Twinnite
Makovicky E, Topa D
Zeitschrift fur Kristallographie 227 (2012) 468-475
Twinnite, Pb0.8Tl0.1Sb1.3As0.8S4, the OD character and the question of its polytypism
Locality: Jas Roux, France
_database_code_amcsd 0019818
CELL PARAMETERS: 7.9970 19.5170 8.6340 90.000 91.061 90.000
SPACE GROUP: P2_1/n
X-RAY WAVELENGTH: 1.541838
Cell Volume: 1347.342
Density (g/cm3): 5.347
MAX. ABS. INTENSITY / VOLUME**2: 38.87498015
RIR: 2.367
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
9.06 24.47 9.7585 0 2 0 2
11.96 2.82 7.3988 1 1 0 4
13.70 2.00 6.4657 0 2 1 4
14.32 7.35 6.1847 1 2 0 4
14.96 2.97 5.9209 -1 0 1 2
15.91 4.24 5.5708 1 1 1 4
17.07 2.77 5.1955 0 3 1 4
17.76 1.21 4.9938 1 2 1 4
18.18 5.25 4.8793 0 4 0 2
20.28 3.19 4.3789 -1 3 1 4
20.58 3.42 4.3163 0 0 2 2
20.91 6.72 4.2477 0 4 1 4
21.08 28.54 4.2144 0 1 2 4
21.33 26.31 4.1650 1 4 0 4
22.24 18.35 3.9978 2 0 0 2
22.70 42.53 3.9165 2 1 0 4
23.69 7.06 3.7564 -1 1 2 4
24.05 3.70 3.7007 1 1 2 4
24.06 25.62 3.6994 2 2 0 4
24.75 39.99 3.5967 0 3 2 4
24.99 49.18 3.5636 -1 2 2 4
25.04 1.56 3.5567 0 5 1 4
25.14 1.52 3.5425 2 1 1 4
25.33 44.08 3.5160 1 2 2 4
25.39 100.00 3.5077 1 5 0 4
26.16 19.41 3.4061 2 3 0 4
26.37 1.12 3.3794 2 2 1 4
27.03 9.87 3.2992 -1 3 2 4
27.35 22.07 3.2613 1 3 2 4
27.37 2.50 3.2589 -1 5 1 4
27.42 3.07 3.2528 0 6 0 2
27.53 1.52 3.2405 1 5 1 4
28.87 24.71 3.0924 2 4 0 4
29.34 3.67 3.0439 0 6 1 4
29.65 13.24 3.0130 1 6 0 4
29.66 35.14 3.0117 -1 4 2 4
29.96 21.84 2.9828 1 4 2 4
30.19 9.16 2.9605 -2 0 2 2
30.54 1.97 2.9270 -2 1 2 4
30.76 8.72 2.9063 2 0 2 2
30.89 4.10 2.8951 0 5 2 4
31.11 2.71 2.8746 2 1 2 4
31.38 6.95 2.8509 -1 6 1 4
31.52 1.09 2.8386 1 6 1 4
31.58 47.87 2.8330 -2 2 2 4
32.05 7.14 2.7929 2 5 0 4
32.14 75.30 2.7854 2 2 2 4
32.77 1.83 2.7330 -1 5 2 4
32.88 4.25 2.7236 -1 0 3 2
33.04 1.68 2.7114 1 5 2 4
33.21 4.14 2.6975 -1 1 3 4
33.25 45.46 2.6946 -2 3 2 4
33.29 1.08 2.6917 1 0 3 2
33.78 26.67 2.6536 2 3 2 4
33.95 6.52 2.6407 3 1 0 4
34.05 23.68 2.6327 1 7 0 4
34.18 4.94 2.6234 -1 2 3 4
34.90 7.13 2.5710 3 2 0 4
35.58 3.49 2.5231 2 6 0 4
35.59 3.91 2.5225 -1 7 1 4
35.72 4.27 2.5139 1 7 1 4
35.74 1.40 2.5123 -1 3 3 4
36.24 4.14 2.4787 -1 6 2 4
36.43 1.57 2.4663 3 3 0 4
36.49 4.00 2.4626 1 6 2 4
38.12 2.77 2.3607 3 3 1 4
38.44 43.80 2.3420 0 7 2 4
38.49 16.84 2.3390 3 4 0 4
38.58 9.25 2.3334 1 8 0 4
