Macphersonite
Steele I M, Pluth J J, Livingstone A
Mineralogical Magazine 62 (1998) 451-459
Crystal structure of macphersonite (Pb4SO4(CO3)2(OH)2): comparison with leadhillite
Locality: Leadhills-Wanlockhead orefield, Scotland
Note: space group changed from Pcab to Pbca
_database_code_amcsd 0014534
CELL PARAMETERS: 9.2420 23.0500 10.3830 90.000 90.000 90.000
SPACE GROUP: Pbca
X-RAY WAVELENGTH: 1.541838
Cell Volume: 2211.871
Density (g/cm3): 6.467
MAX. ABS. INTENSITY / VOLUME**2: 131.9061265
RIR: 6.642
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
7.67 20.54 11.5250 0 2 0 2
11.47 2.15 7.7141 0 2 1 4
14.96 8.19 5.9222 1 2 1 8
15.38 4.37 5.7625 0 4 0 2
17.60 1.58 5.0385 0 4 1 4
19.21 10.14 4.6210 2 0 0 2
19.59 4.70 4.5308 2 1 0 4
19.61 23.91 4.5263 1 0 2 4
19.99 12.92 4.4415 1 1 2 8
20.07 8.28 4.4238 1 4 1 8
20.71 3.94 4.2891 2 2 0 4
21.09 6.32 4.2130 1 2 2 8
22.43 7.40 3.9642 2 2 1 8
22.45 14.53 3.9600 2 3 0 4
22.80 33.66 3.8999 1 3 2 8
23.15 1.32 3.8417 0 6 0 2
24.70 1.97 3.6050 2 4 0 4
25.02 3.84 3.5595 1 4 2 8
25.81 1.60 3.4517 2 0 2 4
26.17 13.03 3.4056 2 4 1 8
26.55 1.39 3.3569 1 6 1 8
26.90 3.38 3.3148 0 2 3 4
26.96 1.07 3.3066 2 2 2 8
27.33 53.61 3.2636 2 5 0 4
27.62 100.00 3.2298 1 5 2 8
27.80 6.20 3.2096 1 1 3 8
29.92 5.47 2.9863 1 3 3 8
30.12 3.39 2.9670 0 4 3 4
30.25 3.45 2.9541 2 6 0 4
30.52 10.50 2.9295 3 1 1 8
30.52 8.46 2.9289 1 6 2 8
31.04 14.09 2.8812 0 8 0 2
31.49 2.32 2.8414 2 6 1 8
32.24 1.53 2.7763 0 8 1 4
32.40 1.02 2.7630 2 5 2 8
32.48 5.44 2.7568 3 3 1 8
32.56 4.81 2.7504 2 1 3 8
33.66 1.20 2.6628 1 7 2 8
33.71 2.57 2.6590 1 8 1 8
33.83 36.83 2.6493 3 0 2 4
34.41 2.67 2.6060 2 3 3 8
34.55 20.79 2.5958 0 0 4 2
34.74 5.72 2.5820 3 2 2 8
35.45 2.04 2.5323 0 2 4 4
35.94 2.09 2.4991 1 0 4 4
36.76 1.91 2.4449 2 8 0 4
36.98 3.80 2.4306 1 8 2 8
37.80 2.53 2.3798 2 8 1 8
38.98 1.57 2.3105 4 0 0 2
39.08 18.80 2.3050 0 10 0 2
39.35 3.04 2.2897 3 1 3 8
39.79 1.66 2.2654 4 2 0 4
39.83 5.36 2.2631 2 0 4 4
40.17 2.25 2.2446 4 1 1 8
40.63 2.21 2.2207 2 2 4 8
40.77 2.38 2.2134 4 2 1 8
40.78 5.30 2.2126 4 3 0 4
40.94 1.39 2.2044 3 3 3 8
41.29 1.11 2.1863 1 10 1 8
41.60 9.74 2.1709 2 3 4 8
41.74 1.57 2.1640 4 3 1 8
42.29 2.20 2.1370 3 4 3 8
42.65 1.14 2.1198 2 7 3 8
42.84 1.05 2.1109 4 0 2 4
43.07 6.56 2.1002 4 4 1 8
43.83 8.19 2.0656 4 5 0 4
43.89 3.84 2.0626 2 10 0 4
44.09 8.64 2.0540 1 10 2 8
44.32 1.84 2.0437 0 2 5 4
