U8Cs2Se4Ni3O48(H2O)4 Wylie E M, Burns P C The Canadian Mineralogist 50 (2012) 147-157 Crystal structures of six new uranyl selenate and selenite compounds and their relationship with uranyl mineral structures Note: Compound 1 Locality: synthetic _database_code_amcsd 0019085 CELL PARAMETERS: 8.7550 14.2280 17.9270 90.000 103.739 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2169.203 Density (g/cm3): 5.374 MAX. ABS. INTENSITY / VOLUME**2: 129.8632063 RIR: 7.868 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.16 12.19 8.7070 0 0 2 2 12.15 2.36 7.2824 -1 1 1 4 12.44 100.00 7.1140 0 2 0 2 16.09 16.33 5.5090 0 2 2 4 20.40 1.98 4.3535 0 0 4 2 20.89 7.87 4.2522 2 0 0 2 20.96 6.75 4.2384 -2 0 2 2 22.63 13.29 3.9287 1 3 1 4 23.96 5.38 3.7134 0 2 4 4 24.45 1.61 3.6412 -2 2 2 4 24.92 2.06 3.5728 -1 3 3 4 25.03 40.60 3.5570 0 4 0 2 25.40 30.25 3.5066 2 0 2 2 25.57 24.79 3.4835 -2 0 4 2 27.08 2.24 3.2928 0 4 2 4 28.38 46.20 3.1453 2 2 2 4 28.53 53.73 3.1286 -2 2 4 4 30.81 24.51 2.9023 0 0 6 2 31.59 4.59 2.8320 -1 3 5 4 32.75 2.81 2.7346 2 0 4 2 32.83 2.86 2.7283 2 4 0 4 32.87 1.91 2.7247 -2 4 2 4 32.98 1.16 2.7163 -2 0 6 2 33.21 1.17 2.6977 -1 5 1 4 33.34 18.64 2.6873 0 2 6 4 34.00 4.54 2.6368 1 5 1 4 35.68 1.54 2.5166 -1 1 7 4 35.96 10.15 2.4972 2 4 2 4 36.09 10.28 2.4888 -2 4 4 4 37.94 2.23 2.3713 0 6 0 2 39.05 1.15 2.3068 3 1 3 4 39.38 2.90 2.2880 0 6 2 4 40.10 17.80 2.2487 0 4 6 4 40.67 2.24 2.2183 -3 3 5 4 40.73 1.61 2.2155 -1 5 5 4 41.25 11.93 2.1887 -4 0 2 2 41.63 1.59 2.1693 2 0 6 2 41.66 1.82 2.1680 2 4 4 4 41.89 2.15 2.1565 -2 0 8 2 42.52 1.40 2.1261 4 0 0 2 42.66 1.07 2.1192 -4 0 4 2 43.14 1.66 2.0969 3 3 3 4 43.25 10.14 2.0919 -4 2 2 4 43.48 4.73 2.0815 0 2 8 4 44.47 2.68 2.0371 4 2 0 4 44.60 1.87 2.0315 1 3 7 4 44.61 1.96 2.0310 -4 2 4 4 45.22 3.01 2.0050 -3 5 3 4 46.21 7.11 1.9643 2 6 2 4 46.32 9.20 1.9602 -2 6 4 4 46.52 6.96 1.9522 1 7 1 4 47.78 1.59 1.9037 -1 7 3 4 48.86 9.96 1.8641 -4 4 2 4 49.42 1.57 1.8441 -2 4 8 4 49.65 4.85 1.8363 0 6 6 4 50.53 3.58 1.8063 3 5 3 4 51.38 3.57 1.7785 0 8 0 2 51.51 3.13 1.7742 2 0 8 