39.40 1.83 2.2869 2 7 0 4
39.68 3.70 2.2712 -3 1 2 4
39.76 3.23 2.2669 -3 4 1 4
40.01 6.66 2.2537 -1 7 2 4
40.10 1.04 2.2484 3 4 1 4
40.23 12.69 2.2415 1 7 2 4
40.37 1.99 2.2344 3 1 2 4
40.52 4.80 2.2264 -3 2 2 4
41.19 2.21 2.1917 3 2 2 4
41.86 34.34 2.1581 0 0 4 2
41.87 4.21 2.1573 -3 3 2 4
42.13 4.11 2.1451 0 1 4 4
42.53 5.96 2.1257 3 3 2 4
42.54 1.58 2.1251 3 5 1 4
42.57 1.04 2.1238 0 8 2 4
42.92 1.44 2.1072 0 2 4 4
43.92 14.14 2.0616 3 6 0 4
44.01 9.47 2.0573 -1 8 2 4
44.22 2.94 2.0480 1 8 2 4
44.60 1.73 2.0318 1 9 1 4
44.64 2.30 2.0297 -2 7 2 4
44.66 4.49 2.0289 -2 8 1 4
44.67 1.77 2.0286 1 2 4 4
45.06 1.92 2.0120 2 7 2 4
45.52 1.04 1.9927 -1 3 4 4
45.55 1.25 1.9913 2 5 3 4
45.62 7.46 1.9885 4 1 0 4
46.00 8.74 1.9731 -3 5 2 4
46.37 2.82 1.9582 4 2 0 4
46.53 6.14 1.9517 0 10 0 2
46.60 7.60 1.9488 3 5 2 4
46.89 2.49 1.9377 0 9 2 4
46.97 1.86 1.9345 -3 2 3 4
47.17 4.87 1.9266 3 7 0 4
47.25 1.65 1.9238 -1 4 4 4
47.51 3.32 1.9140 -2 0 4 2
47.59 1.70 1.9107 4 3 0 4
47.65 4.73 1.9087 1 4 4 4
47.71 7.92 1.9062 2 9 0 4
47.75 2.07 1.9048 -2 1 4 4
48.18 3.63 1.8886 -3 3 3 4
48.29 1.02 1.8846 2 0 4 2
48.34 4.28 1.8827 -2 8 2 4
48.47 4.72 1.8782 -2 2 4 4
48.53 4.34 1.8758 2 1 4 4
48.67 2.47 1.8707 -3 6 2 4
48.73 5.01 1.8686 2 8 2 4
48.84 1.55 1.8648 -2 9 1 4
49.06 1.15 1.8569 3 3 3 4
49.25 7.90 1.8500 3 6 2 4
49.26 5.92 1.8497 4 4 0 4
49.40 13.73 1.8448 -1 5 4 4
49.79 9.03 1.8315 1 5 4 4
49.84 4.07 1.8296 -3 4 3 4
49.92 5.65 1.8268 -4 0 2 2
50.16 2.61 1.8188 -4 1 2 4
50.41 2.88 1.8101 2 3 4 4
50.68 5.27 1.8012 4 0 2 2
50.91 7.23 1.7935 4 1 2 4
51.27 1.73 1.7818 -2 4 4 4
51.35 2.76 1.7792 4 5 0 4
51.70 4.94 1.7681 -3 7 2 4
52.02 3.77 1.7580 2 4 4 4
52.15 4.57 1.7539 2 10 0 4
52.26 3.66 1.7506 3 7 2 4
52.29 5.50 1.7494 -2 9 2 4
52.32 3.39 1.7487 1 6 4 4
52.64 2.42 1.7387 -1 10 2 4
52.66 1.73 1.7380 2 9 2 4
52.67 1.51 1.7379 0 11 1 4
52.73 1.08 1.7359 4 3 2 4
52.82 5.86 1.7331 1 10 2 4
52.86 2.72 1.7321 1 11 0 4
53.57 1.96 1.7108 -4 4 2 4
53.83 1.87 1.7030 4 6 0 4
54.03 1.19 1.6971 2 5 4 4
54.29 2.96 1.6897 4 4 2 4
54.33 1.25 1.6887 1 9 3 4
54.41 1.12 1.6863 -3 1 4 4
54.56 3.16 1.6821 3 9 0 4
54.59 2.34 1.6812 1 0 5 2
54.65 3.19 1.6794 2 8 3 4
54.81 1.17 1.6750 1 1 5 4
54.84 5.22 1.6740 -1 7 4 4
55.07 1.46 1.6677 -3 2 4 4
55.20 1.39 1.6641 1 7 4 4
55.46 1.11 1.6568 1 2 5 4
