Alfredstelznerite Cooper M A, Hawthorne F C, Galliski M A, Marquez-Zavalia M F The Canadian Mineralogist 48 (2010) 129-138 The crystal structure of alfredstelznerite, Ca4(H2O)4[B4O4(OH)6]4(H2O)15, a complex hydroxy-hydrated calcium borate mineral Locality: Santa Rosa mine, Sijes, Salta, Argentina _database_code_amcsd 0006321 CELL PARAMETERS: 12.1610 40.4770 10.1843 90.000 90.000 90.000 SPACE GROUP: Pca2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 5013.128 Density (g/cm3): 1.797 MAX. ABS. INTENSITY / VOLUME**2: 5.395070432 RIR: 0.977 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 2.18 23.72 40.4770 0 1 0 2 6.55 10.22 13.4923 0 3 0 2 7.59 4.08 11.6467 1 1 0 4 8.48 11.28 10.4239 1 2 0 4 8.74 100.00 10.1193 0 4 0 2 9.79 5.37 9.0332 1 3 0 4 10.93 2.39 8.0954 0 5 0 2 11.38 7.99 7.7785 1 4 0 4 12.15 3.74 7.2846 1 2 1 4 13.10 6.84 6.7579 1 3 1 4 13.14 21.86 6.7388 1 5 0 4 14.33 4.55 6.1817 1 4 1 4 14.57 5.17 6.0805 2 0 0 2 15.02 4.43 5.8993 1 6 0 4 15.77 4.94 5.6199 1 5 1 4 16.98 20.16 5.2208 2 0 1 2 17.01 1.72 5.2120 2 4 0 4 17.37 1.50 5.1047 1 6 1 4 17.42 3.16 5.0922 0 0 2 1 17.96 1.57 4.9382 0 2 2 2 19.00 1.44 4.6714 1 8 0 4 19.02 1.23 4.6657 1 1 2 4 19.13 10.49 4.6397 2 4 1 4 19.40 3.27 4.5754 1 2 2 4 19.52 4.78 4.5487 0 4 2 2 20.02 1.78 4.4359 1 3 2 4 20.24 2.47 4.3875 2 5 1 4 21.06 3.19 4.2182 1 9 0 4 21.52 14.10 4.1288 2 6 1 4 22.78 4.09 3.9040 2 0 2 2 22.95 3.41 3.8750 2 7 1 4 23.20 10.80 3.8333 2 2 2 4 24.03 2.08 3.7027 3 2 1 4 24.19 3.10 3.6797 0 11 0 2 24.44 5.38 3.6423 2 4 2 4 24.56 1.34 3.6246 3 5 0 4 24.81 3.95 3.5891 0 8 2 2 25.64 1.24 3.4746 3 6 0 4 26.15 2.87 3.4074 2 9 1 4 26.38 5.42 3.3790 2 6 2 4 26.42 5.05 3.3731 0 12 0 2 26.44 2.14 3.3709 0 9 2 2 26.78 4.80 3.3286 1 11 1 4 27.57 2.98 3.2356 2 7 2 4 27.63 2.02 3.2279 1 2 3 4 27.89 1.86 3.1989 2 10 1 4 28.08 7.48 3.1778 1 3 3 4 28.22 3.70 3.1618 3 1 2 4 28.49 7.25 3.1332 3 2 2 4 28.67 2.22 3.1136 0 13 0 2 28.69 4.36 3.1114 1 4 3 4 28.83 1.01 3.0965 1 12 1 4 28.89 5.74 3.0908 2 8 2 4 28.92 8.31 3.0873 3 3 2 4 29.52 1.70 3.0263 3 4 2 4 29.62 17.28 3.0163 1 13 0 4 29.70 4.12 3.0077 2 11 1 4 30.15 4.59 2.9641 2 0 3 2 30.23 2.42 2.9562 2 1 3 4 30.27 2.50 2.9529 3 5 2 4 30.30 2.47 2.9496 2 12 