Bottinoite Bonazzi P, Mazzi F American Mineralogist 81 (1996) 1494-1500 Bottinoite, Ni(H2O)6[Sb(OH)6]2: Crystal structure, twinning and hydrogen-bond model Sample: BS2, synthetic Note: U(1,2) for Sb1 and Sb3 changed to match symmetry constraints. _database_code_amcsd 0001841 CELL PARAMETERS: 16.0600 16.0600 9.7920 90.000 90.000 120.000 SPACE GROUP: P3 X-RAY WAVELENGTH: 1.541838 Cell Volume: 2187.223 Density (g/cm3): 2.688 MAX. ABS. INTENSITY / VOLUME**2: 53.00923917 RIR: 6.421 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.03 4.83 9.7920 0 0 1 1 11.02 2.47 8.0300 1 1 0 3 14.26 1.65 6.2092 1 1 1 3 14.26 1.14 6.2092 2 -1 1 3 18.12 33.02 4.8960 0 0 2 1 19.14 100.00 4.6361 3 0 0 3 19.22 1.55 4.6182 0 1 2 3 19.22 1.76 4.6182 1 0 2 3 21.20 2.53 4.1902 0 3 1 3 21.20 2.38 4.1902 3 0 1 3 21.25 1.08 4.1803 2 -1 2 3 22.21 1.03 4.0034 0 2 2 3 22.21 1.08 4.0034 2 0 2 3 26.48 31.01 3.3664 0 3 2 3 26.48 35.02 3.3664 3 0 2 3 33.48 7.64 2.6767 3 3 0 3 34.74 4.07 2.5819 6 -3 1 3 34.78 1.05 2.5796 1 4 2 3 34.78 1.72 2.5796 -1 5 2 3 34.78 3.44 2.5796 5 -1 2 3 38.32 7.32 2.3486 6 -3 2 3 38.32 14.95 2.3486 3 3 2 3 38.85 5.09 2.3181 6 0 0 3 41.72 5.17 2.1648 0 3 4 3 41.72 5.29 2.1648 3 0 4 3 43.18 6.32 2.0951 0 6 2 3 43.18 8.59 2.0951 6 0 2 3 43.74 1.64 2.0697 6 -3 3 3 44.70 1.20 2.0272 5 2 2 3 50.52 6.07 1.8064 3 3 4 3 50.52 5.59 1.8064 6 -3 4 3 52.20 6.26 1.7523 3 6 0 3 52.20 5.93 1.7523 6 3 0 3 54.52 4.37 1.6832 0 6 4 3 54.52 4.50 1.6832 6 0 4 3 55.72 3.13 1.6498 -3 9 2 3 55.72 3.54 1.6498 3 6 2 3 55.72 3.69 1.6498 6 3 2 3 55.72 3.48 1.6498 9 -3 2 3 59.85 3.16 1.5454 9 0 0 3 60.10 1.02 1.5394 0 3 6 3 63.08 2.11 1.4737 0 9 2 3 63.08 2.16 1.4737 9 0 2 3 65.51 1.02 1.4249 3 6 4 3 65.51 1.03 1.4249 -3 9 4 3 65.51 1.06 1.4249 6 3 4 3 70.34 2.89 1.3383 6 6 0 3 73.33 1.61 1.2910 12 -6 2 3 73.33 1.15 1.2910 6 6 2 3 73.68 1.71 1.2858 3 9 0 3 73.68 1.64 1.2858 9 3 0 3 76.62 1.23 1.2437 -3 12 2 3 76.62 1.08 1.2437 3 9 2 3 76.62 1.15 1.2437 12 -3 2 3 79.15 1.07 1.2100 1 1 8 3 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.