Cs4[(UO2)3O(MoO4)2(MoO5)] Krivovichev S V, Burns P C The Canadian Mineralogist 40 (2002) 201-209 Crystal chemistry of uranyl molybdates. VI. New uranyl molybdate units in the structures of Cs4[(UO2)3O(MoO4)2(MoO5)] and Cs6[(UO2)(MoO4)4] _database_code_amcsd 0005765 CELL PARAMETERS: 7.5100 7.8970 9.7740 79.279 81.269 87.251 SPACE GROUP: P1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 562.827 Density (g/cm3): 5.468 MAX. ABS. INTENSITY / VOLUME**2: 64.83209746 RIR: 3.861 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.31 31.45 9.5011 0 0 1 1 11.41 6.35 7.7576 0 1 0 1 11.92 100.00 7.4214 1 0 0 1 13.36 2.09 6.6253 0 1 1 1 14.03 11.90 6.3114 1 0 1 1 16.00 1.48 5.5378 0 -1 1 1 16.19 5.50 5.4748 -1 0 1 1 16.36 6.22 5.4179 1 1 0 1 16.70 4.46 5.3091 -1 1 0 1 18.68 4.77 4.7505 0 0 2 1 18.99 9.79 4.6741 -1 1 1 1 19.31 2.48 4.5961 1 -1 1 1 20.07 5.08 4.4236 0 1 2 1 20.68 1.30 4.2959 -1 -1 1 1 21.82 9.25 4.0725 1 1 2 1 22.93 6.39 3.8788 0 2 0 1 23.15 1.00 3.8428 0 2 1 1 23.66 11.57 3.7602 -1 0 2 1 23.67 4.41 3.7595 0 -1 2 1 23.98 34.10 3.7107 2 0 0 1 24.45 12.37 3.6407 2 0 1 1 24.90 32.71 3.5755 -1 1 2 1 25.24 7.81 3.5281 1 2 1 1 25.41 9.58 3.5059 1 -1 2 1 25.70 18.83 3.4666 1 2 0 1 26.09 22.12 3.4152 2 1 1 1 26.14 13.96 3.4093 -1 2 0 1 26.34 49.82 3.3831 0 -2 1 1 26.41 21.15 3.3743 2 1 0 1 26.84 2.90 3.3213 -2 1 0 1 26.91 38.43 3.3126 0 2 2 1 26.96 11.49 3.3074 -1 2 1 1 27.04 20.98 3.2976 -2 0 1 1 27.71 23.14 3.2197 -1 -1 2 1 27.99 23.18 3.1881 2 -1 1 1 28.16 46.57 3.1684 1 2 2 1 28.18 29.09 3.1670 0 0 3 1 28.28 12.86 3.1557 2 0 2 1 28.45 6.11 3.1376 0 1 3 1 28.62 29.69 3.1188 1 -2 1 1 28.94 9.52 3.0850 -2 1 1 1 29.00 48.66 3.0792 1 0 3 1 29.04 1.58 3.0744 2 1 2 1 29.39 20.20 3.0395 -1 -2 1 1 30.84 10.02 2.8994 -1 2 2 1 32.18 3.58 2.7814 2 2 1 1 32.31 5.36 2.7709 -1 0 3 1 32.33 1.50 2.7689 0 -2 2 1 32.41 3.08 2.7623 0 -1 3 1 32.64 1.49 2.7438 -1 1 3 1 32.71 3.47 2.7374 -2 0 2 1 33.73 1.58 2.6570 -2 1 2 1 33.74 4.58 2.6562 1 -2 2 1 33.77 2.49 2.6545 -2 2 0 1 34.07 1.31 2.6315 2 2 2 1 34.45 1.78 2.6033 2 0 3 1 34.91 2.80 2.5698 -2 2 1 1 35.29 3.27 2.5436 2 -2 1 1 35.75 1.04 2.5119 -2 -1 2 1 36.03 1.01 2.4930 -1 -1 3 1 36.16 1.21 2.4838 3 0 1 1 36.32 6.16 2.4738 3 0 0 1 36.43 5.56 2.4664 0 3 2 1 36.91 1.93 2.4351 -1 2 3 1 37.05 1.17 2.4266 -1 3 0 1 37.10 2.27 2.4233 -1 3 1 1 37.31 1.14 2.4100 1 3 2 1 37.54 1.51 2.3959 0 1 4 1 37.95 1.83 2.3709 3 1 0 1 38.06 7.02 2.3644 1 0 4 1 38.37 4.67 2.3459 2 2 3 1 38.52 3.54 2.3370 -2 2 2 1 39.20 1.12 2.2980 2 -2 2 1 39.43 3.71 2.2851 1 -3 1 1 39.58 2.44 2.2767 -1 3 2 1 39.86 