Rosickyite
Steudel R, Steidel J, Reinhardt R
Zeitschrift fur Naturforschung B38 (1983) 1548-1556
X-ray structural analyses of cyclodecasulfur (S10) and of a
cyclohexasulfur-cyclodecasulfur molecular addition compound (S6*S10)
Locality: synthetic
Sample: at T = 163 K
Note: structure pertaining to mix of S6 and S10
_database_code_amcsd 0015842
CELL PARAMETERS: 19.5410 9.4310 8.8310 90.000 105.110 90.000
SPACE GROUP: I2/a
X-RAY WAVELENGTH: 1.541838
Cell Volume: 1571.209
Density (g/cm3): 2.169
MAX. ABS. INTENSITY / VOLUME**2: 5.808633403
RIR: 0.872
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
15.28 8.37 5.7970 -2 1 1 4
18.34 49.28 4.8381 2 1 1 4
18.82 9.93 4.7164 4 0 0 2
20.51 8.83 4.3313 -2 0 2 2
20.84 39.45 4.2628 0 0 2 2
21.06 18.30 4.2178 2 2 0 4
21.21 100.00 4.1889 -4 1 1 4
21.46 1.09 4.1416 -1 2 1 4
22.24 9.05 3.9968 -1 1 2 4
22.63 3.18 3.9289 1 2 1 4
23.90 6.76 3.7239 -3 1 2 4
24.22 5.36 3.6747 -4 0 2 2
24.26 22.36 3.6688 -3 2 1 4
25.07 15.27 3.5526 2 0 2 2
25.43 66.66 3.5031 5 1 0 4
25.65 14.01 3.4727 4 1 1 4
27.31 92.46 3.2661 3 2 1 4
27.97 9.14 3.1899 -2 2 2 4
28.22 59.27 3.1622 0 2 2 4
28.39 16.60 3.1442 6 0 0 2
29.77 13.73 3.0014 3 1 2 4
30.01 7.50 2.9779 -5 2 1 4
30.30 4.49 2.9495 0 3 1 4
30.62 12.55 2.9200 -6 0 2 2
30.85 46.50 2.8985 -4 2 2 4
30.94 10.09 2.8904 -2 3 1 4
31.53 10.15 2.8374 2 2 2 4
31.82 3.13 2.8119 3 3 0 4
31.87 45.93 2.8077 -2 1 3 4
32.62 3.69 2.7455 2 3 1 4
33.67 2.53 2.6620 -4 1 3 4
34.16 4.63 2.6245 5 2 1 4
34.21 2.78 2.6207 6 1 1 4
34.28 8.17 2.6160 6 2 0 4
34.38 2.47 2.6088 -4 3 1 4
34.61 17.53 2.5913 7 1 0 4
35.05 15.99 2.5604 -1 3 2 4
36.16 2.36 2.4841 -3 3 2 4
36.18 15.18 2.4826 -6 2 2 4
36.56 33.70 2.4580 1 3 2 4
36.58 10.45 2.4563 2 1 3 4
36.95 1.69 2.4330 5 1 2 4
37.17 3.78 2.4190 4 2 2 4
37.23 7.38 2.4152 5 3 0 4
37.39 6.23 2.4052 4 3 1 4
37.95 4.73 2.3711 -6 1 3 4
38.06 1.14 2.3643 -8 1 1 4
38.16 3.86 2.3582 8 0 0 2
38.33 4.33 2.3484 1 2 3 4
38.51 2.60 2.3377 -8 0 2 2
39.70 11.60 2.2701 -5 3 2 4
40.30 2.00 2.2378 1 4 1 4
41.71 4.20 2.1657 -4 0 4 2
42.07 9.65 2.1477 -2 3 3 4
42.29 2.46 2.1373 4 1 3 4
42.41 2.09 2.1314 0 0 4 2
42.52 3.73 2.1262 -1 1 4 4
42.90 8.61 2.1082 0 3 3 4
43.19 5.57 2.0944 -8 2 2 4
43.47 5.38 2.0817 8 1 1 4
43.94 1.73 2.0606 -9 1 2 4
44.22 4.15 2.0481 -7 2 3 4
44.27 6.81 2.0461 7 3 0 4
45.12 4.73 2.0093 -5 4 1 4
45.28 1.11 2.0027 7 1 2 4
46.02 17.15 1.9720 -9 2 1 4
46.21 1.04 1.9645 2 4 2 4
46.77 3.72 1.9422 0 2 4 4
47.34 5.48 1.9203 -10 0 2 2
47.56 1.78 1.9119 -10 1 1 4
48.16 1.01 1.8895 5 4 1 4
48.50 8.68 1.8768 1 5 0 4
48.76 6.09 1.8676 8 0 2 2
48.85 3.80 1.8645 5 2 3 4
48.92 5.33 1.8619 -6 2 4 4
49.62 1.36 1.8374 -8 0 4 2
49.67 1.01 1.8356 -1 4 3 4
49.92 4.27 1.8270 -2 5 1 4
50.52 1.31 1.8067 3 5 0 4
50.63 2.29 1.8028 -3 3 4 4
50.72 4.10 1.8000 -7 4 1 4
50.74 1.38 1.7994 4 3 3 4
50.74 1.43 1.7994 -9 2 3 4
51.32 9.35 1.7804 9 2 1 4
