Goethite Alvarez M, Sileo E E, Rueda E H American Mineralogist 93 (2008) 584-590 Structure and reactivity of synthetic Co-substituted goethites Locality: synthetic Sample: G5, 5 mol% Co Note: changed O(x) to match reported bond distances _database_code_amcsd 0004540 CELL PARAMETERS: 4.5975 9.9395 3.0183 90.000 90.000 90.000 SPACE GROUP: Pbnm X-RAY WAVELENGTH: 1.541838 Cell Volume: 137.927 Density (g/cm3): 4.237 MAX. ABS. INTENSITY / VOLUME**2: 42.28153729 RIR: 3.249 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 17.85 11.71 4.9697 0 2 0 2 21.29 100.00 4.1727 1 1 0 4 26.41 10.92 3.3749 1 2 0 4 33.33 40.30 2.6879 1 3 0 4 34.77 23.91 2.5798 0 2 1 4 35.58 4.75 2.5231 1 0 1 4 36.15 14.77 2.4849 0 4 0 2 36.75 65.37 2.4456 1 1 1 8 39.19 3.30 2.2987 2 0 0 2 40.08 8.46 2.2498 1 2 1 8 40.27 2.65 2.2396 2 1 0 4 41.30 14.53 2.1860 1 4 0 4 43.37 1.04 2.0864 2 2 0 4 45.17 3.59 2.0073 1 3 1 8 47.39 5.66 1.9184 0 4 1 4 50.76 10.81 1.7986 2 1 1 8 51.63 2.52 1.7704 1 4 1 8 53.38 33.05 1.7163 2 2 1 8 54.37 9.59 1.6874 2 4 0 4 55.47 3.15 1.6566 0 6 0 2 57.57 6.83 1.6011 2 3 1 8 59.17 22.80 1.5615 1 5 1 8 61.44 9.87 1.5092 0 0 2 2 61.69 4.57 1.5036 2 5 0 4 63.12 3.10 1.4729 2 4 1 8 63.53 4.41 1.4645 3 2 0 4 64.13 10.14 1.4522 0 6 1 4 65.81 5.96 1.4192 1 1 2 8 67.32 4.34 1.3909 3 3 0 4 68.05 1.07 1.3777 1 2 2 8 68.69 4.36 1.3665 3 0 1 4 69.25 5.33 1.3567 1 7 0 4 69.43 1.98 1.3537 3 1 1 8 70.01 1.91 1.3440 2 6 0 4 71.62 1.64 1.3176 3 2 1 8 71.72 6.70 1.3159 1 3 2 8 73.41 2.90 1.2899 0 4 2 4 75.22 2.10 1.2632 3 3 1 8 75.34 1.09 1.2616 2 0 2 4 76.74 2.31 1.2419 1 4 2 8 80.16 3.25 1.1974 3 4 1 8 84.29 2.35 1.1489 0 8 1 4 84.94 2.86 1.1418 4 1 0 4 86.41 1.07 1.1261 3 5 1 8 86.52 1.07 1.1250 3 6 0 4 86.52 3.66 1.1249 2 4 2 8 87.42 1.31 1.1156 0 6 2 4 89.71 1.28 1.0930 2 8 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.