -2 4 2 4
33.96 4.48 2.6398 3 3 2 4
34.10 3.66 2.6292 -5 1 2 4
34.15 64.30 2.6254 2 2 5 4
34.18 8.40 2.6231 -3 1 7 4
34.19 16.20 2.6228 -4 2 5 4
34.51 1.90 2.5991 -2 4 3 4
34.56 1.05 2.5956 -5 1 1 4
34.83 4.04 2.5758 -3 3 5 4
35.14 8.04 2.5539 -2 2 7 4
35.17 1.27 2.5517 -5 1 4 4
35.33 1.17 2.5404 4 2 2 4
36.07 35.68 2.4902 -2 0 8 2
36.42 1.81 2.4668 1 1 7 4
36.43 1.00 2.4662 3 3 3 4
36.64 1.28 2.4524 -5 1 5 4
37.48 1.09 2.3994 -3 3 6 4
37.69 5.27 2.3866 0 0 8 2
37.83 1.82 2.3781 2 4 3 4
37.99 11.54 2.3684 4 2 3 4
38.10 1.07 2.3617 -3 1 8 4
38.43 12.88 2.3426 0 4 5 4
38.44 1.58 2.3420 -2 4 5 4
38.52 1.05 2.3370 1 3 6 4
39.01 1.96 2.3090 -1 3 7 4
40.23 1.74 2.2416 -6 0 2 2
40.45 5.27 2.2301 -1 5 3 4
40.49 13.56 2.2278 -5 3 2 4
40.56 1.68 2.2241 -3 3 7 4
40.67 5.14 2.2184 -5 3 3 4
40.88 16.80 2.2073 -5 3 1 4
40.95 2.01 2.2037 -4 4 3 4
41.07 4.41 2.1976 4 2 4 4
41.18 1.57 2.1920 -5 1 7 4
41.38 4.67 2.1821 4 4 0 4
41.62 12.92 2.1698 0 4 6 4
41.76 16.52 2.1631 -1 1 9 4
41.84 3.70 2.1591 5 3 0 4
41.94 3.08 2.1543 1 5 3 4
41.94 1.17 2.1541 -4 4 4 4
42.18 75.11 2.1423 -1 5 4 4
42.45 7.49 2.1295 2 2 7 4
42.51 6.70 2.1264 1 3 7 4
43.03 1.81 2.1021 -1 3 8 4
43.32 2.83 2.0887 -6 0 6 2
43.46 5.43 2.0824 -4 4 5 4
43.55 2.80 2.0784 -2 2 9 4
43.55 11.08 2.0781 -6 2 4 4
43.88 7.74 2.0634 -3 5 3 4
44.00 3.21 2.0580 -3 3 8 4
44.09 1.64 2.0538 1 5 4 4
44.19 8.20 2.0496 2 0 8 2
44.24 1.60 2.0474 -2 4 7 4
44.40 8.92 2.0404 4 4 2 4
44.56 38.03 2.0335 -6 2 5 4
45.16 8.28 2.0078 0 4 7 4
45.29 3.72 2.0021 5 3 2 4
45.30 25.91 2.0017 5 1 4 4
45.46 6.17 1.9953 -4 4 6 4
45.60 1.24 1.9892 4 0 6 2
46.02 6.71 1.9720 3 5 2 4
46.07 5.26 1.9702 -6 2 6 4
46.52 1.25 1.9522 6 2 1 4
46.62 17.07 1.9483 -1 1 10 4
46.69 7.73 1.9456 1 5 5 4
46.70 3.99 1.9449 -3 5 5 4
46.74 2.01 1.9436 1 3 8 4
47.04 1.79 1.9319 -1 5 6 4
47.28 3.95 1.9226 -1 3 9 4
47.40 5.06 1.9178 -5 1 9 4
47.63 1.12 1.9093 0 0 10 2
47.66 3.02 1.9080 -4 0 10 2
47.68 1.90 1.9073 -2 4 8 4
47.74 10.12 1.9051 -3 3 9 4
47.83 6.03 1.9016 -7 1 3 4
47.90 11.00 1.8993 -6 0 8 2
47.90 2.61 1.8992 -4 4 7 4
47.94 5.99 1.8975 -2 6 1 4
47.97 2.70 1.8964 3 5 3 4
48.04 5.90 1.8938 -2 2 10 4
48.05 6.56 1.8934 -7 1 4 4
48.13 6.93 1.8905 2 6 0 4
48.26 1.09 1.8859 -2 6 2 4
48.72 12.38 1.8690 5 1 5 4
48.77 1.84 1.8672 -7 1 5 4
48.82 15.51 1.8656 2 6 1 4
48.82 1.50 1.8655 -3 5 6 4
48.89 4.17 1.8628 -7 1 1 4
48.99 7.88 1.8595 0 4 8 4
49.07 2.67 1.8567 -2 6 3 4
49.27 4.02 1.8496 4 4 4 4
49.43 6.29 1.8440 -5 3 8 4
49.46 3.21 1.8428 3 1 8 4
