Mitryaevaite Cahill C L, Krivovichev S V, Burns P C, Bekenova G K, Shabanova T A The Canadian Mineralogist 39 (2001) 179-186 The crystal structure of mitryaevaite, Al5(PO4)2[(P,S)O3(OH,O)]2F2(OH)2(H2O)8*6.48H2O, determined from a microcrystal using synchrotron radiation _database_code_amcsd 0005711 CELL PARAMETERS: 6.9180 10.1270 10.2960 77.036 73.989 76.272 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 663.714 Density (g/cm3): 2.209 MAX. ABS. INTENSITY / VOLUME**2: 13.43862366 RIR: 1.981 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.07 100.00 9.7523 0 0 1 2 9.12 1.88 9.6942 0 1 0 2 11.73 3.28 7.5473 0 1 1 2 13.56 17.66 6.5320 1 0 0 2 13.93 17.24 6.3558 0 -1 1 2 14.44 1.11 6.1349 1 0 1 2 14.74 4.04 6.0089 1 1 1 2 17.74 1.04 5.0004 -1 1 0 2 18.03 6.55 4.9187 -1 0 1 2 19.01 1.23 4.6687 0 2 1 2 19.19 4.82 4.6262 1 -1 1 2 19.50 8.68 4.5522 1 1 2 2 19.78 1.08 4.4875 -1 -1 1 2 20.00 3.48 4.4398 1 0 2 2 20.67 1.37 4.2966 1 2 0 2 20.70 2.85 4.2918 -1 1 1 2 21.75 2.01 4.0860 0 -1 2 2 23.58 8.35 3.7737 0 2 2 2 24.29 2.69 3.6640 1 -1 2 2 24.84 10.03 3.5845 -1 2 0 2 26.52 11.55 3.3609 -1 2 1 2 26.69 1.44 3.3405 -1 1 2 2 26.72 10.43 3.3361 1 1 3 2 27.07 1.52 3.2936 -1 -1 2 2 27.31 7.31 3.2660 2 0 0 2 27.31 2.30 3.2653 1 3 1 2 27.41 1.49 3.2535 0 1 3 2 27.44 3.27 3.2508 0 0 3 2 27.60 3.97 3.2314 0 3 0 2 27.63 1.91 3.2288 1 0 3 2 27.91 4.40 3.1962 2 1 2 2 28.08 1.31 3.1779 0 -2 2 2 28.39 5.71 3.1434 2 2 1 2 28.43 9.19 3.1395 1 3 0 2 29.74 1.36 3.0044 2 2 2 2 29.99 1.23 2.9794 2 2 0 2 30.39 5.93 2.9415 2 -1 1 2 30.45 7.00 2.9352 0 -1 3 2 30.47 3.60 2.9333 -2 1 0 2 30.48 1.74 2.9332 0 3 2 2 30.59 2.81 2.9225 0 -3 1 2 30.85 3.07 2.8985 -2 0 1 2 31.17 7.21 2.8696 -2 -1 1 2 32.30 10.94 2.7719 -1 -3 1 2 32.54 2.95 2.7514 2 1 3 2 33.15 3.34 2.7022 -1 3 0 2 33.70 2.31 2.6594 2 2 3 2 33.72 1.37 2.6580 1 3 3 2 34.03 1.04 2.6348 -1 3 1 2 34.14 1.36 2.6265 2 3 2 2 35.04 8.77 2.5610 1 1 4 2 35.78 2.73 2.5097 1 4 1 2 35.78 2.07 2.5095 0 -2 3 2 36.65 1.10 2.4517 0 4 1 2 36.90 1.37 2.4359 1 4 2 2 37.07 1.13 2.4252 1 4 0 2 37.41 2.02 2.4042 -1 2 3 2 38.98 1.39 2.3104 2 1 4 2 39.28 2.23 2.2935 -2 -3 1 2 39.54 2.90 2.2790 -1 -2 3 2 40.01 4.62 2.2532 1 3 4 2 40.19 3.53 2.2437 -2 -2 2 2 40.25 3.91 2.2407 3 2 1 2 40.26 1.10 2.2399 1 4 3 2 40.64 1.48 2.2199 2 0 4 2 42.90 1.45 2.1081 -2 3 0 2 43.50 1.19 2.0805 3 3 1 2 43.55 2.59 2.0781 2 -3 1 2 43.66 1.35 2.0731 -2 0 3 2 44.56 1.92 2.0335 1 -3 3 2 44.73 2.41 2.0261 -3 0 1 2 44.80 1.87 2.0230 -2 1 3 2 44.90 1.05 2.0189 1 -2 4 2 44.90 1.52 2.0188 -1 4 2 2 45.88 2.27 1.9778 -1 -4 2 2 46.63 2.56 1.9477 2 1 5 2 46.83 1.11 1.9400 2 2 5 2 46.86 3.38 1.9388 0 5 0 2 47.12 1.18 1.9286 3 2 4 2 47.42 1.53 1.9171 0 5 2 2 47.69 1.46 1.9069 -2 3 2 2 48.97 1.46 1.8602 -3 2 0 2 49.68 1.25 1.8352 -3 -3 1 2 49.77 1.53 1.8320 2 -2 4 2 51.23 3.87 1.7833 -3 2 1 2 51.99 2.18 1.7590 -1 0 5 2 52.93 2.30 1.7299 3 2 5 2 53.24 1.83 1.7206 4 1 2 2 53.55 1.12 1.7114 0 -2 5 2 54.40 1.19 1.6864 3 3 5 2 54.61 1.02 1.6805 -2 4 2 2 55.05 1.44 1.6681 2 2 6 2 55.22 1.17 1.6634 -3 -3 2 2 56.00 1.12 1.6420 1 3 6 2 56.89 1.08 1.6184 -3 3 1 2 58.81 1.23 1.5701 -4 -1 1 2 59.09 1.36 1.5635 -2 3 4 2 59.57 3.37 1.5520 0 -6 1 2 59.86 2.64 1.5450 -2 5 0 2 60.37 1.21 1.5333 -3 -4 2 2 60.44 1.39 1.5318 -2 5 1 2 62.31 1.46 1.4901 3 5 5 2 63.54 1.26 1.4641 1 1 7 2 63.68 1.09 1.4613 0 -6 2 2 65.62 1.15 1.4228 -1 6 3 2 67.14 1.33 1.3942 -3 -4 3 2 75.80 1.35 1.2549 1 -5 5 2 80.61 1.04 1.1918 5 5 0 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.