Minguzzite
Herpin P
Bulletin de la Societe Francaise de Mineralogie et de Cristallographie 81 (1958) 245-256
Structure cristalline des trioxalates complexes de potassium II. Structure du
ferrotrioxalate de potassium racemique et comparaison avec les trioxalates
complexes actifs
Locality: synthetic
Note: C3'(y) changed to 0.259, but still unable to reproduce reported bond distances
_database_code_amcsd 0012109
CELL PARAMETERS: 7.6600 19.8700 10.2700 90.000 105.100 90.000
SPACE GROUP: P2_1/c
X-RAY WAVELENGTH: 1.541838
Cell Volume: 1509.166
Density (g/cm3): 2.190
MAX. ABS. INTENSITY / VOLUME**2: 7.994017797
RIR: 1.188
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
8.90 71.26 9.9350 0 2 0 2
12.61 26.49 7.0182 0 2 1 4
12.77 100.00 6.9310 1 1 0 4
13.68 12.22 6.4708 -1 1 1 4
14.93 1.66 5.9324 1 2 0 4
17.31 9.19 5.1236 1 1 1 4
17.86 19.17 4.9675 0 4 0 2
17.89 23.96 4.9577 0 0 2 2
19.30 10.12 4.5984 -1 1 2 4
19.99 7.98 4.4413 0 4 1 4
20.02 1.40 4.4361 0 2 2 4
24.07 1.70 3.6978 2 0 0 2
24.49 17.78 3.6343 1 1 2 4
25.06 49.19 3.5527 -2 2 1 4
25.71 1.18 3.4655 2 2 0 4
25.93 8.37 3.4366 -1 5 1 4
26.04 5.02 3.4219 -2 0 2 2
26.90 2.19 3.3142 -1 1 3 4
26.92 13.25 3.3117 0 6 0 2
27.63 41.38 3.2279 1 3 2 4
28.06 2.13 3.1801 1 5 1 4
28.41 11.90 3.1411 0 6 1 4
28.46 4.23 3.1361 0 2 3 4
29.30 15.09 3.0479 2 2 1 4
29.36 14.42 3.0418 -1 5 2 4
29.58 2.41 3.0203 -2 4 1 4
29.81 5.31 2.9974 -1 3 3 4
30.13 5.82 2.9662 2 4 0 4
31.75 9.65 2.8180 -2 4 2 4
32.51 1.87 2.7538 0 6 2 4
32.54 6.73 2.7517 0 4 3 4
32.55 4.51 2.7506 -2 2 3 4
32.74 9.15 2.7351 1 1 3 4
33.10 9.13 2.7067 1 5 2 4
33.29 25.51 2.6915 2 4 1 4
33.81 9.90 2.6515 2 0 2 2
34.20 8.66 2.6220 -1 7 1 4
34.96 19.96 2.5664 -1 5 3 4
35.03 2.32 2.5618 2 2 2 4
35.45 1.37 2.5323 -3 1 1 4
35.95 2.35 2.4978 -2 6 1 4
36.16 4.44 2.4838 0 8 0 2
36.42 3.19 2.4669 2 6 0 4
36.51 9.61 2.4608 -3 1 2 4
36.74 2.06 2.4464 3 1 0 4
36.94 5.26 2.4335 -1 7 2 4
37.67 3.87 2.3877 -1 3 4 4
37.80 1.52 2.3797 -2 6 2 4
38.77 2.74 2.3224 -3 3 2 4
38.98 1.64 2.3103 3 3 0 4
39.18 6.30 2.2992 -2 2 4 4
39.77 5.76 2.2664 -3 1 3 4
40.05 1.77 2.2514 1 7 2 4
40.63 2.41 2.2207 0 8 2 4
41.65 26.10 2.1687 -1 7 3 4
41.71 5.52 2.1656 -2 6 3 4
42.14 8.99 2.1445 2 2 3 4
42.35 4.96 2.1341 -2 4 4 4
