Hilgardite
Rumanova I M, Iorysh Z I, Belov N V
Soviet Physics Doklady 22 (1977) 460-462
Crystal structure of triclinic chilgardite Ca2[B5O9]Cl*H2O =
Ca2[B3+-B2deltaO9]Cl*H2O
Note: polytype hilgardite-1A
Locality: not given
_database_code_amcsd 0015604
CELL PARAMETERS: 6.4630 6.5640 6.3020 61.630 118.770 105.780
SPACE GROUP: P1
X-RAY WAVELENGTH: 1.541838
Cell Volume: 205.878
Density (g/cm3): 2.692
MAX. ABS. INTENSITY / VOLUME**2: 5.288466101
RIR: 0.640
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
15.37 37.42 5.7666 0 1 0 1
15.67 31.69 5.6563 1 0 0 1
17.59 16.28 5.0430 0 0 1 1
17.74 3.04 5.0008 -1 1 1 1
18.03 1.51 4.9193 0 1 1 1
21.38 18.91 4.1562 -1 1 0 1
22.63 1.14 3.9294 1 1 0 1
27.85 14.80 3.2032 0 -1 1 1
28.03 34.51 3.1831 -1 2 1 1
28.18 9.98 3.1665 1 0 1 1
28.32 28.65 3.1509 -1 1 2 1
28.39 12.32 3.1440 -2 1 1 1
28.65 11.64 3.1158 -1 -1 1 1
28.72 1.77 3.1088 0 2 1 1
28.96 7.92 3.0835 1 1 1 1
29.08 20.71 3.0709 -2 0 1 1
31.02 100.00 2.8833 0 2 0 1
31.64 94.54 2.8281 2 0 0 1
32.31 13.47 2.7711 -1 0 2 1
32.43 28.97 2.7606 0 1 2 1
32.45 6.69 2.7591 -1 2 2 1
32.63 28.73 2.7446 -2 1 2 1
34.10 11.83 2.6291 -1 2 0 1
34.53 10.02 2.5974 -2 1 0 1
35.51 2.74 2.5283 -2 2 1 1
35.60 6.06 2.5215 0 0 2 1
35.74 6.46 2.5124 1 2 0 1
35.92 1.97 2.5004 -2 2 2 1
36.15 10.26 2.4847 2 1 0 1
36.53 5.33 2.4596 0 2 2 1
37.15 2.03 2.4200 1 2 1 1
37.19 4.84 2.4179 -2 -1 1 1
41.96 5.53 2.1529 0 -2 1 1
42.15 16.16 2.1440 -1 3 1 1
42.38 20.44 2.1326 -1 -1 2 1
42.61 4.03 2.1217 -1 3 2 1
42.66 29.21 2.1193 2 0 1 1
42.82 7.14 2.1119 1 1 2 1
42.87 2.25 2.1095 -1 -2 1 1
42.88 1.54 2.1089 -3 1 1 1
42.97 5.60 2.1046 0 3 1 1
43.13 10.22 2.0976 -3 1 2 1
43.55 4.36 2.0782 2 1 1 1
43.55 4.37 2.0781 -2 2 0 1
44.39 4.71 2.0408 -1 1 3 1
44.58 5.57 2.0324 -2 2 3 1
44.64 30.82 2.0300 -1 2 3 1
44.67 5.95 2.0287 -2 1 3 1
44.72 6.13 2.0265 0 -1 2 1
45.08 6.31 2.0109 -2 3 2 1
45.44 17.09 1.9958 -3 2 2 1
46.18 17.72 1.9658 -2 -1 2 1
46.21 6.01 1.9647 2 2 0 1
46.25 9.30 1.9630 0 3 2 1
46.46 1.43 1.9547 1 2 2 1
46.64 13.88 1.9475 -3 0 2 1
47.16 1.93 1.9271 1 -2 1 1
47.29 4.74 1.9222 0 3 0 1
47.40 10.98 1.9179 -2 3 1 1
47.59 3.07 1.9107 2 -1 1 1
47.85 7.89 1.9011 -3 2 1 1
48.27 3.02 1.8854 3 0 0 1
49.20 4.93 1.8519 -1 3 0 1
49.62 4.09 1.8374 -2 -2 1 1
49.64 15.21 1.8365 1 3 1 1
49.75 4.17 1.8328 -1 0 3 1
49.93 5.33 1.8265 0 1 3 1
50.00 10.76 1.8240 2 2 1 1
50.08 5.12 1.8216 -2 3 3 1
50.10 5.01 1.8208 -3 -1 1 1
