Goethite Alvarez M, Sileo E E, Rueda E H American Mineralogist 93 (2008) 584-590 Structure and reactivity of synthetic Co-substituted goethites Locality: synthetic Sample: G0, 0 mol% Co Note: changed OH(x) to match reported bond distances _database_code_amcsd 0004538 CELL PARAMETERS: 4.6163 9.9564 3.0248 90.000 90.000 90.000 SPACE GROUP: Pbnm X-RAY WAVELENGTH: 1.541838 Cell Volume: 139.025 Density (g/cm3): 4.196 MAX. ABS. INTENSITY / VOLUME**2: 41.32483172 RIR: 3.207 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 17.82 12.24 4.9782 0 2 0 2 21.21 100.00 4.1880 1 1 0 4 26.33 11.08 3.3849 1 2 0 4 33.25 41.26 2.6947 1 3 0 4 34.70 24.00 2.5850 0 2 1 4 35.48 4.80 2.5300 1 0 1 4 36.08 14.47 2.4891 0 4 0 2 36.65 66.19 2.4521 1 1 1 8 39.02 3.23 2.3082 2 0 0 2 39.97 8.64 2.2555 1 2 1 8 40.10 2.81 2.2485 2 1 0 4 41.20 14.93 2.1909 1 4 0 4 43.20 1.13 2.0940 2 2 0 4 45.06 3.48 2.0121 1 3 1 8 47.29 5.94 1.9220 0 4 1 4 50.58 10.76 1.8045 2 1 1 8 51.50 2.46 1.7744 1 4 1 8 53.20 33.62 1.7217 2 2 1 8 54.19 9.68 1.6925 2 4 0 4 55.37 3.34 1.6594 0 6 0 2 57.38 6.92 1.6058 2 3 1 8 59.03 23.03 1.5648 1 5 1 8 61.29 10.00 1.5124 0 0 2 2 61.50 4.62 1.5077 2 5 0 4 62.93 3.27 1.4770 2 4 1 8 63.25 4.47 1.4701 3 2 0 4 64.00 10.05 1.4549 0 6 1 4 65.63 5.96 1.4225 1 1 2 8 67.04 4.41 1.3960 3 3 0 4 67.88 1.08 1.3808 1 2 2 8 68.40 4.42 1.3715 3 0 1 4 69.10 5.36 1.3593 1 7 0 4 69.14 2.04 1.3587 3 1 1 8 69.80 1.99 1.3473 2 6 0 4 71.33 1.78 1.3222 3 2 1 8 71.54 6.85 1.3189 1 3 2 8 73.23 2.86 1.2925 0 4 2 4 74.92 2.05 1.2675 3 3 1 8 75.09 1.08 1.2650 2 0 2 4 76.54 2.38 1.2446 1 4 2 8 79.85 3.26 1.2012 3 4 1 8 84.11 2.41 1.1509 0 8 1 4 84.52 2.90 1.1464 4 1 0 4 86.08 1.10 1.1295 3 5 1 8 86.20 1.04 1.1283 3 6 0 4 86.25 3.68 1.1277 2 4 2 8 87.21 1.39 1.1178 0 6 2 4 89.46 1.24 1.0955 2 8 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.