Pyromorphite
Miyake M, Ishigaki K, Suzuki T
Journal of Solid State Chemistry 61 (1986) 230-235
Structure refinements of Pb2+ ion-exchanged apatites by X-ray powder pattern-fitting
Note: Sample OHAp
Locality: synthetic
Note: apatite group
_database_code_amcsd 0013571
CELL PARAMETERS: 9.8800 9.8800 7.4170 90.000 90.000 120.000
SPACE GROUP: P6_3/m
X-RAY WAVELENGTH: 1.541838
Cell Volume: 627.008
Density (g/cm3): 5.921
MAX. ABS. INTENSITY / VOLUME**2: 96.76959695
RIR: 5.322
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
10.34 1.12 8.5563 1 0 0 6
17.96 2.41 4.9400 1 1 0 6
20.76 32.32 4.2782 2 0 0 6
21.61 42.83 4.1115 1 1 1 12
24.00 14.53 3.7085 0 0 2 2
26.19 40.20 3.4026 1 0 2 12
27.58 15.48 3.2340 1 2 0 6
27.58 22.06 3.2340 2 1 0 6
30.13 86.66 2.9658 1 1 2 12
30.15 40.92 2.9644 1 2 1 12
30.15 59.08 2.9644 2 1 1 12
31.36 55.39 2.8521 3 0 0 6
31.94 2.10 2.8022 2 0 2 12
36.37 1.26 2.4700 2 2 0 6
37.91 1.82 2.3731 1 3 0 6
39.87 1.56 2.2608 3 0 2 12
40.81 15.70 2.2109 1 1 3 12
42.25 6.94 2.1391 4 0 0 6
44.05 29.32 2.0558 2 2 2 12
45.37 10.79 1.9989 1 3 2 12
45.37 9.94 1.9989 3 1 2 12
46.22 14.70 1.9641 1 2 3 12
46.22 14.21 1.9641 2 1 3 12
46.25 5.37 1.9630 2 3 0 6
46.25 3.19 1.9630 3 2 0 6
47.94 11.87 1.8976 2 3 1 12
47.94 12.11 1.8976 3 2 1 12
48.77 7.92 1.8671 1 4 0 6
48.77 8.86 1.8671 4 1 0 6
49.13 12.35 1.8542 0 0 4 2
49.17 32.19 1.8529 4 0 2 12
53.89 3.44 1.7013 2 0 4 12
55.07 1.01 1.6677 4 1 2 12
56.95 3.54 1.6170 2 4 0 6
56.95 1.61 1.6170 4 2 0 6
57.27 5.15 1.6086 1 2 4 12
57.27 3.84 1.6086 2 1 4 12
57.31 5.39 1.6075 3 3 1 12
59.46 10.16 1.5546 3 0 4 12
59.49 5.42 1.5538 5 0 2 12
60.19 2.63 1.5373 2 3 3 12
60.19 7.11 1.5373 3 2 3 12
60.22 1.13 1.5368 1 5 0 6
60.22 2.21 1.5368 5 1 0 6
61.63 5.16 1.5050 3 3 2 12
61.64 3.76 1.5048 1 5 1 12
61.64 6.31 1.5048 5 1 1 12
65.72 1.46 1.4207 1 1 5 12
66.76 2.79 1.4011 4 0 4 12
68.46 2.05 1.3705 3 3 3 12
69.75 1.93 1.3483 1 2 5 12
69.75 4.17 1.3483 2 1 5 12
69.77 1.92 1.3479 2 3 4 12
69.77 1.24 1.3479 3 2 4 12
69.81 2.30 1.3473 2 5 1 12
69.81 2.54 1.3473 5 2 1 12
70.79 3.51 1.3310 6 0 2 12
71.74 3.74 1.3157 1 4 4 12
71.74 3.52 1.3157 4 1 4 12
71.77 2.56 1.3152 3 4 2 12
71.77 1.68 1.3152 4 3 2 12
72.41 2.24 1.3052 1 5 3 12
72.41 2.82 1.3052 5 1 3 12
72.43 1.01 1.3048 6 1 0 6
73.72 4.26 1.2852 2 5 2 12
73.72 3.00 1.2852 5 2 2 12
73.72 1.34 1.2851 1 6 1 12
73.72 1.19 1.2851 6 1 1 12
77.25 1.32 1.2350 4 4 0 6
78.48 1.98 1.2187 2 4 4 12
78.48 1.78 1.2187 4 2 4 12
80.01 3.66 1.1992 1 1 6 12
80.08 1.37 1.1984 2 5 3 12
80.08 1.66 1.1984 5 2 3 12
81.29 1.34 1.1835 3 2 5 12
81.29 2.13 1.1835 2 3 5 12
81.32 1.75 1.1832 5 1 4 12
83.22 1.49 1.1609 7 0 2 12
88.43 2.18 1.1055 2 2 6 12
88.77 1.13 1.1021 3 3 5 12
89.36 1.08 1.0963 1 3 6 12
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.