50.31 6.04 1.8136 -3 2 3 1
50.43 4.43 1.8096 -1 3 3 1
50.46 3.38 1.8085 0 2 3 1
51.03 1.29 1.7896 1 3 0 1
51.86 1.02 1.7631 3 1 0 1
52.54 13.16 1.7418 1 -1 2 1
53.00 3.04 1.7279 -3 3 2 1
55.05 3.27 1.6681 1 3 2 1
55.09 1.47 1.6669 -3 3 3 1
55.12 7.42 1.6662 -3 -1 2 1
55.90 1.37 1.6447 -1 -2 2 1
56.09 1.84 1.6398 0 3 3 1
56.73 2.31 1.6228 2 1 2 1
57.10 2.80 1.6130 -4 1 2 1
57.18 6.46 1.6110 2 -2 1 1
57.45 5.04 1.6040 -3 3 1 1
57.55 1.63 1.6016 0 -2 2 1
57.90 2.12 1.5928 0 -3 1 1
58.09 3.39 1.5880 -1 4 1 1
58.89 1.40 1.5683 -1 -3 1 1
59.01 1.06 1.5654 3 0 1 1
59.59 3.75 1.5516 -1 -1 3 1
60.00 1.51 1.5418 2 2 2 1
60.10 1.52 1.5395 1 1 3 1
60.12 1.01 1.5390 3 2 0 1
60.17 3.25 1.5379 -4 0 1 1
60.35 1.18 1.5337 -2 -1 3 1
60.60 3.06 1.5281 -1 4 3 1
60.62 1.80 1.5276 -4 2 3 1
60.71 1.45 1.5255 2 3 1 1
60.88 1.20 1.5217 -2 1 4 1
60.94 4.77 1.5204 -1 2 4 1
61.18 1.45 1.5150 -3 2 4 1
61.22 2.62 1.5140 -4 1 3 1
62.08 1.15 1.4950 -2 4 1 1
63.31 2.01 1.4689 -3 3 4 1
63.60 1.02 1.4629 -1 3 4 1
63.66 1.40 1.4617 -3 1 4 1
63.67 2.93 1.4615 0 -1 3 1
64.49 1.21 1.4449 -3 4 2 1
64.63 2.27 1.4420 -4 3 3 1
64.65 2.57 1.4416 0 4 0 1
64.68 1.05 1.4411 -2 -3 1 1
64.95 1.03 1.4357 -4 3 2 1
65.67 1.13 1.4218 -4 -1 1 1
65.97 2.10 1.4161 -1 4 0 1
66.07 2.19 1.4141 4 0 0 1
67.28 2.56 1.3916 -4 1 0 1
67.32 2.07 1.3910 -3 -2 2 1
67.62 1.08 1.3855 -2 0 4 1
67.68 1.96 1.3844 2 3 2 1
67.85 1.42 1.3813 -4 -1 2 1
69.29 1.36 1.3561 -1 0 4 1
69.30 1.72 1.3559 4 1 0 1
70.24 1.01 1.3400 2 -3 1 1
70.51 1.10 1.3356 -3 0 4 1
70.52 1.75 1.3354 -3 4 1 1
70.61 1.55 1.3339 -1 4 4 1
71.04 1.26 1.3269 -4 3 1 1
72.15 1.47 1.3092 1 -1 3 1
72.83 1.09 1.2987 -4 2 0 1
73.50 1.11 1.2884 -2 5 2 1
74.13 3.11 1.2791 -1 5 3 1
74.71 1.64 1.2706 2 2 3 1
75.14 1.24 1.2644 3 3 1 1
75.22 1.77 1.2632 -4 -2 1 1
75.65 3.60 1.2571 0 -4 1 1
75.71 1.16 1.2562 2 4 0 1
77.12 1.10 1.2367 2 0 3 1
77.28 1.29 1.2346 4 0 1 1
77.54 1.07 1.2311 -5 1 1 1
78.26 1.02 1.2216 -2 -1 4 1
78.60 1.33 1.2172 -5 0 1 1
78.64 1.01 1.2166 1 -3 2 1
78.73 1.03 1.2154 -2 5 4 1
78.92 4.03 1.2130 1 2 4 1
79.60 1.05 1.2044 3 -1 2 1
81.50 1.06 1.1810 -1 5 4 1
82.19 2.07 1.1728 -2 -4 1 1
82.26 1.44 1.1720 -5 1 4 1
82.29 1.38 1.1717 1 5 1 1
82.36 1.14 1.1708 -4 3 0 1
83.54 1.24 1.1573 3 3 2 1
83.79 1.47 1.1545 -5 -1 1 1
86.41 2.81 1.1261 2 -4 1 1
88.48 1.09 1.1050 -4 -3 1 1
88.74 2.22 1.1024 1 4 4 1
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.