50.06 6.79 1.8221 -1 5 7 4
50.35 11.91 1.8123 3 5 4 4
50.46 1.00 1.8085 2 4 7 4
50.52 3.08 1.8066 5 3 4 4
50.73 1.20 1.7996 -4 4 8 4
51.01 7.55 1.7902 -5 1 10 4
51.11 12.26 1.7870 6 2 3 4
51.17 8.31 1.7853 1 3 9 4
51.53 3.83 1.7736 2 2 9 4
51.56 2.25 1.7724 6 0 4 2
51.59 4.17 1.7715 -1 1 11 4
51.61 1.15 1.7708 -5 5 1 4
51.63 4.15 1.7703 -7 1 7 4
51.73 3.02 1.7670 -1 3 10 4
52.06 15.95 1.7567 -5 5 4 4
52.08 1.76 1.7561 0 6 5 4
52.28 5.79 1.7498 4 4 5 4
52.44 1.49 1.7449 5 1 6 4
52.46 1.71 1.7442 -5 3 9 4
52.61 10.05 1.7395 6 4 0 4
53.07 4.79 1.7256 0 4 9 4
53.67 1.54 1.7078 -6 4 6 4
53.85 5.68 1.7025 -7 3 1 4
53.92 10.52 1.7005 -4 4 9 4
53.99 1.91 1.6982 6 2 4 4
54.00 1.55 1.6980 7 1 2 4
54.07 2.18 1.6961 6 4 1 4
54.13 8.24 1.6944 3 1 9 4
54.16 2.10 1.6934 4 0 8 2
54.64 5.29 1.6798 -1 7 1 4
54.64 2.56 1.6797 0 6 6 4
54.68 2.13 1.6786 -5 5 6 4
54.94 7.77 1.6711 -8 0 2 2
55.03 5.25 1.6688 7 3 0 4
55.79 2.33 1.6479 1 3 10 4
55.83 4.74 1.6466 -5 3 10 4
55.92 3.19 1.6444 1 7 2 4
56.32 5.90 1.6334 2 2 10 4
56.39 2.81 1.6317 -6 2 10 4
56.61 1.39 1.6257 1 5 8 4
56.69 2.77 1.6236 -1 1 12 4
56.80 1.25 1.6209 -2 6 7 4
56.83 1.03 1.6201 -8 2 4 4
57.19 9.07 1.6106 8 0 0 2
57.28 1.89 1.6085 -8 2 5 4
57.43 8.88 1.6047 -4 4 10 4
57.96 1.91 1.5911 0 0 12 2
58.16 3.20 1.5862 -8 2 1 4
58.18 3.66 1.5855 -3 7 1 4
58.27 2.15 1.5835 -3 7 2 4
58.73 2.19 1.5721 -4 2 12 4
58.77 2.12 1.5711 3 3 9 4
59.29 1.22 1.5587 4 4 7 4
59.33 4.32 1.5576 3 7 1 4
59.68 1.09 1.5493 3 5 7 4
59.85 1.06 1.5452 -6 2 11 4
59.89 1.60 1.5443 -4 6 7 4
60.74 5.84 1.5248 -7 3 9 4
60.83 2.16 1.5228 0 6 8 4
60.96 2.96 1.5198 5 3 7 4
61.21 1.05 1.5142 -1 3 12 4
61.39 2.02 1.5103 -1 7 6 4
61.94 2.34 1.4982 -1 1 13 4
62.05 2.28 1.4957 -7 5 3 4
62.17 2.22 1.4932 3 7 3 4
62.35 1.03 1.4893 -4 6 8 4
62.57 1.35 1.4846 -2 2 13 4
62.59 2.97 1.4841 -6 6 3 4
62.80 1.21 1.4797 5 5 5 4
62.96 1.86 1.4763 -6 6 4 4
63.23 6.73 1.4706 4 4 8 4
63.26 1.15 1.4700 -9 1 2 4
63.32 5.10 1.4687 -4 2 13 4
63.37 1.17 1.4678 -9 1 6 4
63.39 1.23 1.4674 3 3 10 4
63.45 2.18 1.4660 -5 1 13 4
63.46 2.26 1.4658 -7 3 10 4
63.47 3.07 1.4656 0 8 2 4
63.65 1.82 1.4620 -8 0 10 2
63.86 1.17 1.4576 -7 5 6 4
63.94 1.13 1.4560 -8 4 2 4
64.00 2.71 1.4547 6 6 0 4
64.02 1.20 1.4545 7 5 0 4
64.41 2.57 1.4466 0 6 9 4
64.51 1.14 1.4445 0 8 3 4
64.57 1.28 1.4433 -2 8 2 4
64.60 1.25 1.4427 6 2 7 4
64.77 1.11 1.4393 -8 4 6 4
64.91 1.04 1.4366 -3 5 11 4
65.16 2.72 1.4317 -4 6 9 4
65.18 1.07 1.4313 -3 3 13 4
65.27 3.98 1.4295 -5 7 1 4
65.29 5.24 1.4290 6 6 1 4