42.74 4.26 2.1155 1 9 0 4
42.99 6.16 2.1038 -3 5 2 4
43.05 3.96 2.1012 -1 9 1 4
43.52 2.44 2.0797 -2 8 1 4
43.62 2.83 2.0751 1 3 4 4
43.91 2.69 2.0618 2 8 0 4
44.34 1.67 2.0430 -1 1 5 4
45.10 4.71 2.0101 -2 8 2 4
45.34 2.07 2.0003 -1 9 2 4
45.38 1.85 1.9984 3 1 2 4
45.87 1.48 1.9785 -3 5 3 4
46.26 2.93 1.9626 2 8 1 4
46.62 2.44 1.9483 0 10 1 4
46.71 7.78 1.9447 0 2 5 4
46.75 2.18 1.9432 -3 3 4 4
47.25 1.55 1.9237 -2 6 4 4
47.29 1.45 1.9221 3 3 2 4
47.49 2.32 1.9147 1 5 4 4
47.92 4.71 1.8983 -3 7 1 4
48.76 1.36 1.8676 -3 7 2 4
49.29 4.23 1.8489 4 0 0 2
49.30 12.50 1.8483 2 0 4 2
50.19 5.43 1.8177 4 2 0 4
50.43 8.04 1.8097 -3 5 4 4
50.75 2.07 1.7991 -4 2 3 4
51.26 3.40 1.7823 -3 1 5 4
51.44 1.02 1.7764 -4 4 2 4
51.72 4.92 1.7674 3 7 1 4
51.92 3.30 1.7612 -2 10 1 4
52.13 1.77 1.7545 0 8 4 4
52.39 2.67 1.7466 -1 11 1 4
52.84 2.37 1.7328 4 4 0 4
52.85 1.15 1.7323 2 4 4 4
53.01 1.15 1.7276 -3 3 5 4
53.52 2.85 1.7121 -2 8 4 4
53.53 1.54 1.7118 4 2 1 4
53.56 1.16 1.7110 -4 0 4 2
54.06 1.67 1.6963 -2 6 5 4
54.61 3.00 1.6806 -2 0 6 2
55.20 4.15 1.6640 -1 7 5 4
55.45 1.56 1.6571 -2 2 6 4
55.56 3.43 1.6541 -4 6 1 4
55.75 4.56 1.6490 -3 9 2 4
56.09 2.46 1.6396 3 7 2 4
56.37 1.22 1.6323 -2 10 3 4
57.05 1.13 1.6143 4 6 0 4
57.56 1.81 1.6012 4 0 2 2
57.96 1.13 1.5912 -1 11 3 4
59.52 3.16 1.5530 1 9 4 4
59.54 1.50 1.5526 -4 2 5 4
59.56 1.64 1.5521 3 1 4 4
60.13 1.50 1.5388 4 6 1 4
60.78 1.17 1.5239 4 4 2 4
60.90 1.19 1.5211 1 7 5 4
61.83 2.31 1.5005 3 7 3 4
62.00 1.76 1.4968 1 13 0 4
62.07 3.05 1.4954 -3 9 4 4
63.22 2.39 1.4708 2 12 1 4
65.29 1.41 1.4291 2 6 5 4
65.32 1.09 1.4285 -5 5 2 4
65.35 1.29 1.4280 1 5 6 4
66.11 1.07 1.4135 -5 3 4 4
66.56 1.06 1.4050 0 14 1 4
66.63 1.17 1.4036 0 10 5 4
66.70 1.01 1.4023 0 2 7 4
67.29 2.61 1.3914 -1 13 3 4
68.16 1.97 1.3759 0 8 6 4
68.80 1.19 1.3645 0 14 2 4
69.52 1.55 1.3521 -1 9 6 4
70.17 1.53 1.3413 -5 7 1 4
70.91 2.32 1.3290 -5 7 3 4
73.48 2.36 1.2887 -4 2 7 4
75.21 1.69 1.2634 3 11 3 4
75.59 1.05 1.2579 -6 2 3 4
75.60 1.07 1.2577 5 5 2 4
75.61 1.21 1.2576 1 9 6 4
77.71 1.20 1.2288 5 9 0 4
78.65 1.14 1.2165 -1 5 8 4
79.68 1.04 1.2034 1 7 7 4
80.27 1.01 1.1960 4 2 5 4
83.49 1.21 1.1579 2 16 1 4
85.87 1.26 1.1317 -1 1 9 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.