2.33 2.2614 -1 -3 1 1 39.87 2.98 2.2608 0 -2 3 1 40.03 1.81 2.2525 -2 0 3 1 40.38 1.50 2.2339 -2 1 3 1 40.80 7.26 2.2118 0 2 4 1 40.99 1.18 2.2017 -3 -1 1 1 41.24 1.79 2.1890 1 3 3 1 41.33 3.14 2.1843 -1 1 4 1 41.53 2.00 2.1744 3 -1 2 1 41.57 5.73 2.1723 -1 0 4 1 41.62 4.04 2.1699 2 1 4 1 41.74 1.34 2.1642 0 -1 4 1 41.84 3.95 2.1591 3 2 1 1 41.98 1.94 2.1524 1 -1 4 1 42.02 3.62 2.1504 2 3 2 1 42.07 2.74 2.1479 -2 -2 2 1 42.08 1.78 2.1475 2 0 4 1 42.19 6.05 2.1420 2 3 0 1 42.73 2.74 2.1160 0 -3 2 1 42.88 2.70 2.1092 -1 -2 3 1 42.95 5.57 2.1057 3 2 2 1 42.96 4.54 2.1052 3 2 0 1 42.97 4.38 2.1049 3 1 3 1 42.99 7.91 2.1038 3 0 3 1 43.10 4.32 2.0987 -2 -1 3 1 43.50 3.90 2.0806 -2 3 1 1 43.64 4.88 2.0739 -3 0 2 1 43.80 1.93 2.0668 -3 2 0 1 43.92 1.42 2.0613 1 -3 2 1 44.08 1.06 2.0545 -2 2 3 1 44.15 2.79 2.0511 -1 3 3 1 44.43 1.07 2.0391 -1 2 4 1 44.49 3.96 2.0362 2 2 4 1 44.52 2.32 2.0353 -3 1 2 1 44.63 5.98 2.0302 3 -2 1 1 44.76 2.20 2.0246 2 -3 1 1 44.99 5.40 2.0149 2 -2 3 1 45.12 1.19 2.0095 -1 -3 2 1 45.13 7.49 2.0091 -3 2 1 1 45.54 1.11 1.9920 -2 -3 1 1 45.78 1.79 1.9822 2 -1 4 1 46.04 15.08 1.9714 0 4 1 1 46.19 6.95 1.9652 -3 -2 1 1 46.24 1.43 1.9634 3 -1 3 1 46.84 3.72 1.9394 0 4 0 1 47.03 2.21 1.9322 0 3 4 1 47.09 5.75 1.9299 1 4 1 1 47.14 2.66 1.9281 0 1 5 1 47.53 1.80 1.9129 3 -2 2 1 48.26 1.40 1.8858 1 4 0 1 48.37 2.94 1.8818 -1 4 1 1 48.43 11.42 1.8797 0 -2 4 1 48.47 2.47 1.8780 -3 2 2 1 48.61 7.98 1.8730 4 0 1 1 48.70 4.60 1.8697 1 -2 4 1 49.08 3.79 1.8562 -2 -2 3 1 49.09 6.21 1.8557 1 2 5 1 49.10 4.92 1.8554 4 0 0 1 49.16 1.88 1.8534 3 0 4 1 49.41 1.41 1.8445 4 1 1 1 49.44 6.16 1.8434 0 2 5 1 49.86 1.18 1.8290 2 1 5 1 49.98 4.69 1.8249 -3 0 3 1 50.24 1.21 1.8161 2 3 4 1 50.33 1.21 1.8129 -3 1 3 1 50.33 1.70 1.8128 4 1 0 1 50.36 1.70 1.8118 -1 3 4 1 50.71 1.67 1.8004 -1 1 5 1 50.79 1.77 1.7978 4 -1 1 1 50.83 1.71 1.7962 -4 1 0 1 51.09 5.73 1.7877 -2 2 4 1 51.19 1.10 1.7845 3 2 4 1 51.34 4.06 1.7796 -1 0 5 1 51.36 3.06 1.7789 2 4 1 1 51.55 1.24 1.7730 0 -1 5 1 51.83 2.71 1.7641 2 4 2 1 51.87 1.10 1.7626 -1 -3 3 1 51.95 5.99 1.7601 2 2 5 1 52.14 2.74 1.7543 3 3 3 1 52.18 5.72 1.7530 2 -2 4 1 52.80 1.74 1.7339 -4 1 1 1 52.82 2.48 1.7333 2 4 0 1 53.15 1.20 1.7231 -4 -1 1 1 53.42 1.29 1.7150 -1 4 3 1 53.48 2.24 1.7134 4 0 3 1 53.68 2.60 1.7076 4 2 2 1 53.75 4.26 1.7054 -2 4 1 1 53.78 2.08 1.7046 -2 4 0 1 53.83 1.86 1.7030 -3 -3 1 1 54.23 4.98 1.6916 0 -4 2 1 54.34 1.30 1.6882 2 -1 5 1 54.38 2.28 1.6871 4 2 0 1 54.50 1.76 1.6836 0 3 5 1 54.79 1.29 1.6755 -1 -1 5 1 55.01 1.43 1.6692 -3 3 2 1 55.29 4.17 1.6616 