Harmotome Stuckenschmidt E, Fuess H, Kvick A European Journal of Mineralogy 2 (1990) 861-874 Investigation of the structure of harmotome by X-ray (293 K, 100 K) and neutron diffraction (15 K) Sample: 15 K _database_code_amcsd 0006411 CELL PARAMETERS: 9.8840 14.1000 8.6550 90.000 124.590 90.000 SPACE GROUP: P2_1/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 992.986 Density (g/cm3): 2.367 MAX. ABS. INTENSITY / VOLUME**2: 7.604735850 RIR: 1.046 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.87 54.61 8.1369 1 0 0 2 10.91 75.58 8.1064 -1 0 1 2 12.42 77.82 7.1251 0 0 1 2 12.56 13.26 7.0475 1 1 0 4 12.60 7.96 7.0277 -1 1 1 4 13.93 100.00 6.3593 0 1 1 4 16.67 1.09 5.3197 -1 2 1 4 17.70 34.19 5.0114 0 2 1 4 20.71 19.58 4.2880 1 0 1 2 20.78 8.94 4.2746 -1 0 2 2 21.66 11.67 4.1025 1 1 1 4 21.73 26.65 4.0908 -1 1 2 4 21.84 35.14 4.0698 1 3 0 4 21.86 10.87 4.0660 -1 3 1 4 21.96 42.25 4.0467 -2 2 1 4 22.66 3.82 3.9233 0 3 1 4 22.75 9.71 3.9090 2 1 0 4 22.83 19.78 3.8954 -2 1 2 4 24.29 3.78 3.6636 1 2 1 4 24.35 4.04 3.6552 -1 2 2 4 24.99 3.47 3.5626 0 0 2 2 25.27 3.63 3.5250 0 4 0 2 25.27 2.79 3.5238 2 2 0 4 25.79 12.73 3.4540 0 1 2 4 26.17 5.52 3.4057 -2 3 1 4 27.58 16.86 3.2345 1 4 0 4 27.59 29.95 3.2326 -1 4 1 4 27.77 14.08 3.2128 -3 0 1 2 28.06 6.63 3.1796 0 2 2 4 28.17 2.88 3.1677 1 3 1 4 28.25 35.30 3.1595 0 4 1 4 28.49 44.67 3.1325 -3 1 1 4 28.54 43.75 3.1273 -3 1 2 4 29.03 11.56 3.0761 2 3 0 4 29.09 15.44 3.0695 -2 3 2 4 30.58 4.64 2.9235 -3 2 1 4 30.62 23.17 2.9193 -3 2 2 4 30.88 6.67 2.8954 2 0 1 2 31.00 1.13 2.8845 -2 0 3 2 31.17 3.07 2.8698 -2 4 1 4 31.51 7.57 2.8391 0 3 2 4 31.54 3.07 2.8363 2 1 1 4 31.66 1.12 2.8259 -2 1 3 4 32.67 4.99 2.7414 1 0 2 2 32.74 7.82 2.7356 -1 0 3 2 32.89 20.99 2.7230 1 4 1 4 32.93 17.28 2.7196 -1 4 2 4 33.29 12.73 2.6910 1 1 2 4 33.37 25.29 2.6855 -1 1 3 4 33.46 11.02 2.6784 2 2 1 4 33.57 12.49 2.6696 -2 2 3 4 33.64 16.60 2.6645 1 5 0 4 33.64 8.54 2.6641 2 4 0 4 33.65 5.13 2.6635 3 1 0 4 33.65 13.27 2.6634 -1 5 1 4 33.79 1.24 