Gladite
Synecek V, Hybler J
Neues Jahrbuch fur Mineralogie, Monatshefte 1974 (1974) 541-560
The crystal structures of krupkaite, CuPbBi3S6, and of gladite, CuPbBi5S9,
and the classification of superstructures in the bismuthinite-aikinite group,
Locality: Krupka, Ore Mountains, NW-Bohemia
_database_code_amcsd 0014751
CELL PARAMETERS: 33.6200 11.4800 4.0000 90.000 90.000 90.000
SPACE GROUP: Pbnm
X-RAY WAVELENGTH: 1.541838
Cell Volume: 1543.830
Density (g/cm3): 6.901
MAX. ABS. INTENSITY / VOLUME**2: 86.15189515
RIR: 4.065
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
5.26 4.53 16.8100 2 0 0 2
8.14 9.79 10.8641 1 1 0 4
9.33 1.14 9.4802 2 1 0 4
15.44 14.45 5.7400 0 2 0 2
15.66 2.49 5.6581 1 2 0 4
15.82 4.10 5.6033 6 0 0 2
16.32 2.57 5.4320 2 2 0 4
17.36 18.01 5.1088 3 2 0 4
17.61 1.55 5.0355 6 1 0 4
21.14 2.75 4.2025 8 0 0 2
22.17 56.93 4.0096 6 2 0 4
22.53 5.13 3.9464 8 1 0 4
23.62 25.39 3.7672 3 0 1 4
23.85 1.60 3.7312 2 3 0 4
24.15 1.64 3.6854 2 1 1 8
24.16 1.61 3.6835 7 2 0 4
24.58 100.00 3.6214 3 3 0 4
24.88 49.91 3.5794 3 1 1 8
25.07 90.63 3.5522 9 1 0 4
25.58 1.90 3.4827 4 3 0 4
26.51 3.96 3.3620 10 0 0 2
26.81 1.05 3.3258 5 3 0 4
27.08 1.32 3.2932 5 1 1 8
27.17 20.12 3.2818 0 2 1 4
27.30 4.39 3.2662 1 2 1 8
27.70 1.36 3.2209 2 2 1 8
28.24 6.82 3.1601 6 3 0 4
28.34 50.60 3.1495 3 2 1 8
28.50 73.30 3.1321 6 1 1 8
28.51 8.98 3.1309 9 2 0 4
29.85 1.48 2.9929 7 3 0 4
30.10 4.28 2.9691 7 1 1 8
30.26 2.56 2.9535 11 1 0 4
31.16 4.36 2.8700 0 4 0 2
31.59 85.34 2.8318 6 2 1 8
31.62 1.12 2.8294 8 3 0 4
31.63 1.00 2.8291 2 4 0 4
31.94 2.47 2.8017 12 0 0 2
32.20 1.34 2.7803 3 4 0 4
32.80 18.61 2.7301 9 0 1 4
32.91 3.97 2.7218 12 1 0 4
33.38 1.06 2.6846 3 3 1 8
33.52 2.31 2.6731 9 3 0 4
33.75 34.64 2.6561 9 1 1 8
33.96 1.78 2.6396 5 4 0 4
35.13 41.80 2.5544 6 4 0 4
35.54 1.32 2.5257 10 3 0 4
35.66 13.82 2.5178 12 2 0 4
36.23 13.88 2.4796 6 3 1 8
36.47 1.13 2.4637 7 4 0 4
38.33 1.24 2.3484 10 2 1 8
38.61 23.62 2.3319 0 4 1 4
38.71 3.79 2.3263 1 4 1 8
39.47 29.88 2.2830 3 4 1 8
39.60 3.13 2.2759 9 4 0 4
39.88 3.29 2.2606 12 3 0 4
40.07 19.05 2.2502 12 1 1 8
40.32 4.61 2.2366 11 2 1 8
40.59 8.04 2.2225 9 3 1 8
41.03 2.75 2.1998 15 1 0 4
41.97 8.68 2.1529 6 4 1 8
42.17 3.42 2.1427 13 3 0 4
42.36 1.42 2.1339 13 1 1 8
42.42 16.01 2.1308 12 2 1 8
42.55 6.58 2.1246 6 5 0 4
43.05 1.04 2.1012 16 0 0 2
43.34 4.51 2.0878 15 2 0 4
44.72 1.41 2.0265 14 1 1 8
45.23 4.91 2.0048 12 4 0 4
45.34 36.83 2.0000 0 0 2 2
45.88 1.32 1.9781 9 4 1 8
45.89 1.25 1.9775 2 5 1 8
46.12 35.77 1.9680 12 3 1 8
46.31 6.62 1.9606 3 5 1 8
46.42 11.99 1.9561 9 5 0 4
46.44 18.56 1.9553 15 0 1 4
46.89 2.26 1.9376 4 5 1 8
46.98 18.94 1.9340 15 3 0 4
47.15 2.70 1.9275 15 1 1 8
47.52 10.53 1.9133 0 6 0 2
48.18 1.45 1.8886 0 2 2 4
48.25 1.30 1.8860 3 6 0 4
48.52 7.87 1.8763 6 5 1 8
48.75 10.05 1.8678 18 0 0 2
48.91 2.10 1.8624 3 2 2 8
49.44 1.16 1.8435 18 1 0 4
49.49 1.04 1.8417 14 4 0 4
49.53 2.10 1.8403 5 6 0 4
50.33 1.41 1.8131 14 3 1 8
50.40 1.28 1.8107 6 6 0 4
50.95 1.81 1.7923 12 4 1 8
51.03 11.06 1.7897 6 2 2 8
