Al Cl4 H4 N
Mairesse G, Barbier P, Wignacourt J, Rubbens A, Wallart F
Canadian Journal of Chemistry 56 (1978) 764-771
X-ray, Raman, infrared, and nuclear magnetic resonance studies of the
crystal structure of ammonium tetrachloroaluminate, N H4 Al Cl4
_cod_database_code 1004065
_database_code_amcsd 0012165
CELL PARAMETERS: 11.0220 7.0720 9.2570 90.000 90.000 90.000
SPACE GROUP: Pnma
X-RAY WAVELENGTH: 1.541838
Cell Volume: 721.561
Density (g/cm3): 1.682
MAX. ABS. INTENSITY / VOLUME**2: 4.515162699
RIR: 0.874
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
12.49 10.23 7.0886 1 0 1 4
15.77 92.49 5.6197 0 1 1 4
16.08 17.86 5.5110 2 0 0 2
17.72 11.60 5.0065 1 1 1 8
18.74 84.92 4.7354 2 0 1 4
19.18 7.09 4.6285 0 0 2 2
20.43 4.43 4.3470 2 1 0 4
22.60 20.34 3.9347 2 1 1 8
24.36 75.29 3.6538 1 1 2 8
25.13 41.91 3.5443 2 0 2 4
25.19 13.19 3.5360 0 2 0 2
26.09 7.31 3.4149 3 0 1 4
28.16 20.59 3.1686 2 1 2 8
28.20 100.00 3.1642 1 2 1 8
29.04 47.47 3.0751 3 1 1 8
30.03 26.63 2.9761 2 2 0 4
30.07 25.79 2.9714 1 0 3 4
31.08 63.57 2.8776 3 0 2 4
31.58 46.61 2.8333 2 2 1 8
31.64 23.52 2.8282 0 1 3 4
31.85 31.98 2.8099 0 2 2 4
32.49 3.73 2.7555 4 0 0 2
32.69 7.02 2.7394 1 1 3 8
32.90 31.62 2.7228 1 2 2 8
33.28 10.62 2.6924 2 0 3 4
33.62 8.26 2.6654 3 1 2 8
33.94 39.93 2.6410 4 0 1 4
34.95 5.08 2.5675 4 1 0 4
35.68 6.38 2.5162 2 1 3 8
36.58 2.25 2.4564 3 2 1 8
38.00 2.08 2.3677 4 0 2 4
38.08 2.77 2.3629 3 0 3 4
38.92 1.14 2.3142 0 0 4 2
39.45 3.98 2.2844 0 3 1 4
39.62 39.02 2.2749 1 2 3 8
39.80 1.78 2.2649 1 0 4 4
40.16 15.57 2.2452 4 1 2 8
40.24 16.35 2.2411 3 1 3 8
40.32 1.70 2.2369 1 3 1 8
40.41 4.81 2.2319 3 2 2 8
41.55 1.03 2.1735 4 2 0 4
42.19 2.15 2.1421 2 2 3 8
42.36 1.48 2.1337 2 0 4 4
42.73 8.56 2.1159 4 2 1 8
42.85 1.47 2.1103 2 3 1 8
43.88 17.37 2.0634 1 3 2 8
44.06 11.60 2.0553 4 0 3 4
44.13 4.54 2.0522 5 1 1 8
46.21 7.80 1.9646 3 2 3 8
46.25 2.62 1.9628 2 3 2 8
46.83 7.15 1.9400 3 3 1 8
47.68 6.72 1.9072 1 2 4 8
48.22 2.47 1.8872 3 1 4 8
48.60 5.70 1.8732 0 3 3 4
49.63 13.39 1.8370 6 0 0 2
49.72 4.81 1.8336 5 2 1 8
49.95 3.49 1.8258 1 0 5 4
50.02 1.68 1.8236 3 3 2 8
50.66 3.02 1.8019 6 0 1 4
50.98 2.32 1.7913 4 3 0 4
50.99 4.77 1.7910 0 1 5 4
51.39 9.44 1.7780 6 1 0 4
51.42 5.47 1.7769 4 2 3 8
51.53 1.63 1.7736 2 3 3 8
51.70 24.59 1.7680 0 4 0 2
52.11 3.53 1.7550 2 0 5 4
52.40 7.46 1.7461 6 1 1 8
52.78 10.41 1.7344 5 2 2 8