44.60 23.17 2.0315 2 5 4 8
44.91 1.20 2.0183 1 1 5 8
45.12 4.47 2.0095 1 9 3 8
45.88 3.61 1.9777 3 1 4 8
46.35 1.68 1.9591 1 3 5 8
46.48 3.20 1.9536 0 4 5 4
46.57 8.57 1.9502 3 8 2 8
46.70 1.21 1.9449 4 6 1 8
46.96 6.74 1.9349 3 9 1 8
47.12 4.19 1.9285 0 8 4 4
47.57 2.15 1.9114 1 4 5 8
47.83 1.65 1.9016 1 11 2 8
48.11 1.19 1.8913 4 7 0 4
48.40 3.61 1.8805 2 9 3 8
48.83 1.05 1.8651 2 7 4 8
49.25 1.48 1.8500 4 6 2 8
49.57 1.09 1.8391 2 3 5 8
50.03 4.08 1.8232 3 5 4 8
50.04 4.88 1.8230 4 4 3 8
50.29 1.12 1.8141 5 1 1 8
50.74 2.09 1.7994 2 4 5 8
50.79 1.23 1.7975 5 2 1 8
51.34 2.24 1.7798 2 8 4 8
52.63 14.90 1.7390 3 10 2 8
52.75 4.72 1.7353 5 4 1 8
53.14 8.44 1.7235 0 10 4 4
53.20 1.33 1.7218 5 2 2 8
53.30 1.48 1.7186 4 6 3 8
53.35 1.07 1.7171 3 1 5 8
53.54 2.27 1.7117 3 9 3 8
53.93 1.19 1.7000 3 7 4 8
53.99 2.05 1.6983 5 3 2 8
54.19 1.65 1.6926 4 9 1 8
54.47 1.54 1.6846 0 8 5 4
54.49 2.18 1.6839 4 3 4 8
54.53 1.28 1.6827 1 2 6 8
55.32 2.51 1.6607 1 3 6 8
55.51 3.55 1.6554 2 13 0 4
55.67 8.62 1.6509 1 13 2 8
55.91 1.09 1.6446 5 6 1 8
56.49 2.21 1.6290 5 5 2 8
56.98 3.67 1.6163 4 5 4 8
57.03 2.75 1.6149 2 10 4 8
57.78 4.13 1.5958 1 5 6 8
58.05 1.04 1.5890 1 9 5 8
58.86 2.15 1.5689 5 4 3 8
60.11 1.65 1.5393 5 7 2 8
60.34 1.79 1.5339 2 14 1 8
60.57 1.21 1.5286 4 7 4 8
60.94 2.41 1.5203 6 1 1 8
61.34 1.28 1.5112 1 7 6 8
61.46 2.65 1.5088 3 0 6 4
61.60 1.11 1.5057 5 0 4 4
62.04 1.40 1.4960 3 2 6 8
63.67 1.18 1.4616 1 1 7 8
63.83 2.70 1.4582 2 15 0 4
63.98 5.43 1.4551 1 15 2 8
64.68 1.19 1.4411 3 11 4 8
66.47 1.50 1.4066 4 13 0 4
66.57 1.66 1.4046 6 1 3 8
66.72 1.51 1.4018 5 6 4 8
67.06 3.16 1.3957 2 13 4 8
67.64 1.55 1.3851 4 0 6 4
70.45 1.36 1.3366 3 8 6 8
70.86 1.37 1.3298 4 14 1 8
71.72 1.39 1.3160 6 2 4 8
72.13 2.49 1.3095 6 9 1 8
72.55 1.33 1.3030 4 6 6 8
72.62 1.00 1.3019 3 4 7 8
74.03 1.32 1.2806 0 18 0 2
74.26 1.26 1.2772 7 4 1 8
74.66 1.64 1.2714 1 9 7 8
74.66 2.13 1.2713 2 15 4 8
75.28 2.42 1.2624 3 10 6 8
76.14 1.38 1.2503 4 14 3 8
77.12 1.22 1.2367 4 13 4 8
77.37 1.68 1.2333 6 9 3 8
77.46 1.38 1.2322 1 18 2 8
77.81 1.25 1.2275 1 13 6 8
78.31 1.87 1.2209 5 14 1 8
80.54 1.34 1.1927 7 7 2 8
80.98 1.07 1.1872 4 10 6 8
83.43 1.05 1.1585 5 14 3 8
83.50 1.03 1.1577 3 5 8 8
83.93 1.93 1.1529 3 18 2 8
84.33 1.12 1.1484 0 18 4 4
84.40 1.03 1.1477 4 15 4 8
85.08 1.18 1.1403 1 15 6 8
87.35 1.22 1.1163 6 5 6 8
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.