51.45 2.31 1.7761 18 2 0 4
51.55 1.63 1.7728 17 0 1 4
51.65 2.36 1.7696 16 2 1 8
51.75 1.98 1.7665 15 4 0 4
52.04 11.15 1.7572 9 5 1 8
52.25 22.95 1.7507 3 3 2 8
52.31 1.32 1.7488 19 1 0 4
52.51 21.70 1.7428 9 1 2 8
52.56 2.79 1.7412 15 3 1 8
53.06 9.96 1.7260 0 6 1 4
53.30 1.01 1.7189 10 0 2 4
53.73 3.17 1.7059 3 6 1 8
53.83 1.46 1.7029 9 6 0 4
54.28 1.68 1.6900 6 3 2 8
54.44 2.48 1.6855 9 2 2 8
54.83 4.33 1.6743 18 1 1 8
55.04 1.50 1.6684 11 5 1 8
55.23 1.67 1.6633 20 1 0 4
55.73 1.47 1.6495 6 6 1 8
56.05 1.40 1.6409 0 4 2 4
56.51 1.19 1.6285 17 4 0 4
56.72 4.47 1.6231 12 5 1 8
57.15 1.58 1.6117 12 1 2 8
57.52 2.25 1.6024 19 1 1 8
58.62 16.09 1.5747 6 4 2 8
58.65 1.22 1.5740 6 7 0 4
58.95 2.62 1.5669 9 6 1 8
58.98 5.45 1.5660 12 2 2 8
59.00 3.66 1.5655 18 4 0 4
59.99 4.19 1.5421 21 2 0 4
60.39 1.88 1.5328 14 5 1 8
61.34 1.46 1.5113 2 7 1 8
61.69 7.47 1.5037 3 7 1 8
61.75 1.45 1.5023 9 4 2 8
61.78 6.27 1.5017 9 7 0 4
61.95 1.54 1.4979 12 3 2 8
62.16 1.22 1.4933 4 7 1 8
62.79 1.36 1.4798 15 1 2 8
63.07 1.47 1.4740 21 1 1 8
63.52 3.31 1.4647 6 7 1 8
63.64 1.71 1.4621 13 3 2 8
63.85 4.07 1.4578 18 4 1 8
63.93 3.40 1.4563 6 5 2 8
63.98 2.51 1.4552 15 6 0 4
64.29 1.47 1.4489 18 5 0 4
64.52 2.33 1.4443 15 2 2 8
64.79 7.80 1.4389 21 2 1 8
64.92 1.37 1.4364 20 3 1 8
65.59 2.01 1.4234 3 8 0 4
65.98 2.71 1.4159 12 4 2 8
66.01 3.37 1.4153 12 7 0 4
66.78 1.24 1.4008 24 0 0 2
66.91 6.91 1.3984 9 5 2 8
67.35 11.03 1.3903 15 3 2 8
67.63 1.55 1.3853 22 2 1 8
67.78 6.25 1.3826 0 6 2 4
68.63 4.83 1.3675 15 6 1 8
68.77 6.13 1.3651 18 0 2 4
68.93 1.33 1.3623 18 5 1 8
69.01 1.13 1.3609 24 2 0 4
69.40 1.30 1.3542 5 6 2 8
70.18 1.36 1.3410 3 8 1 8
70.45 2.31 1.3365 18 6 0 4
70.97 1.51 1.3280 18 2 2 8
71.22 1.31 1.3240 15 4 2 8
71.30 1.16 1.3227 19 5 1 8
71.48 11.96 1.3198 21 4 1 8
71.77 2.08 1.3153 3 1 3 8
71.88 2.83 1.3134 24 1 1 8
71.90 3.98 1.3131 6 8 1 8
72.96 1.02 1.2966 9 6 2 8
73.39 2.68 1.2901 3 2 3 8
73.47 3.72 1.2889 6 1 3 8
74.15 1.18 1.2788 20 1 2 8
74.91 1.15 1.2676 18 6 1 8
74.93 1.63 1.2674 3 9 0 4
75.08 5.13 1.2652 6 2 3 8
75.69 4.38 1.2565 15 7 1 8
75.75 1.19 1.2557 9 0 3 4
76.28 2.37 1.2483 9 1 3 8
77.03 1.26 1.2379 27 1 0 4
77.22 1.21 1.2354 11 8 1 8
77.42 2.86 1.2327 18 4 2 8
77.74 1.10 1.2285 6 3 3 8
78.29 3.35 1.2212 21 2 2 8
78.64 1.80 1.2167 12 8 1 8
79.22 2.16 1.2092 0 4 3 4
79.77 2.85 1.2022 3 4 3 8
79.88 5.18 1.2008 9 7 2 8
80.16 1.86 1.1974 12 1 3 8
80.28 1.01 1.1958 24 5 0 4
80.85 2.61 1.1889 27 0 1 4
81.73 1.75 1.1783 12 2 3 8
81.78 1.94 1.1777 18 7 1 8
81.86 2.18 1.1767 15 6 2 8
82.15 1.25 1.1734 18 5 2 8
83.22 1.58 1.1609 12 9 0 4
83.33 1.77 1.1597 3 8 2 8
83.58 1.43 1.1569 15 8 1 8
83.69 1.72 1.1556 9 9 1 8
83.71 3.06 1.1553 12 7 2 8
84.33 4.66 1.1484 12 3 3 8
84.43 1.14 1.1474 24 0 2 4
84.56 2.45 1.1459 15 0 3 4
86.10 1.13 1.1294 6 5 3 8
86.50 1.05 1.1251 24 2 2 8
87.49 1.69 1.1149 12 9 1 8
87.85 2.26 1.1112 18 6 2 8
88.64 2.34 1.1035 0 10 1 4
88.81 1.83 1.1017 9 5 3 8
89.62 1.76 1.0939 0 6 3 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.