2.6523 -3 3 1 4 34.20 10.85 2.6221 0 5 1 4 35.12 3.55 2.5550 1 2 2 4 35.19 3.04 2.5503 -1 2 3 4 35.46 17.87 2.5314 3 2 0 4 35.58 10.54 2.5231 -3 2 3 4 35.84 9.75 2.5057 0 4 2 4 36.36 2.61 2.4710 -4 0 2 2 36.45 8.37 2.4652 2 3 1 4 36.93 2.82 2.4339 -4 1 2 4 37.88 4.00 2.3750 0 0 3 2 38.00 5.26 2.3680 1 3 2 4 38.06 8.94 2.3642 -1 3 3 4 38.23 5.06 2.3539 -1 5 2 4 38.30 2.54 2.3500 0 6 0 2 38.43 8.86 2.3426 -3 3 3 4 38.44 1.59 2.3420 0 1 3 4 38.51 2.35 2.3375 -4 0 1 2 38.61 3.45 2.3319 -4 2 2 4 38.61 1.65 2.3317 -4 0 3 2 38.86 5.84 2.3177 2 5 0 4 38.91 12.83 2.3148 -2 5 2 4 39.06 3.55 2.3060 -4 1 1 4 39.16 10.48 2.3004 -4 1 3 4 39.94 3.80 2.2571 -1 6 1 4 40.06 4.48 2.2507 0 2 3 4 40.31 4.08 2.2374 2 4 1 4 40.41 5.99 2.2323 -2 4 3 4 40.66 4.37 2.2187 -4 2 1 4 42.03 13.34 2.1496 3 4 0 4 42.14 5.90 2.1445 -3 4 3 4 42.15 1.89 2.1440 2 0 2 2 42.60 2.79 2.1223 -2 6 1 4 42.79 1.53 2.1132 -2 1 4 4 43.32 2.26 2.0888 -4 3 3 4 43.94 4.58 2.0608 1 6 1 4 43.97 6.43 2.0593 -1 6 2 4 44.01 2.64 2.0575 -3 2 4 4 44.15 8.89 2.0513 2 2 2 4 44.28 4.42 2.0454 -2 2 4 4 44.72 4.93 2.0266 -4 0 4 2 44.79 1.17 2.0234 -4 4 2 4 44.87 3.85 2.0202 2 5 1 4 44.95 1.81 2.0164 -2 5 3 4 45.03 5.89 2.0134 4 1 0 4 45.45 3.35 1.9955 1 0 3 2 45.53 3.55 1.9923 -1 0 4 2 46.01 1.70 1.9727 -1 1 4 4 46.24 2.53 1.9635 -1 5 3 4 46.26 3.51 1.9625 3 3 1 4 46.28 2.76 1.9617 0 6 2 4 46.40 4.22 1.9570 -5 0 3 2 46.42 1.11 1.9560 -3 3 4 4 46.44 1.47 1.9553 1 7 0 4 46.45 1.35 1.9548 3 5 0 4 46.46 3.01 1.9545 4 2 0 4 46.55 2.07 1.9510 -3 5 3 4 46.62 2.26 1.9481 -4 4 1 4 46.63 8.62 1.9477 -4 2 4 4 46.69 2.24 1.9456 -2 3 4 4 46.82 2.14 1.9405 -5 1 2 4 47.35 2.17 1.9200 1 2 3 4 47.42 4.23 1.9172 -1 2 4 4 47.96 1.30 1.8968 -3 6 1 4 47.99 2.63 1.8956 -3 6 2 4 49.49 2.43 1.8416 3 4 1 4 49.63 1.25 1.8368 1 3 3 4 49.78 1.78 1.8318 2 4 2 4 49.90 1.56 1.8277 -5 0 1 2 49.90 1.42 1.8276 -2 4 4 4 50.07 1.92 1.8219 -2 6 3 4 50.22 5.81 1.8166 0 5 3 4 50.47 1.65 1.8083 -5 3 2 4 50.49 2.49 1.8074 -5 1 4 4 50.56 2.22 1.8052 2 7 0 4 50.60 1.32 1.8038 -2 7 2 4 50.73 1.81 1.7996 -4 5 1 4 50.81 2.39 1.7970 -4 5 3 4 51.20 1.57 1.7842 1 6 2 4 51.29 1.81 1.7813 0 0 4 2 51.45 3.02 1.7761 3 6 0 4 51.54 1.23 1.7732 -3 6 3 4 51.88 8.39 1.7625 0 8 0 2 51.90 1.39 1.7619 4 4 0 4 52.17 2.97 1.7534 0 7 2 4 53.18 1.41 1.7223 -1 8 1 4 53.40 3.92 1.7158 4 0 1 2 53.44 5.49 1.7147 3 5 1 4 53.56 4.72 1.7110 -5 4 3 4 53.56 2.27 1.7109 0 8 1 4 53.58 4.39 1.7104 -3 5 4 4 53.63 3.86 1.7089 -4 0 5 2 53.71 3.50 1.7066 -3 7 1 4 53.74 3.27 1.7058 -3 7 2 4 53.82 1.63 1.7034 -2 5 4 4 53.84 4.63 1.7029 -4 6 2 4 54.06 3.14 1.6965 -4 1 5 4 54.47 1.16 1.6847 3 2 2 4 54.67 2.43 1.6790 -3 2 5 4 54.70 1.47 1.6779 2 0 3 2 54.97 7.52 1.6705 0 6 3 4 55.12 1.48 1.6661 2 1 3 4 55.14 5.10 1.6657 0 3 4 4 55.27 1.18 1.6619 -2 1 5 4 55.44 3.78 1.6573 -4 6 1 4 55.58 1.45 1.6535 2 7 1 4 55.72 1.83 1.6498 4 5 0 4 55.81 7.60 1.6473 -6 0 3 2 56.22 2.45 1.6362 -6 1 3 4 56.51 1.27 1.6284 -2 2 5 4 56.54 1.05 1.6276 3 3 2 4 56.71 1.88 1.6232 1 7 2 4 56.74 1.04 1.6225 -5 4 1 4 56.76 1.93 1.6220 -1 7 3 4 56.88 1.06 1.6189 -5 4 4 4 56.94 1.73 1.6173 2 8 0 4 56.96 2.97 1.6166 5 1 0 4 57.03 1.38 1.6150 -3 7 3 4 57.26 2.76 1.6089 -5 5 2 4 57.36 2.13 1.6064 -6 0 2 2 57.87 1.56 1.5933 -6 1 4 4 58.01 1.15 1.5898 0 4 4 4 58.14 2.42 1.5868 -3 6 4 4 58.18 1.05 1.5857 5 2 0 4 58.40 2.94 1.5802 2 3 3 4 58.55 1.75 1.5766 -2 3 5 4 58.97 1.91 1.5663 -6 2 2 4 59.56 2.68 1.5521 -3 4 5 4 60.16 1.36 1.5382 -1 9 1 4 60.31 2.79 1.5347 -4 6 4 4 60.40 3.02 1.5327 -5 3 5 4 60.48 3.21 1.5306 -5 5 4 4 60.51 4.40 1.5301 0 9 1 4 60.63 2.80 1.5273 1 2 4 4 60.71 1.45 1.5254 -1 2 5 4 60.76 5.20 1.5243 -4 7 3 4 60.95 1.13 1.5201 -6 3 2 4 60.97 1.36 1.5197 -1 6 4 4 61.60 1.43 1.5055 2 8 1 4 61.68 1.45 1.5038 -5 6 3 4 62.58 1.39 1.4843 1 3 4 4 62.89 3.70 1.4777 3 5 2 4 62.90 1.04 1.4775 5 4 0 4 63.08 1.46 1.4738 -3 5 5 4 63.11 1.60 1.4731 3 7 1 4 63.19 1.52 1.4715 1 9 1 4 63.21 1.37 1.4710 -1 9 2 4 63.51 1.60 1.4648 -6 2 1 4 63.76 2.68 1.4596 -6 4 4 4 64.60 2.42 1.4427 -5 6 1 4 64.73 1.62 1.4401 4 1 2 4 