2 51.79 3.76 1.7652 -2 0 10 2 51.83 1.91 1.7640 1 5 7 4 51.91 5.89 1.7615 -1 7 5 4 52.17 6.66 1.7533 4 0 4 2 52.54 5.41 1.7417 -4 0 8 2 53.21 9.58 1.7215 2 2 8 4 53.48 8.52 1.7133 -2 2 10 4 53.85 5.30 1.7024 4 2 4 4 54.22 5.91 1.6918 -4 2 8 4 55.71 3.45 1.6500 -3 7 3 4 56.53 1.69 1.6278 -5 3 1 4 57.28 3.70 1.6083 -4 6 2 4 57.47 1.12 1.6036 0 6 8 4 58.10 3.53 1.5877 2 4 8 4 58.16 2.08 1.5862 2 8 2 4 58.25 1.47 1.5840 -2 8 4 4 58.36 4.40 1.5812 -2 4 10 4 58.71 5.31 1.5726 4 4 4 4 59.05 5.36 1.5643 -4 4 8 4 59.98 3.26 1.5422 1 9 1 4 60.34 2.46 1.5339 3 7 3 4 60.61 1.73 1.5278 -3 5 9 4 61.11 3.25 1.5164 0 8 6 4 61.47 1.06 1.5085 -5 3 7 4 61.50 2.89 1.5077 1 7 7 4 64.18 2.10 1.4512 0 0 12 2 64.59 2.79 1.4428 -1 9 5 4 65.66 2.45 1.4219 0 2 12 4 65.73 3.93 1.4206 2 6 8 4 65.90 2.08 1.4174 6 0 0 2 65.97 3.18 1.4160 -2 6 10 4 66.14 2.08 1.4128 -6 0 6 2 66.14 1.13 1.4127 -1 5 11 4 66.30 1.45 1.4098 4 6 4 4 66.62 1.86 1.4038 -4 6 8 4 67.36 3.25 1.3901 6 2 0 4 67.60 2.69 1.3857 -6 2 6 4 67.91 2.74 1.3803 -4 8 2 4 67.94 3.09 1.3796 -3 9 3 4 70.02 3.24 1.3437 0 4 12 4 71.54 2.85 1.3188 -5 7 1 4 71.67 2.02 1.3167 6 4 0 4 71.91 2.31 1.3130 -6 4 6 4 72.13 2.46 1.3096 3 9 3 4 73.19 1.96 1.2932 1 9 7 4 74.61 2.24 1.2720 1 11 1 4 74.72 1.39 1.2704 -1 7 11 4 75.95 1.79 1.2529 -5 7 7 4 76.26 1.53 1.2486 4 8 4 4 76.56 1.27 1.2444 -4 8 8 4 77.04 1.18 1.2378 0 6 12 4 78.64 1.44 1.2166 6 6 0 4 78.80 2.51 1.2145 -1 11 5 4 78.86 1.25 1.2137 -6 6 6 4 78.90 1.19 1.2133 4 0 10 2 79.50 1.00 1.2057 -4 0 14 2 80.26 1.82 1.1961 4 2 10 4 80.68 2.00 1.1909 -3 9 9 4 80.86 2.14 1.1887 -4 2 14 4 81.91 1.67 1.1761 -3 11 3 4 82.53 1.27 1.1689 6 0 6 2 82.61 1.08 1.1680 -5 9 1 4 83.20 1.07 1.1612 -6 0 12 2 83.79 1.10 1.1544 5 7 5 4 83.88 2.17 1.1534 6 2 6 4 84.34 1.67 1.1484 4 4 10 4 84.55 2.14 1.1460 -6 2 12 4 84.93 1.44 1.1418 -4 4 14 4 85.66 1.33 1.1340 -1 9 11 4 85.87 1.23 1.1318 3 11 3 4 86.85 1.12 1.1215 -5 9 7 4 86.88 1.58 1.1211 1 11 7 4 87.93 1.37 1.1105 6 4 6 4 87.95 2.28 1.1103 2 2 14 4 88.60 1.47 1.1038 -6 4 12 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.