0 4 30.71 2.73 2.9117 4 4 0 4 30.89 2.89 2.8951 2 3 3 4 30.92 9.43 2.8921 1 13 1 4 31.01 2.05 2.8835 4 2 1 4 31.45 11.95 2.8446 2 4 3 4 31.58 3.47 2.8332 2 12 1 4 31.85 1.33 2.8100 2 10 2 4 32.19 1.04 2.7807 3 7 2 4 32.30 1.81 2.7714 2 13 0 4 33.51 1.25 2.6745 4 6 1 4 33.51 2.18 2.6742 2 13 1 4 33.99 1.65 2.6377 2 7 3 4 34.35 15.85 2.6104 4 0 2 2 34.41 1.80 2.6060 4 8 0 4 34.75 1.86 2.5814 3 2 3 4 35.09 2.03 2.5575 2 8 3 4 35.12 3.59 2.5555 3 3 3 4 35.25 6.66 2.5461 0 0 4 1 35.49 2.10 2.5293 2 14 1 4 35.52 6.47 2.5276 4 4 2 4 35.62 1.71 2.5206 3 4 3 4 36.39 1.88 2.4691 0 4 4 2 36.76 1.05 2.4451 4 9 1 4 37.44 5.43 2.4023 3 11 2 4 37.48 5.32 2.3997 3 13 1 4 37.52 2.01 2.3972 2 15 1 4 38.06 2.33 2.3645 4 10 1 4 38.33 3.46 2.3485 2 0 4 2 38.47 6.62 2.3398 1 15 2 4 38.53 1.10 2.3366 1 17 0 4 39.39 1.70 2.2877 2 4 4 4 39.45 1.09 2.2841 4 11 1 4 39.57 3.55 2.2775 1 17 1 4 39.59 1.88 2.2766 2 16 1 4 39.80 1.45 2.2648 4 0 3 2 39.98 3.19 2.2548 1 13 3 4 40.60 1.35 2.2218 3 13 2 4 40.83 2.21 2.2101 4 4 3 4 41.23 1.22 2.1895 5 7 1 4 41.38 2.01 2.1819 5 2 2 4 42.24 1.79 2.1394 5 9 0 4 42.50 1.53 2.1273 4 13 1 4 42.55 2.75 2.1249 3 11 3 4 42.57 3.84 2.1237 1 17 2 4 43.43 1.58 2.0834 3 5 4 4 43.79 2.63 2.0671 4 8 3 4 43.88 3.02 2.0634 1 11 4 4 44.10 1.41 2.0537 3 6 4 4 44.11 3.46 2.0530 3 17 0 4 44.13 1.27 2.0521 4 14 1 4 44.71 2.55 2.0268 6 0 0 2 44.87 3.22 2.0202 3 7 4 4 44.91 1.23 2.0182 4 15 0 4 45.42 2.70 1.9969 3 13 3 4 45.64 1.70 1.9878 6 0 1 2 45.65 1.06 1.9874 6 4 0 4 45.87 1.25 1.9783 6 2 1 4 46.02 4.66 1.9724 5 9 2 4 46.52 2.24 1.9520 4 0 4 2 46.56 9.96 1.9506 6 4 1 4 46.69 5.65 1.9456 1 13 4 4 47.05 4.63 1.9314 2 0 5 2 47.22 3.84 1.9248 1 17 3 4 47.43 3.33 1.9167 4 4 4 4 47.77 4.69 1.9041 3 17 2 4 47.95 1.24 1.8971 2 4 5 4 48.32 2.05 1.8837 5 13 1 4 48.40 1.35 1.8807 0 20 2 2 48.56 1.03 1.8750 2 13 4 4 48.66 1.42 1.8713 1 21 1 4 49.06 1.54 1.8568 2 6 5 4 50.90 1.61 1.7939 5 13 2 4 51.18 1.31 1.7849 1 19 3 4 51.23 2.43 1.7832 1 21 2 4 52.06 1.73 1.7568 3 17 3 4 52.59 1.02 1.7403 6 0 3 2 52.75 1.85 1.7353 2 22 1 4 53.30 1.23 1.7186 5 5 4 4 54.69 2.91 1.6782 5 17 1 4 54.84 1.22 1.6740 0 4 6 2 61.48 1.61 1.5082 2 26 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.