53.49 59.51 1.7130 3 2 4 8
53.82 4.01 1.7033 2 1 5 8
54.51 1.06 1.6835 2 4 0 4
54.97 3.94 1.6705 4 3 2 8
55.03 9.01 1.6688 3 3 3 8
55.48 6.23 1.6563 2 4 1 8
56.74 4.70 1.6223 1 2 5 8
57.22 5.46 1.6099 3 1 5 8
57.62 15.79 1.5997 5 2 3 8
57.76 1.77 1.5962 5 0 4 4
58.15 2.19 1.5863 5 3 1 8
58.32 5.46 1.5821 2 4 2 8
58.47 1.29 1.5785 6 0 3 4
58.73 1.47 1.5720 2 2 5 8
59.96 1.26 1.5428 0 0 6 2
60.06 1.33 1.5405 6 1 3 8
60.18 5.47 1.5376 6 2 2 8
60.22 9.01 1.5367 4 0 5 4
60.98 3.62 1.5194 1 4 3 8
61.56 10.66 1.5064 3 4 2 8
61.57 1.24 1.5063 3 3 4 8
61.96 1.44 1.4977 3 2 5 8
62.15 1.83 1.4935 1 1 6 8
62.28 1.91 1.4907 7 0 2 4
62.52 1.33 1.4857 2 0 6 4
62.89 2.38 1.4778 2 4 3 8
63.30 8.98 1.4692 4 4 1 8
63.81 3.54 1.4586 7 1 2 8
63.94 2.73 1.4560 0 3 5 4
64.00 3.16 1.4548 5 2 4 8
64.04 4.10 1.4540 2 1 6 8
64.29 3.86 1.4490 6 3 0 4
64.67 2.43 1.4414 6 2 3 8
65.17 2.07 1.4316 6 3 1 8
65.63 1.08 1.4225 3 0 6 4
65.69 8.68 1.4213 7 2 1 8
65.88 1.18 1.4177 5 0 5 4
66.07 3.64 1.4141 0 2 6 4
66.41 1.41 1.4077 2 3 5 8
66.68 3.18 1.4026 1 2 6 8
66.69 2.47 1.4025 7 0 3 4
66.92 2.08 1.3982 0 5 1 4
68.05 1.96 1.3778 8 0 0 2
68.50 1.10 1.3697 2 2 6 8
68.90 1.02 1.3627 8 0 1 4
69.43 3.90 1.3536 3 3 5 8
70.09 1.54 1.3426 1 5 2 8
70.22 4.38 1.3403 4 4 3 8
71.32 1.53 1.3224 4 1 6 8
71.44 2.03 1.3205 8 0 2 4
71.73 1.04 1.3159 5 2 5 8
71.87 1.30 1.3137 2 5 2 8
71.91 1.15 1.3130 1 0 7 4
72.31 2.42 1.3067 3 5 1 8
72.50 4.29 1.3037 7 2 3 8
73.67 3.30 1.2859 2 0 7 4
73.68 1.03 1.2858 0 5 3 4
73.92 1.27 1.2822 1 3 6 8
74.48 6.40 1.2739 6 4 0 4
74.64 1.23 1.2716 8 2 1 8
74.74 1.47 1.2701 1 4 5 8
75.31 1.57 1.2620 6 4 1 8
75.45 2.88 1.2599 7 3 2 8
75.58 1.25 1.2581 4 2 6 8
75.66 1.52 1.2569 2 3 6 8
76.48 1.85 1.2455 2 4 5 8
77.56 1.05 1.2309 1 2 7 8
78.12 2.17 1.2235 6 2 5 8
78.82 2.20 1.2142 4 5 2 8
78.84 1.30 1.2141 9 0 1 4
80.57 2.50 1.1922 4 0 7 4
80.74 1.81 1.1902 5 2 6 8
81.19 1.01 1.1848 5 4 4 8
83.06 2.63 1.1627 1 6 1 8
83.31 5.95 1.1598 4 4 5 8
83.55 3.41 1.1571 0 0 8 2
84.76 1.22 1.1438 2 6 1 8
84.90 1.02 1.1422 0 6 2 4
85.13 1.33 1.1397 7 4 2 8
85.46 1.11 1.1361 1 6 2 8
85.48 2.52 1.1359 7 2 5 8
86.74 1.78 1.1227 9 2 2 8
86.93 1.72 1.1207 6 5 0 4
86.94 3.87 1.1205 6 2 6 8
87.72 1.96 1.1126 6 5 1 8
89.11 1.96 1.0988 7 4 3 8
89.44 2.54 1.0956 1 6 3 8
89.56 1.13 1.0945 10 0 1 4
89.58 1.56 1.0943 1 2 8 8
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.