Kryzhanovskite
Moore P B, Araki T
Inorganic Chemistry 15 (1976) 316-321
A mixed-valence solid-solution series: Crystal structures of phosphoferrite,
Fe3(H2O)3[PO4]2, and kryzhanovskite, Fe3(OH)3[PO4]2
Note: this sample was synthesized by heating phosphoferrite in air
Locality: synthetic
_database_code_amcsd 0012681
CELL PARAMETERS: 9.5180 9.7490 8.0310 90.000 90.000 90.000
SPACE GROUP: Pbna
X-RAY WAVELENGTH: 1.541838
Cell Volume: 745.204
Density (g/cm3): 3.641
MAX. ABS. INTENSITY / VOLUME**2: 21.58983193
RIR: 1.931
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
14.43 4.41 6.1380 1 0 1 4
17.07 15.53 5.1942 1 1 1 8
18.20 31.96 4.8745 0 2 0 2
18.65 29.35 4.7590 2 0 0 2
20.77 21.52 4.2767 2 1 0 4
22.14 2.21 4.0155 0 0 2 2
23.30 18.99 3.8172 1 2 1 8
26.17 8.74 3.4052 2 2 0 4
28.47 100.00 3.1350 2 2 1 8
28.81 3.42 3.0993 0 2 2 4
29.10 26.75 3.0690 2 0 2 4
30.33 26.92 2.9470 1 2 2 8
30.54 2.20 2.9274 2 1 2 8
31.68 1.33 2.8242 3 1 1 8
33.39 13.65 2.6837 2 3 0 4
34.54 6.03 2.5971 2 2 2 8
34.81 11.42 2.5770 1 0 3 4
35.56 3.72 2.5243 3 2 1 8
36.05 15.88 2.4914 1 1 3 8
36.81 4.65 2.4416 1 3 2 8
36.88 2.03 2.4372 0 4 0 2
37.28 8.05 2.4120 3 1 2 8
37.81 3.76 2.3795 4 0 0 2
38.36 7.22 2.3464 0 2 3 4
38.60 6.29 2.3322 0 4 1 4
39.56 9.85 2.2782 1 2 3 8
39.72 1.28 2.2691 2 1 3 8
39.79 9.71 2.2652 1 4 1 8
40.61 11.58 2.2214 4 1 1 8
40.70 1.60 2.2170 3 2 2 8
41.33 8.97 2.1845 3 3 1 8
43.20 2.33 2.0943 2 4 1 8
43.43 9.84 2.0835 0 4 2 4
43.81 2.97 2.0663 4 2 1 8
44.27 3.32 2.0460 3 0 3 4
44.52 3.56 2.0353 1 4 2 8
45.16 1.49 2.0078 0 0 4 2
45.29 1.81 2.0024 3 1 3 8
45.92 9.16 1.9762 3 3 2 8
47.20 1.29 1.9258 1 1 4 8
47.35 2.28 1.9199 4 3 0 4
47.65 3.91 1.9086 2 4 2 8
48.00 3.12 1.8953 2 3 3 8
48.22 3.36 1.8874 4 2 2 8
48.24 12.10 1.8865 3 2 3 8
48.44 9.67 1.8791 3 4 1 8
48.77 2.80 1.8672 4 3 1 8
49.19 1.69 1.8523 5 0 1 4
49.26 1.35 1.8499 2 0 4 4
50.13 2.82 1.8197 5 1 1 8
50.20 2.45 1.8174 2 1 4 8
52.88 4.61 1.7315 5 2 1 8
52.88 2.18 1.7314 3 3 3 8
54.14 5.20 1.6939 5 1 2 8
54.93 1.86 1.6715 3 1 4 8
54.96 2.46 1.6707 4 2 3 8
57.25 3.75 1.6092 5 3 1 8
57.31 1.61 1.6076 2 3 4 8
57.90 1.18 1.5926 0 6 1 4
58.25 1.99 1.5838 1 0 5 4
58.79 4.45 1.5707 1 6 1 8
58.92 3.56 1.5675 4 4 2 8
58.99 2.37 1.5657 6 1 0 4
59.59 2.70 1.5514 5 0 3 4
59.67 5.03 1.5497 0 4 4 4
60.18 2.12 1.5377 2 6 0 4
60.29 5.79 1.5350 3 5 2 8
60.42 4.68 1.5321 5 1 3 8
60.71 4.84 1.5255 0 2 5 4
60.94 1.37 1.5203 5 3 2 8
61.14 1.75 1.5158 4 1 4 8
61.39 5.29 1.5102 2 6 1 8
61.57 3.87 1.5063 1 2 5 8
61.57 1.72 1.5062 0 6 2 4
61.69 1.11 1.5036 2 1 5 8
62.03 1.06 1.4962 2 5 3 8
62.42 2.97 1.4877 1 6 2 8
62.68 7.70 1.4822 4 5 1 8
63.03 1.51 1.4747 5 4 1 8
63.09 13.74 1.4735 2 4 4 8
63.57 2.08 1.4637 4 2 4 8
63.80 1.75 1.4588 6 1 2 8
64.10 2.45 1.4527 2 2 5 8
65.09 2.09 1.4330 3 0 5 4
65.47 2.40 1.4256 6 3 0 4
65.59 3.28 1.4233 3 6 1 8
65.88 1.34 1.4178 3 1 5 8
66.82 1.49 1.4000 5 3 3 8
67.42 1.33 1.3890 0 6 3 4
67.50 2.40 1.3876 4 3 4 8
69.02 1.28 1.3607 3 6 2 8
69.56 3.49 1.3515 6 1 3 8
70.20 2.74 1.3406 7 0 1 4
70.45 1.55 1.3367 2 7 0 4
71.89 2.29 1.3134 1 1 6 8
72.84 1.32 1.2986 4 4 4 8
73.50 1.35 1.2885 2 0 6 4
74.13 1.96 1.2790 1 2 6 8
74.28 2.58 1.2768 7 1 2 8
74.57 1.04 1.2727 4 6 2 8
74.87 1.18 1.2682 2 7 2 8
78.27 1.29 1.2215 5 6 1 8
78.49 1.66 1.2186 0 8 0 2
79.70 1.14 1.2030 7 1 3 8
82.73 1.01 1.1666 4 0 6 4
83.53 1.25 1.1575 1 8 2 8
87.18 1.09 1.1181 6 5 3 8
88.82 2.29 1.1017 1 8 3 8
89.38 1.15 1.0962 1 5 6 8
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.