Na10 P6 Sn2 Eisenmann B, Klein J, Somer M Zeitschrift fur Kristallographie 197 (1991) 269-270 Crystal structure of decasodium di-mue-phosphidobis(diphosphidostannate(IV)) _cod_database_code 1008463 _database_code_amcsd 0016367 CELL PARAMETERS: 13.4000 7.4560 8.2890 90.000 90.200 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 828.152 Density (g/cm3): 2.619 MAX. ABS. INTENSITY / VOLUME**2: 13.11881016 RIR: 1.631 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.54 30.13 7.0603 -1 0 1 2 12.58 100.00 7.0383 1 0 1 2 13.21 15.88 6.7000 2 0 0 2 13.59 46.69 6.5153 1 1 0 4 15.99 48.02 5.5433 0 1 1 4 17.30 50.93 5.1266 -1 1 1 4 17.80 50.07 4.9835 2 1 0 4 20.82 15.48 4.2661 2 1 1 4 21.44 16.72 4.1445 0 0 2 2 22.58 16.72 3.9378 -3 0 1 2 22.65 8.87 3.9264 3 0 1 2 23.87 10.15 3.7280 0 2 0 2 24.57 2.62 3.6225 0 1 2 4 24.79 8.20 3.5916 1 2 0 4 25.23 3.94 3.5302 -2 0 2 2 25.31 12.06 3.5191 2 0 2 2 25.49 15.65 3.4942 1 1 2 4 25.58 6.55 3.4820 -3 1 1 4 25.64 7.29 3.4741 3 1 1 4 26.21 5.13 3.4000 0 2 1 4 26.61 5.32 3.3500 4 0 0 2 27.07 2.58 3.2944 1 2 1 4 27.38 1.06 3.2577 2 2 0 4 27.96 8.57 3.1906 -2 1 2 4 29.23 3.30 3.0557 4 1 0 4 29.44 13.67 3.0337 -2 2 1 4 29.48 10.77 3.0302 2 2 1 4 31.16 7.21 2.8701 -4 1 1 4 31.25 46.04 2.8621 3 2 0 4 31.76 48.36 2.8177 -3 1 2 4 31.85 42.48 2.8093 3 1 2 4 32.30 12.27 2.7717 0 2 2 4 32.99 8.69 2.7155 -1 2 2 4 33.02 1.13 2.7130 1 2 2 4 33.09 34.18 2.7072 -3 2 1 4 33.13 4.91 2.7042 1 0 3 2 33.14 30.84 2.7035 3 2 1 4 34.36 5.20 2.6098 -4 0 2 2 34.48 1.27 2.6009 4 0 2 2 34.62 10.72 2.5908 0 1 3 4 35.16 7.33 2.5526 -5 0 1 2 35.23 1.08 2.5474 5 0 1 2 35.26 5.41 2.5453 -1 1 3 4 35.60 7.36 2.5220 5 1 0 4 36.48 1.88 2.4632 -4 1 2 4 36.59 5.02 2.4558 4 1 2 4 36.78 9.28 2.4437 1 3 0 4 37.17 4.09 2.4191 -2 1 3 4 37.23 1.93 2.4150 -5 1 1 4 37.25 3.69 2.4138 2 1 3 4 37.30 5.85 2.4106 5 1 1 4 37.67 1.51 2.3880 -4 2 1 4 37.72 5.05 2.3846 4 2 1 4 37.79 47.79 2.3806 0 3 1 4 38.17 5.41 2.3576 -3 2 2 4 38.24 32.02 2.3534 -3 0 3 2 38.26 8.66 2.3526 3 2 2 4 38.37 33.81 2.3461 3 0 3 2 40.18 4.13 2.2443 -3 1 3 4 40.21 7.96 2.2425 2 3 1 4 40.30 5.28 2.2379 3 1 3 4 40.39 48.51 2.2333 6 0 0 2 40.64 17.58 2.2198 0 2 3 4 41.87 2.60 2.1576 -5 1 2 4 42.41 16.06 2.1315 0 3 2 