1 -4 2 1 55.38 6.94 1.6590 1 4 4 1 55.48 1.68 1.6563 0 4 4 1 55.57 1.13 1.6537 -2 4 2 1 55.65 1.33 1.6516 2 -4 1 1 55.75 3.47 1.6488 -4 0 2 1 55.79 1.58 1.6477 3 -3 2 1 56.08 2.23 1.6399 -2 -4 1 1 56.09 1.87 1.6396 4 2 3 1 56.18 2.40 1.6372 -1 -4 2 1 56.56 1.03 1.6271 -2 3 4 1 56.62 2.05 1.6256 3 0 5 1 56.64 1.50 1.6252 1 1 6 1 56.78 2.15 1.6214 -4 2 1 1 57.22 2.49 1.6099 -2 -2 4 1 57.29 1.44 1.6082 -2 -3 3 1 57.46 1.26 1.6039 -4 -2 1 1 57.63 1.24 1.5995 -2 0 5 1 57.72 1.52 1.5972 -3 -2 3 1 57.73 5.51 1.5968 1 0 6 1 57.84 2.63 1.5941 4 -2 2 1 58.24 1.08 1.5842 2 4 4 1 58.27 1.17 1.5835 0 0 6 1 58.45 1.56 1.5790 3 -2 4 1 58.52 2.55 1.5772 -1 4 4 1 59.13 1.26 1.5624 -2 4 3 1 59.24 2.08 1.5598 -2 2 5 1 59.26 2.15 1.5594 2 -4 2 1 59.43 1.00 1.5553 4 3 2 1 59.97 1.18 1.5425 -4 2 2 1 60.07 1.90 1.5401 -3 2 4 1 60.10 1.51 1.5396 2 0 6 1 60.46 1.13 1.5311 2 2 6 1 60.98 1.47 1.5195 1 -4 3 1 61.43 1.31 1.5093 1 -1 6 1 61.85 1.11 1.5002 5 0 1 1 63.02 1.35 1.4750 2 5 2 1 63.80 1.04 1.4589 -1 -5 1 1 63.80 1.51 1.4588 3 4 4 1 64.23 1.70 1.4502 -1 5 3 1 65.10 1.50 1.4328 -1 -1 6 1 65.16 1.66 1.4317 3 0 6 1 65.32 1.17 1.4285 5 1 3 1 65.44 1.27 1.4262 5 0 3 1 65.45 1.32 1.4260 -3 -2 4 1 65.81 4.20 1.4191 4 2 5 1 65.81 1.45 1.4191 3 -4 2 1 66.24 3.33 1.4110 -3 0 5 1 66.72 1.09 1.4018 0 -5 2 1 67.04 2.30 1.3961 4 -2 4 1 67.05 2.57 1.3957 5 2 0 1 67.23 1.97 1.3926 -3 4 3 1 67.55 2.90 1.3868 4 4 1 1 67.67 1.10 1.3846 5 2 3 1 68.11 1.25 1.3766 5 -2 1 1 68.22 1.93 1.3746 -3 -4 2 1 68.29 2.67 1.3735 -4 -2 3 1 68.98 1.29 1.3614 -5 0 2 1 69.22 1.20 1.3572 4 -3 3 1 69.64 1.95 1.3502 5 0 4 1 69.69 2.49 1.3492 -5 2 1 1 69.75 1.25 1.3483 5 -2 2 1 70.00 2.06 1.3440 -1 -4 4 1 70.94 2.56 1.3285 -4 2 4 1 71.02 2.17 1.3273 -4 4 0 1 71.59 1.15 1.3181 -4 4 1 1 71.74 1.36 1.3157 4 4 4 1 72.33 1.04 1.3064 -3 4 4 1 72.55 1.15 1.3030 -1 2 7 1 72.63 1.25 1.3017 4 0 6 1 72.79 1.40 1.2993 -4 -4 1 1 72.80 1.27 1.2991 -1 4 6 1 73.20 1.14 1.2929 0 6 0 1 74.00 1.62 1.2809 0 6 3 1 74.11 1.47 1.2793 1 6 3 1 74.19 1.79 1.2781 1 6 0 1 74.43 1.01 1.2746 -5 0 3 1 74.79 2.07 1.2694 -1 6 0 1 75.73 1.15 1.2560 -4 -2 4 1 76.15 1.43 1.2501 6 0 1 1 76.25 1.62 1.2486 1 -4 5 1 77.11 1.09 1.2369 6 0 0 1 77.38 1.05 1.2332 1 4 7 1 77.41 1.22 1.2328 -4 4 3 1 78.16 1.73 1.2229 1 -2 7 1 78.46 1.05 1.2190 -4 2 5 1 78.97 1.08 1.2124 2 4 7 1 78.98 1.65 1.2122 1 2 8 1 80.95 1.19 1.1876 0 0 8 1 83.84 1.36 1.1539 3 -4 5 1 84.38 1.19 1.1478 3 -2 7 1 86.25 1.25 1.1277 0 -6 3 1 86.71 1.16 1.1230 -3 4 6 1 89.51 1.09 1.0950 -5 0 5 1 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.