Bottinoite Bonazzi P, Mazzi F American Mineralogist 81 (1996) 1494-1500 Bottinoite, Ni(H2O)6[Sb(OH)6]2: Crystal structure, twinning and hydrogen-bond model Sample: BN1, natural Locality: Bottino mine, Apuan Alps, Italy Note: U(1,2) for Sb5 and Sb6 changed to match symmetry constraints. _database_code_amcsd 0001842 CELL PARAMETERS: 16.0450 16.0450 9.7840 90.000 90.000 120.000 SPACE GROUP: P3 X-RAY WAVELENGTH: 1.541838 Cell Volume: 2181.356 Density (g/cm3): 2.695 MAX. ABS. INTENSITY / VOLUME**2: 53.26952254 RIR: 6.435 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.04 4.53 9.7840 0 0 1 1 11.03 2.47 8.0225 1 1 0 3 14.28 1.51 6.2037 1 1 1 3 14.28 1.17 6.2037 2 -1 1 3 18.13 34.01 4.8920 0 0 2 1 19.16 100.00 4.6318 3 0 0 3 19.23 1.58 4.6144 0 1 2 3 19.23 1.65 4.6144 1 0 2 3 21.22 2.41 4.1864 0 3 1 3 21.22 2.50 4.1864 3 0 1 3 21.27 1.20 4.1767 2 -1 2 3 22.22 1.24 3.9999 0 2 2 3 22.22 1.25 3.9999 2 0 2 3 24.87 1.03 3.5797 1 2 2 3 26.50 30.97 3.3634 0 3 2 3 26.50 34.12 3.3634 3 0 2 3 33.51 7.49 2.6742 3 3 0 3 34.78 4.03 2.5796 6 -3 1 3 34.81 1.01 2.5773 1 4 2 3 34.81 1.73 2.5773 -1 5 2 3 34.81 3.30 2.5773 5 -1 2 3 38.36 7.12 2.3465 6 -3 2 3 38.36 14.39 2.3465 3 3 2 3 38.89 4.97 2.3159 6 0 0 3 41.76 4.88 2.1629 0 3 4 3 41.76 5.13 2.1629 3 0 4 3 43.22 6.16 2.0932 0 6 2 3 43.22 8.25 2.0932 6 0 2 3 43.78 1.72 2.0679 6 -3 3 3 44.75 1.23 2.0254 5 2 2 3 50.57 5.78 1.8049 3 3 4 3 50.57 5.19 1.8049 6 -3 4 3 52.25 6.10 1.7507 3 6 0 3 52.25 5.67 1.7507 6 3 0 3 54.57 4.02 1.6817 0 6 4 3 54.57 4.35 1.6817 6 0 4 3 55.77 2.89 1.6483 -3 9 2 3 55.77 3.55 1.6483 3 6 2 3 55.77 3.48 1.6483 9 -3 2 3 55.77 3.55 1.6483 6 3 2 3 59.91 3.05 1.5439 9 0 0 3 63.15 1.99 1.4723 0 9 2 3 63.15 2.11 1.4723 9 0 2 3 65.58 1.01 1.4236 3 6 4 3 65.58 1.00 1.4236 6 3 4 3 65.58 1.00 1.4236 9 -3 4 3 70.42 2.79 1.3371 6 6 0 3 73.41 1.52 1.2898 12 -6 2 3 73.41 1.08 1.2898 6 6 2 3 73.76 1.66 1.2846 3 9 0 3 73.76 1.55 1.2846 9 3 0 3 76.70 1.11 1.2425 -3 12 2 3 76.70 1.06 1.2425 3 9 2 3 76.70 1.10 1.2425 12 -3 2 3 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.