data_global
_chemical_name_mineral 'Minium'
loop_
_publ_author_name
'Dinnebier R E'
'Carlson S'
'Hanfland M'
'Jansen M'
_journal_name_full 'American Mineralogist'
_journal_volume 88 
_journal_year 2003
_journal_page_first 996
_journal_page_last 1002
_publ_section_title
;
 Bulk modulus and high-pressure crystal structures of minium, Pb3O4,
 determined by X-ray powder diffraction
 Sample: Phase III of Pb3O4 at 13.3 GPa
;
_database_code_amcsd 0003132
_chemical_formula_sum 'Pb3 O4'
_cell_length_a 9.3812
_cell_length_b 6.4610
_cell_length_c 3.3168
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 201.038
_exptl_crystal_density_diffrn     11.326
_symmetry_space_group_name_H-M 'P b a m'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  '1/2+x,1/2-y,z'
  '1/2-x,1/2+y,-z'
  '1/2-x,1/2+y,z'
  '1/2+x,1/2-y,-z'
  'x,y,-z'
  '-x,-y,z'
  '-x,-y,-z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
Pb1   0.67564   0.94970   0.50000   0.01400
Pb2   0.50000   0.50000   0.00000   0.01700
O1   0.31320   0.30140   0.00000   0.04200
O2   0.58410   0.31080   0.50000   0.04200