51.38 9.01 1.7782 1 4 3 4
51.44 1.18 1.7763 4 0 4 2
51.61 2.97 1.7711 -10 1 3 4
52.17 6.69 1.7532 -5 4 3 4
52.47 1.01 1.7440 9 3 0 4
52.72 2.80 1.7363 8 2 2 4
52.78 1.56 1.7344 -1 5 2 4
52.92 1.68 1.7303 -2 1 5 4
53.00 1.37 1.7279 -11 1 2 4
53.18 10.23 1.7224 1 3 4 4
53.36 9.36 1.7168 7 3 2 4
53.53 4.51 1.7120 -8 2 4 4
53.59 1.44 1.7101 -3 5 2 4
53.62 3.24 1.7093 -9 1 4 4
54.37 2.93 1.6874 11 1 0 4
54.38 1.91 1.6871 5 5 0 4
54.50 3.01 1.6837 4 5 1 4
54.70 3.57 1.6779 0 1 5 4
54.95 11.71 1.6709 3 4 3 4
55.03 6.33 1.6688 -6 1 5 4
55.26 7.75 1.6623 4 2 4 4
55.39 4.28 1.6586 -10 3 1 4
55.57 3.44 1.6539 -3 2 5 4
55.78 4.46 1.6479 -7 3 4 4
56.05 5.47 1.6408 -10 0 4 2
56.20 6.14 1.6367 -7 4 3 4
56.25 2.87 1.6353 -5 5 2 4
56.30 1.20 1.6340 7 2 3 4
56.38 4.68 1.6319 -1 2 5 4
56.59 5.96 1.6262 -5 2 5 4
56.82 4.78 1.6204 3 5 2 4
57.11 2.01 1.6127 6 3 3 4
57.19 3.63 1.6106 3 3 4 4
57.62 1.39 1.5998 -12 1 1 4
58.10 9.28 1.5877 -2 5 3 4
58.27 1.72 1.5834 2 1 5 4
58.43 3.06 1.5795 10 0 2 2
58.73 8.01 1.5721 12 0 0 2
58.74 1.27 1.5718 0 6 0 2
58.75 1.08 1.5716 0 5 3 4
59.80 2.14 1.5466 -1 6 1 4
59.85 8.62 1.5453 7 5 0 4
60.15 6.58 1.5383 5 4 3 4
60.33 8.63 1.5341 -11 3 2 4
60.60 1.21 1.5279 10 3 1 4
60.61 2.09 1.5278 -7 5 2 4
61.60 1.82 1.5056 11 3 0 4
61.80 8.84 1.5011 -9 4 3 4
61.91 1.95 1.4989 0 3 5 4
62.25 1.08 1.4914 12 2 0 4
62.31 1.12 1.4900 9 4 1 4
62.55 1.32 1.4849 3 6 1 4
63.23 1.32 1.4705 -4 0 6 2
63.63 1.99 1.4624 -2 0 6 2
63.86 1.43 1.4577 -9 2 5 4
64.12 1.90 1.4523 -10 1 5 4
64.48 1.67 1.4452 -4 6 2 4
64.87 2.93 1.4374 2 6 2 4
65.14 2.26 1.4321 -3 5 4 4
65.31 1.63 1.4288 -1 1 6 4
65.71 3.29 1.4209 0 0 6 2
65.91 1.68 1.4171 -11 4 1 4
66.46 1.95 1.4067 -9 5 2 4
66.58 2.11 1.4045 -8 5 3 4
66.66 3.39 1.4030 -7 1 6 4
67.05 4.12 1.3958 10 1 3 4
67.34 1.52 1.3905 -13 2 3 4
67.45 2.26 1.3885 -11 3 4 4
67.51 1.69 1.3874 -8 0 6 2
69.22 3.06 1.3573 1 4 5 4
69.41 1.22 1.3541 2 0 6 2
69.60 1.06 1.3508 -7 4 5 4
69.72 2.92 1.3488 -14 1 3 4
70.00 1.64 1.3440 6 1 5 4
70.80 1.38 1.3308 0 7 1 4
71.01 1.95 1.3274 11 3 2 4
71.15 2.08 1.3252 -2 7 1 4
72.03 1.18 1.3111 -10 0 6 2
72.08 3.87 1.3104 2 7 1 4
72.08 1.17 1.3104 12 2 2 4
73.03 1.22 1.2957 14 2 0 4
73.09 1.73 1.2946 -4 7 1 4
74.17 1.21 1.2785 -3 7 2 4
74.61 2.34 1.2720 4 0 6 2
74.67 1.38 1.2712 9 4 3 4
75.13 1.17 1.2645 13 1 2 4
75.20 1.41 1.2635 -13 4 1 4
76.40 1.06 1.2466 6 3 5 4
76.79 1.35 1.2413 -9 3 6 4
77.07 1.19 1.2374 -13 2 5 4
78.01 1.35 1.2249 -12 0 6 2
78.62 1.81 1.2169 9 6 1 4
78.65 2.37 1.2165 10 2 4 4
78.66 1.32 1.2164 -5 2 7 4
78.95 1.34 1.2126 3 3 6 4
80.09 1.24 1.1982 14 0 2 2
81.68 1.70 1.1789 0 8 0 2
85.01 1.01 1.1410 -17 1 2 4
85.39 1.05 1.1369 -14 0 6 2
85.63 1.44 1.1343 -15 4 1 4
85.68 1.83 1.1338 -7 5 6 4
86.03 1.10 1.1300 10 5 3 4
87.09 1.46 1.1190 1 5 6 4
87.82 1.22 1.1116 12 6 0 4
88.09 1.55 1.1089 -10 7 1 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.