55.48 3.15 1.6562 3 1 4 4
55.54 1.03 1.6546 -4 5 2 4
56.04 1.79 1.6410 0 11 2 4
56.13 1.32 1.6386 3 2 4 4
56.43 1.53 1.6307 2 6 4 4
56.59 2.48 1.6264 0 12 0 2
56.66 2.24 1.6245 4 7 0 4
56.77 1.07 1.6217 2 11 0 4
56.82 2.32 1.6203 2 10 2 4
57.02 1.84 1.6152 0 10 3 4
57.64 1.93 1.5991 -3 4 4 4
57.68 1.17 1.5983 0 12 1 4
57.89 1.32 1.5928 -4 6 2 4
58.40 2.71 1.5801 1 8 4 4
58.51 2.06 1.5776 -5 0 1 2
58.68 3.26 1.5734 3 4 4 4
59.34 1.49 1.5574 -5 2 1 4
59.48 1.04 1.5540 -1 5 5 4
59.53 1.19 1.5529 -3 5 4 4
59.53 6.18 1.5529 5 3 0 4
59.81 1.18 1.5462 4 8 0 4
60.97 1.29 1.5196 5 4 0 4
61.39 1.44 1.5103 0 11 3 4
61.56 1.13 1.5065 2 12 0 4
61.74 1.87 1.5025 -1 6 5 4
61.79 3.96 1.5015 -3 6 4 4
62.00 1.08 1.4969 -1 12 2 4
62.16 1.81 1.4933 1 12 2 4
62.78 1.91 1.4802 3 6 4 4
62.97 2.96 1.4760 -4 1 4 4
64.36 3.52 1.4476 0 10 4 4
64.39 1.70 1.4469 -3 7 4 4
64.67 1.82 1.4413 -5 4 2 4
65.48 2.09 1.4255 5 4 2 4
65.48 1.11 1.4255 -2 12 2 4
65.63 2.77 1.4225 2 9 4 4
65.80 1.12 1.4193 2 12 2 4
66.44 1.27 1.4072 -5 5 2 4
66.51 2.07 1.4058 -1 2 6 4
66.57 1.29 1.4048 0 3 6 4
66.82 1.40 1.4000 -3 4 5 4
66.99 1.63 1.3969 1 2 6 4
67.11 1.30 1.3947 1 13 2 4
67.22 3.20 1.3927 4 4 4 4
67.60 1.22 1.3858 2 13 1 4
67.96 1.87 1.3794 1 3 6 4
68.28 1.14 1.3737 3 8 4 4
68.30 1.14 1.3734 1 14 0 4
68.57 1.18 1.3686 -5 6 2 4
68.69 2.08 1.3665 -2 10 4 4
68.83 1.65 1.3640 -1 4 6 4
69.35 2.82 1.3551 5 6 2 4
70.62 1.38 1.3337 -4 10 2 4
70.65 2.82 1.3332 2 2 6 4
70.67 1.99 1.3329 -2 3 6 4
71.04 2.52 1.3269 4 11 0 4
71.24 1.04 1.3236 4 10 2 4
71.45 2.12 1.3204 6 2 0 4
71.52 1.33 1.3193 3 9 4 4
72.11 2.93 1.3099 -1 14 2 4
72.26 1.06 1.3075 1 14 2 4
72.82 1.44 1.2989 0 12 4 4
73.78 1.05 1.2842 1 15 0 4
74.16 1.13 1.2786 0 7 6 4
74.25 2.01 1.2773 -6 1 2 4
74.65 1.28 1.2714 -5 3 4 4
75.16 1.86 1.2640 6 1 2 4
75.17 1.08 1.2640 4 11 2 4
75.62 1.33 1.2575 -5 7 3 4
75.80 1.29 1.2550 -3 13 2 4
76.16 2.49 1.2499 5 3 4 4
76.27 1.01 1.2485 4 8 4 4
77.80 1.17 1.2276 -1 8 6 4
78.09 1.05 1.2238 2 15 1 4
81.24 1.16 1.1842 -5 0 5 2
82.26 1.87 1.1720 3 6 6 4
82.48 1.54 1.1695 6 8 0 4
83.69 1.10 1.1556 4 1 6 4
83.90 1.16 1.1533 -2 9 6 4
85.42 1.05 1.1366 -4 11 4 4
87.27 1.25 1.1172 6 2 4 4
88.47 1.21 1.1051 -1 15 4 4
================================================================================
XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.