4 42.88 1.30 2.1089 -2 2 3 4 42.98 9.05 2.1044 1 3 2 4 43.04 6.45 2.1017 -3 3 1 4 43.07 7.96 2.1000 3 3 1 4 43.66 2.28 2.0732 -6 1 1 4 43.68 8.32 2.0722 0 0 4 2 43.73 4.11 2.0698 6 1 1 4 44.12 2.39 2.0527 -4 1 3 4 44.59 1.89 2.0322 -2 3 2 4 45.43 5.44 1.9966 0 1 4 4 45.58 8.07 1.9901 -3 2 3 4 45.69 7.31 1.9856 3 2 3 4 45.79 5.36 1.9817 -2 0 4 2 45.88 3.00 1.9778 2 0 4 2 45.93 1.56 1.9757 -1 1 4 4 46.10 1.22 1.9689 -6 0 2 2 46.24 2.34 1.9632 6 0 2 2 46.79 4.64 1.9415 -4 3 1 4 47.12 2.05 1.9289 -5 2 2 4 47.16 2.33 1.9271 -5 0 3 2 47.22 6.71 1.9250 -3 3 2 4 47.23 3.75 1.9244 5 2 2 4 47.29 6.51 1.9223 3 3 2 4 47.46 2.14 1.9158 6 2 0 4 47.57 3.08 1.9117 2 1 4 4 47.78 1.06 1.9037 -6 1 2 4 48.75 1.99 1.8679 -6 2 1 4 48.79 1.07 1.8666 -7 0 1 2 48.81 2.04 1.8658 -5 1 3 4 48.87 2.67 1.8638 7 0 1 2 48.98 5.30 1.8597 5 1 3 4 49.17 1.13 1.8528 -4 2 3 4 49.31 2.08 1.8480 4 2 3 4 49.32 1.24 1.8478 0 3 3 4 49.80 1.08 1.8310 -1 3 3 4 50.05 3.39 1.8223 5 3 0 4 50.38 1.30 1.8112 0 2 4 4 50.40 2.84 1.8107 -7 1 1 4 50.65 1.56 1.8022 -1 4 1 4 50.66 4.06 1.8019 1 4 1 4 50.81 1.53 1.7969 4 3 2 4 50.85 1.11 1.7958 2 4 0 4 50.85 1.45 1.7956 -1 2 4 4 50.89 2.76 1.7942 1 2 4 4 51.26 3.85 1.7823 -2 3 3 4 51.32 4.92 1.7802 2 3 3 4 51.79 2.34 1.7651 -4 0 4 2 51.97 3.96 1.7596 4 0 4 2 52.28 1.19 1.7498 -2 2 4 4 52.57 1.32 1.7410 -6 2 2 4 52.69 3.29 1.7370 6 2 2 4 53.34 2.17 1.7176 -4 1 4 4 53.51 1.22 1.7125 4 1 4 4 53.84 2.24 1.7029 7 2 0 4 53.94 3.96 1.7000 0 4 2 4 54.13 1.88 1.6943 -6 1 3 4 54.27 2.28 1.6904 7 1 2 4 54.32 2.46 1.6889 6 1 3 4 54.46 1.54 1.6848 -3 4 1 4 54.49 1.62 1.6839 3 4 1 4 55.00 4.97 1.6696 -5 3 2 4 55.81 3.86 1.6472 2 4 2 4 55.86 1.38 1.6459 -1 0 5 2 56.29 4.41 1.6343 8 1 0 4 56.47 12.04 1.6296 -6 3 1 4 56.50 1.30 1.6288 4 4 0 4 56.53 11.16 1.6280 6 3 1 4 56.85 2.71 1.6196 -4 3 3 4 56.90 4.37 1.6183 0 1 5 4 56.97 2.22 1.6164 4 3 3 4 57.38 1.13 1.6059 1 1 5 4 58.08 1.34 1.5880 3 4 2 4 58.37 1.37 1.5810 -1 3 4 4 58.54 1.29 1.5768 -7 2 2 4 58.55 5.11 1.5766 -6 2 3 4 58.64 1.63 1.5743 -2 1 5 4 58.73 4.80 1.5722 6 2 3 4 59.40 2.94 1.5560 -3 0 5 2 59.55 3.33 1.5524 3 0 5 2 59.94 4.92 1.5433 -6 3 2 4 60.06 3.93 1.5405 6 3 2 4 60.28 1.28 1.5354 -1 4 3 4 60.88 3.27 1.5217 -6 0 4 2 61.09 