Bariosincosite
Roca M, Marcos M D, Amoros P, Alamo J, Beltran-Porter A, Beltran-Porter D
Inorganic Chemistry 36 (1997) 3414-3421
Synthesis and crystal structure of a novel lamellar barium derivative:
Ba(VOPO4)2*4H2O. Synthetic pathways for layered oxovanadium phosphate hydrates
M(VOPO4)2*nH2O
_database_code_amcsd 0012720
CELL PARAMETERS: 6.3860 12.7796 6.3870 90.000 90.172 90.000
SPACE GROUP: Pn
X-RAY WAVELENGTH: 1.541838
Cell Volume: 521.244
Density (g/cm3): 3.452
MAX. ABS. INTENSITY / VOLUME**2: 14.10987609
RIR: 1.331
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
13.86 8.94 6.3898 0 2 0 2
15.51 79.26 5.7132 0 1 1 2
15.51 76.14 5.7125 1 1 0 2
19.63 20.86 4.5227 -1 0 1 1
19.65 5.61 4.5173 0 2 1 2
19.65 18.17 4.5169 1 2 0 2
19.69 19.70 4.5092 1 0 1 1
20.89 2.09 4.2522 1 1 1 2
24.11 23.58 3.6916 -1 2 1 2
24.16 23.71 3.6842 1 2 1 2
25.13 53.28 3.5439 0 3 1 2
25.13 39.57 3.5438 1 3 0 2
27.93 61.83 3.1949 0 4 0 2
27.94 5.85 3.1935 0 0 2 1
27.94 17.09 3.1930 2 0 0 1
28.82 52.03 3.0982 0 1 2 2
28.82 27.03 3.0978 2 1 0 2
31.30 2.56 2.8574 0 4 1 2
31.31 6.68 2.8573 1 4 0 2
31.31 40.41 2.8566 0 2 2 2
31.32 59.59 2.8562 2 2 0 2
32.07 41.03 2.7907 -1 1 2 2
32.08 10.48 2.7904 -2 1 1 2
32.15 11.11 2.7843 1 1 2 2
32.15 40.79 2.7840 2 1 1 2
34.37 9.22 2.6095 -1 4 1 2
34.40 8.84 2.6069 1 4 1 2
35.12 8.20 2.5552 0 3 2 2
35.12 5.93 2.5549 2 3 0 2
37.89 45.11 2.3743 -1 3 2 2
37.90 6.56 2.3741 -2 3 1 2
37.92 10.26 2.3730 0 5 1 2
37.92 5.40 2.3729 1 5 0 2
37.96 6.56 2.3704 1 3 2 2
37.96 43.76 2.3702 2 3 1 2
39.86 2.55 2.2614 -2 0 2 1
39.91 4.25 2.2586 0 4 2 2
39.92 5.41 2.2585 2 4 0 2
39.99 5.59 2.2546 2 0 2 1
40.51 6.11 2.2268 -2 1 2 2
42.40 9.65 2.1318 -2 2 2 2
42.44 22.11 2.1299 0 6 0 2
42.52 13.73 2.1261 2 2 2 2
43.07 5.17 2.1000 0 1 3 2
43.08 7.14 2.0997 3 1 0 2
44.84 1.93 2.0215 -1 0 3 1
44.84 21.80 2.0213 -3 0 1 1
44.86 1.85 2.0205 0 6 1 2
44.86 7.54 2.0205 1 6 0 2
44.88 6.81 2.0198 0 2 3 2
44.88 1.97 2.0195 3 2 0 2
44.92 21.41 2.0179 1 0 3 1
44.93 1.37 2.0176 3 0 1 1
45.41 3.55 1.9974 -2 3 2 2
45.45 1.38 1.9955 0 5 2 2
45.51 1.51 1.9930 3 1 1 2
47.15 9.43 1.9274 -1 2 3 2
47.16 6.92 1.9272 -3 2 1 2
47.17 4.36 1.9269 -1 6 1 2
47.19 3.36 1.9259 1 6 1 2
47.24 7.01 1.9242 1 2 3 2
47.24 8.34 1.9240 3 2 1 2
47.72 16.41 1.9057 -1 5 2 2
47.73 2.90 1.9056 -2 5 1 2
47.76 4.28 1.9044 0 3 3 2
47.76 8.64 1.9042 3 3 0 2
47.78 3.49 1.9037 1 5 2 2
47.78 17.33 1.9036 2 5 1 2
49.37 2.86 1.8458 -2 4 2 2
49.48 6.34 1.8421 2 4 2 2
51.58 3.70 1.7720 0 6 2 2
51.58 4.23 1.7719 2 6 0 2
51.59 5.74 1.7717 0 4 3 2
51.59 1.64 1.7715 3 4 0 2
52.05 2.14 1.7570 -2 1 3 2
52.06 4.03 1.7569 -3 1 2 2
52.10 7.30 1.7554 0 7 1 2
52.10 5.04 1.7553 1 7 0 2
52.20 3.75 1.7522 2 1 3 2
52.21 1.95 1.7521 3 1 2 2
53.65 4.90 1.7083 -1 4 3 2
53.66 5.69 1.7081 -3 4 1 2
53.66 2.64 1.7081 -2 6 1 2
53.73 6.20 1.7061 1 4 3 2
53.73 4.41 1.7059 3 4 1 2
54.15 3.67 1.6936 -2 5 2 2
54.20 2.75 1.6922 1 7 1 2
