Birnessite Post J E, Veblen D R American Mineralogist 75 (1990) 477-489 Crystal structure determinations of synthetic sodium, magnesium and potassium birnessite using TEM and the Rietveld method Sample: K-birn _database_code_amcsd 0001302 CELL PARAMETERS: 5.1490 2.8430 7.1760 90.000 100.760 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 103.200 Density (g/cm3): 3.541 MAX. ABS. INTENSITY / VOLUME**2: 64.60492174 RIR: 5.940 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.56 100.00 7.0498 0 0 1 2 25.27 35.91 3.5249 0 0 2 2 35.40 4.85 2.5359 -2 0 1 2 35.49 3.05 2.5292 2 0 0 2 36.25 5.41 2.4784 1 1 0 4 37.34 16.82 2.4080 -1 1 1 4 39.63 1.68 2.2739 1 1 1 4 40.06 14.96 2.2508 2 0 1 2 42.63 16.15 2.1207 -1 1 2 4 46.69 3.65 1.9454 1 1 2 4 47.65 2.89 1.9084 -2 0 3 2 48.03 4.47 1.8943 2 0 2 2 51.05 12.86 1.7889 -1 1 3 4 51.88 1.69 1.7625 0 0 4 2 56.36 3.01 1.6323 1 1 3 4 57.92 1.66 1.5921 -2 0 4 2 58.38 3.84 1.5807 2 0 3 2 61.73 2.67 1.5027 -1 1 4 4 63.37 3.28 1.4678 -3 1 1 4 64.22 5.43 1.4503 3 1 0 4 65.55 4.37 1.4241 -3 1 2 4 65.68 3.31 1.4215 0 2 0 2 67.18 1.60 1.3935 0 2 1 4 68.03 4.18 1.3780 1 1 4 4 68.06 1.39 1.3775 3 1 1 4 70.08 1.86 1.3428 -2 0 5 2 71.57 2.42 1.3183 0 2 2 4 74.29 1.33 1.2767 -1 1 5 4 74.89 1.20 1.2679 -4 0 2 2 79.80 2.37 1.2019 2 2 1 4 81.58 1.39 1.1800 1 1 5 4 85.38 1.12 1.1370 2 2 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.