64.78 1.79 1.4392 -2 5 5 4 65.00 2.67 1.4347 -4 1 6 4 65.18 1.55 1.4313 4 7 0 4 65.41 1.93 1.4268 -6 3 1 4 65.89 2.26 1.4177 -3 1 6 4 66.08 2.02 1.4139 5 1 1 4 66.29 1.66 1.4100 0 10 0 2 66.39 2.34 1.4082 -3 9 1 4 67.00 3.33 1.3968 0 2 5 4 67.05 1.19 1.3958 -6 5 2 4 67.23 1.05 1.3925 -3 6 5 4 67.75 1.16 1.3832 0 10 1 4 68.02 1.74 1.3783 -6 4 1 4 68.22 4.57 1.3747 -6 4 5 4 68.68 1.87 1.3667 -1 5 5 4 68.88 1.21 1.3632 -2 6 5 4 68.97 3.27 1.3615 2 8 2 4 69.05 1.89 1.3602 1 9 2 4 69.09 3.63 1.3595 -1 9 3 4 69.26 2.12 1.3566 3 9 0 4 69.30 1.42 1.3559 -2 10 1 4 69.84 1.94 1.3467 -7 3 3 4 69.90 1.18 1.3458 -7 1 5 4 70.56 1.02 1.3348 -4 4 6 4 70.58 1.68 1.3344 0 7 4 4 70.74 1.80 1.3317 6 2 0 4 70.86 1.32 1.3299 -4 8 4 4 71.18 5.12 1.3246 3 4 3 4 71.40 3.11 1.3210 -3 4 6 4 71.41 1.92 1.3210 1 8 3 4 71.46 1.09 1.3201 -1 8 4 4 71.50 1.08 1.3194 -6 5 5 4 72.43 2.74 1.3048 -7 4 4 4 72.54 1.21 1.3031 -4 7 5 4 72.60 1.79 1.3022 1 6 4 4 72.62 1.85 1.3019 -7 3 2 4 72.84 1.55 1.2985 -6 3 6 4 73.35 1.40 1.2908 -3 10 2 4 73.54 1.39 1.2879 4 5 2 4 74.24 3.43 1.2775 2 4 4 4 74.40 2.78 1.2751 -2 4 6 4 74.91 1.46 1.2677 2 10 1 4 74.97 1.45 1.2668 -2 10 3 4 75.05 1.39 1.2657 6 4 0 4 75.11 1.53 1.2647 -7 4 2 4 75.22 2.00 1.2632 -7 0 6 2 75.24 1.24 1.2630 -5 7 5 4 75.28 1.29 1.2623 -7 4 5 4 75.58 1.87 1.2580 -7 -5 3 4 76.08 1.17 1.2510 3 10 0 4 76.15 1.12 1.2500 -3 10 3 4 76.35 2.30 1.2473 -7 2 1 4 76.91 1.00 1.2396 1 3 5 4 77.00 1.50 1.2385 -1 3 6 4 77.21 1.42 1.2355 1 7 4 4 77.67 1.30 1.2294 4 8 1 4 77.86 2.03 1.2269 -4 8 5 4 78.22 1.35 1.2222 -2 11 2 4 78.50 1.58 1.2185 0 6 5 4 78.50 2.27 1.2184 -6 5 6 4 79.72 1.41 1.2029 3 1 4 4 80.71 1.67 1.1906 -3 11 1 4 80.73 1.69 1.1903 -3 11 2 4 81.31 1.10 1.1833 0 1 6 4 82.04 2.15 1.1746 6 6 0 4 82.14 1.80 1.1735 6 3 1 4 82.70 1.27 1.1669 4 4 3 4 83.05 1.01 1.1628 -1 12 1 4 83.20 1.13 1.1612 5 7 1 4 83.53 1.53 1.1574 -4 10 4 4 84.11 1.23 1.1509 -1 10 4 4 85.73 1.46 1.1332 1 12 1 4 86.16 1.86 1.1287 5 9 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.