65.47 2.18 1.4257 0 2 13 4
65.49 1.02 1.4253 7 5 1 4
65.78 1.50 1.4196 8 2 3 4
65.95 1.36 1.4164 0 8 4 4
65.96 2.54 1.4162 5 7 0 4
66.04 1.65 1.4147 -4 0 14 2
66.32 1.35 1.4095 -2 8 4 4
66.46 1.77 1.4068 1 7 7 4
66.53 1.71 1.4055 -7 3 11 4
66.63 1.48 1.4036 6 0 8 2
66.94 1.05 1.3979 -9 3 3 4
67.35 1.30 1.3904 7 5 2 4
67.44 2.24 1.3886 4 4 9 4
67.50 1.31 1.3876 9 1 1 4
67.56 1.56 1.3865 -3 7 8 4
67.76 1.17 1.3830 -9 1 9 4
68.09 3.13 1.3770 -5 1 14 4
68.31 1.11 1.3731 -4 6 10 4
68.50 1.11 1.3698 -9 3 1 4
68.55 1.73 1.3690 5 7 2 4
68.84 3.32 1.3638 0 0 14 2
68.94 1.81 1.3622 -2 4 13 4
69.14 1.34 1.3586 2 8 4 4
69.15 1.52 1.3584 1 5 11 4
69.21 2.60 1.3574 3 1 12 4
69.32 2.09 1.3556 3 7 6 4
69.63 1.15 1.3502 8 4 2 4
69.64 1.92 1.3502 -8 4 9 4
69.66 1.59 1.3499 1 7 8 4
69.98 2.37 1.3443 0 8 6 4
69.98 2.80 1.3443 -9 1 10 4
70.08 2.88 1.3428 -9 3 8 4
70.10 2.05 1.3423 -3 3 14 4
70.21 4.73 1.3406 -4 8 4 4
70.44 4.42 1.3367 -3 7 9 4
71.28 1.04 1.3231 2 8 5 4
71.79 1.36 1.3149 -4 6 11 4
71.86 1.65 1.3138 -10 2 5 4
71.98 1.16 1.3118 4 8 2 4
72.01 1.20 1.3114 -8 4 10 4
72.18 3.52 1.3088 7 5 4 4
72.33 1.57 1.3064 -10 0 8 2
72.37 1.24 1.3058 1 9 1 4
72.77 2.00 1.2996 -4 8 6 4
73.12 1.99 1.2942 6 2 9 4
73.18 1.84 1.2933 1 7 9 4
73.29 1.58 1.2916 8 0 6 2
73.30 1.26 1.2915 3 3 12 4
73.77 1.28 1.2844 2 8 6 4
73.91 1.50 1.2823 -2 4 14 4
74.12 1.37 1.2792 7 3 7 4
74.31 1.20 1.2764 -8 6 5 4
74.96 4.06 1.2670 -9 5 4 4
75.12 1.94 1.2646 9 1 4 4
75.12 1.07 1.2646 7 5 5 4
75.31 3.83 1.2620 -8 2 13 4
75.39 1.13 1.2608 -7 7 1 4
75.59 1.39 1.2580 -4 6 12 4
75.64 2.27 1.2573 -3 9 3 4
75.78 4.85 1.2553 -9 5 6 4
75.92 2.37 1.2532 -10 0 10 2
76.24 2.84 1.2488 1 3 14 4
76.62 1.06 1.2435 2 8 7 4
77.60 1.01 1.2303 4 6 9 4
77.66 1.22 1.2295 -7 3 14 4
77.81 2.26 1.2275 8 4 5 4
77.81 1.58 1.2275 2 4 13 4
78.01 2.12 1.2248 -6 4 14 4
78.64 2.82 1.2166 7 1 9 4
78.80 1.62 1.2146 -9 1 13 4
79.02 2.53 1.2118 -2 6 13 4
79.15 1.22 1.2101 -2 4 15 4
79.21 1.59 1.2093 -6 8 6 4
80.68 1.38 1.1909 -6 8 7 4
80.83 1.25 1.1891 4 8 6 4
81.31 3.72 1.1833 -7 7 9 4
81.50 1.24 1.1810 5 7 7 4
81.59 1.17 1.1799 7 7 3 4
82.22 1.82 1.1725 10 2 3 4
82.51 1.78 1.1690 -3 1 17 4
83.13 1.04 1.1620 5 9 1 4
83.21 1.87 1.1610 2 10 1 4
83.79 1.03 1.1545 -2 6 14 4
84.59 1.15 1.1456 -8 6 11 4
85.03 1.35 1.1408 4 0 14 2
85.08 1.81 1.1403 -11 3 1 4
86.40 1.02 1.1261 -3 3 17 4
86.69 1.88 1.1231 11 3 0 4
87.58 1.97 1.1140 2 6 13 4
87.67 1.86 1.1131 -8 8 4 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.