2.47 1.5168 -4 4 2 4 61.11 1.65 1.5166 7 3 0 4 61.11 1.59 1.5164 6 0 4 2 61.19 3.84 1.5148 0 2 5 4 61.61 3.01 1.5054 -5 4 1 4 61.66 2.82 1.5043 5 4 1 4 61.70 1.88 1.5034 -8 2 1 4 61.73 1.84 1.5028 -5 2 4 4 61.78 2.22 1.5017 8 2 1 4 61.83 10.79 1.5005 -3 3 4 4 61.92 1.84 1.4985 5 2 4 4 61.95 10.77 1.4980 3 3 4 4 62.27 1.96 1.4910 -6 1 4 4 62.50 1.85 1.4860 6 1 4 4 62.95 1.23 1.4765 2 2 5 4 63.44 1.06 1.4663 -9 0 1 2 63.69 1.52 1.4612 -3 4 3 4 63.77 1.07 1.4594 3 4 3 4 65.61 1.59 1.4229 7 3 2 4 66.66 4.40 1.4031 0 5 2 4 67.12 6.41 1.3946 -3 5 1 4 67.15 7.65 1.3940 3 5 1 4 67.77 3.35 1.3827 9 2 0 4 67.84 1.42 1.3815 0 0 6 2 67.97 1.75 1.3791 0 3 5 4 68.00 3.58 1.3786 -9 1 2 4 68.17 2.38 1.3756 9 1 2 4 68.53 1.31 1.3692 8 3 1 4 68.80 2.52 1.3646 -9 2 1 4 68.88 1.76 1.3631 9 2 1 4 69.16 1.30 1.3584 0 1 6 4 69.19 1.32 1.3577 -2 4 4 4 69.43 1.40 1.3536 -6 4 2 4 69.54 1.59 1.3518 6 4 2 4 69.55 1.99 1.3516 -2 3 5 4 70.35 1.02 1.3382 3 5 2 4 71.54 1.59 1.3188 -3 3 5 4 71.68 1.48 1.3167 3 3 5 4 71.93 2.89 1.3126 -9 0 3 2 71.94 1.73 1.3125 -6 1 5 4 72.08 1.46 1.3103 9 2 2 4 72.18 3.38 1.3088 9 0 3 2 72.21 1.58 1.3083 6 1 5 4 72.37 1.08 1.3058 1 5 3 4 72.43 1.06 1.3049 -8 0 4 2 73.04 2.39 1.2954 0 2 6 4 74.48 1.46 1.2740 4 3 5 4 75.32 1.18 1.2618 9 3 1 4 75.76 1.23 1.2555 -6 2 5 4 76.03 2.20 1.2518 6 2 5 4 76.50 1.49 1.2452 -3 2 6 4 76.66 1.38 1.2431 3 2 6 4 76.70 1.10 1.2424 -8 3 3 4 76.91 1.27 1.2396 8 3 3 4 77.02 1.07 1.2381 -9 2 3 4 77.34 1.06 1.2338 -1 4 5 4 77.70 1.35 1.2289 0 6 1 4 78.10 1.10 1.2237 1 6 1 4 78.26 1.21 1.2216 -9 3 2 4 78.42 1.04 1.2196 9 3 2 4 79.13 3.58 1.2104 0 5 4 4 79.24 1.19 1.2089 -2 6 1 4 79.71 1.25 1.2029 -1 3 6 4 80.17 1.44 1.1972 3 6 0 4 80.57 1.34 1.1923 8 4 2 4 80.86 2.64 1.1887 -6 5 2 4 80.96 1.71 1.1875 6 5 2 4 81.59 1.06 1.1799 -1 0 7 2 82.01 1.15 1.1750 -6 3 5 4 82.28 1.76 1.1718 2 6 2 4 82.48 1.23 1.1695 0 1 7 4 83.87 1.00 1.1536 4 6 1 4 85.72 1.61 1.1333 0 6 3 4 85.82 1.23 1.1323 -3 1 7 4 86.00 1.15 1.1304 3 1 7 4 86.67 1.05 1.1233 5 4 5 4 86.79 1.08 1.1221 -6 2 6 4 87.10 1.11 1.1190 6 2 6 4 87.26 1.04 1.1173 -5 6 1 4 87.32 2.54 1.1167 12 0 0 2 87.99 1.62 1.1099 0 4 6 4 88.88 1.47 1.1010 11 1 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.