56.17 1.90 1.6375 -2 3 3 2
56.17 4.90 1.6374 -3 3 2 2
56.23 2.21 1.6358 0 5 3 2
56.24 6.03 1.6357 3 5 0 2
56.32 4.11 1.6336 2 3 3 2
56.32 1.76 1.6336 3 3 2 2
57.74 1.98 1.5967 0 0 4 1
58.23 6.36 1.5844 0 1 4 2
58.24 8.65 1.5842 4 1 0 2
59.63 2.62 1.5505 -2 6 2 2
59.69 2.84 1.5491 0 2 4 2
59.70 1.91 1.5489 4 2 0 2
59.72 4.06 1.5483 2 6 2 2
60.13 1.92 1.5389 -1 1 4 2
60.13 1.43 1.5388 -1 7 2 2
60.13 2.17 1.5388 -2 7 1 2
60.14 2.20 1.5387 -4 1 1 2
60.18 2.98 1.5377 1 7 2 2
60.18 1.10 1.5377 2 7 1 2
60.22 2.36 1.5367 1 1 4 2
60.23 2.10 1.5365 4 1 1 2
61.57 3.15 1.5063 -1 8 1 2
61.59 3.47 1.5058 0 6 3 2
61.59 2.16 1.5058 1 8 1 2
61.98 2.12 1.4972 -3 1 3 2
62.08 1.65 1.4952 0 3 4 2
62.09 2.00 1.4950 4 3 0 2
62.19 1.88 1.4928 3 1 3 2
63.39 1.78 1.4673 -3 2 3 2
63.44 1.34 1.4663 -1 6 3 2
63.45 13.07 1.4662 -3 6 1 2
63.51 12.58 1.4649 1 6 3 2
63.59 2.08 1.4631 3 2 3 2
63.88 1.75 1.4573 -2 5 3 2
63.88 1.38 1.4572 -3 5 2 2
63.91 1.89 1.4567 -1 3 4 2
63.91 2.31 1.4565 -4 3 1 2
64.00 2.63 1.4549 1 3 4 2
64.00 2.22 1.4547 4 3 1 2
64.01 1.18 1.4545 2 5 3 2
64.02 1.03 1.4545 3 5 2 2
65.25 7.00 1.4298 -2 0 4 1
65.26 1.80 1.4297 -4 0 2 1
65.31 1.77 1.4287 0 8 2 2
65.32 2.23 1.4286 2 8 0 2
65.33 1.11 1.4283 0 4 4 2
65.44 6.99 1.4263 4 0 2 1
65.89 1.84 1.4176 2 1 4 2
67.08 1.34 1.3952 -4 2 2 2
67.58 1.22 1.3861 0 9 1 2
67.58 1.01 1.3861 1 9 0 2
67.60 1.22 1.3859 0 7 3 2
67.60 1.81 1.3858 3 7 0 2
68.87 1.30 1.3634 -3 4 3 2
69.02 1.01 1.3608 2 6 3 2
69.02 1.25 1.3608 3 6 2 2
69.06 1.45 1.3601 3 4 3 2
69.43 1.70 1.3537 3 7 1 2
71.22 1.26 1.3241 1 5 4 2
72.41 6.11 1.3051 -2 4 4 2
72.42 1.77 1.3050 -4 4 2 2
72.44 1.13 1.3047 -2 8 2 2
72.52 1.24 1.3034 2 8 2 2
72.58 1.06 1.3025 2 4 4 2
72.59 6.04 1.3024 4 4 2 2
74.20 1.55 1.2780 0 10 0 2
74.56 1.06 1.2728 -3 1 4 2
74.56 3.16 1.2728 -4 1 3 2
74.60 1.07 1.2722 -2 7 3 2
74.60 2.67 1.2722 -3 7 2 2
74.63 6.38 1.2718 -1 9 2 2
74.67 6.91 1.2712 2 9 1 2
74.68 3.02 1.2711 0 1 5 2
74.69 2.83 1.2709 5 1 0 2
74.72 2.45 1.2704 2 7 3 2
74.81 3.18 1.2692 3 1 4 2
74.81 1.29 1.2691 4 1 3 2
75.92 4.09 1.2534 -1 8 3 2
75.98 2.65 1.2524 3 8 1 2
77.64 1.09 1.2298 -1 10 1 2
77.65 1.13 1.2297 -5 2 1 2
77.74 1.01 1.2285 1 2 5 2
77.75 1.01 1.2283 5 2 1 2
78.11 1.20 1.2236 0 3 5 2
78.12 1.18 1.2234 5 3 0 2
78.24 1.67 1.2218 4 3 3 2
80.99 1.07 1.1872 -2 6 4 2
81.16 1.04 1.1851 4 6 2 2
81.41 1.18 1.1821 -2 1 5 2
81.45 1.40 1.1816 -1 7 4 2
81.45 1.37 1.1816 -4 7 1 2
81.53 1.86 1.1807 1 7 4 2
81.54 1.71 1.1806 4 7 1 2
81.62 1.06 1.1796 5 1 2 2
82.73 1.18 1.1666 -5 4 1 2
82.81 1.05 1.1656 1 4 5 2
83.09 1.88 1.1625 -3 7 3 2
83.27 1.54 1.1604 3 7 3 2
84.75 3.47 1.1439 -4 5 3 2
84.86 2.98 1.1426 0 5 5 2
84.87 2.99 1.1425 5 5 0 2
84.98 3.19 1.1413 3 5 4 2
84.99 1.47 1.1412 4 5 3 2
86.51 1.47 1.1250 1 11 1 2
87.64 3.30 1.1134 -4 2 4 2
87.96 2.59 1.1101 4 2 4 2
89.36 1.24 1.0964 -3 8 3 2
89.54 1.46 1.0947 3 8 3 2
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.