Hexahydroborite Sedlacek P, Dornberger-Schiff K Acta Crystallographica B27 (1971) 1532-1541 An OD-Disordered modification of the calcium monoborate dihydrate Ca[B(OH)4]2*2H2O Locality: synthetic Sample: MDO (2) _database_code_amcsd 0009398 CELL PARAMETERS: 8.0400 6.6900 7.9500 90.000 104.900 90.000 SPACE GROUP: P2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 413.233 Density (g/cm3): 1.849 MAX. ABS. INTENSITY / VOLUME**2: 5.592331259 RIR: 0.985 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.39 100.00 7.7697 1 0 0 2 13.23 50.62 6.6900 0 1 0 2 17.49 15.15 5.0696 1 1 0 4 19.29 11.64 4.6011 -1 1 1 4 22.58 24.43 3.9385 1 1 1 4 23.15 3.08 3.8413 0 0 2 2 26.49 42.06 3.3650 -2 1 1 4 26.53 29.60 3.3595 2 1 0 4 26.65 11.26 3.3450 0 2 0 2 26.66 28.98 3.3436 -1 1 2 4 26.76 16.44 3.3312 0 1 2 4 28.44 21.52 3.1378 1 0 2 2 29.06 8.00 3.0724 1 2 0 4 31.23 6.30 2.8640 -2 1 2 4 31.34 4.62 2.8539 2 1 1 4 31.49 3.41 2.8409 1 1 2 4 32.47 1.74 2.7577 1 2 1 4 34.63 1.15 2.5899 3 0 0 2 35.38 8.84 2.5372 -2 2 1 4 35.59 49.61 2.5226 0 2 2 4 36.21 27.47 2.4805 -3 1 1 4 36.52 2.38 2.4606 -3 0 2 2 36.56 32.99 2.4578 -1 1 3 4 36.90 1.59 2.4362 2 0 2 2 37.23 14.72 2.4152 3 1 0 4 37.61 3.20 2.3917 0 1 3 4 39.00 1.36 2.3094 -3 1 2 4 39.16 3.11 2.3006 -2 2 2 4 39.25 2.19 2.2953 2 2 1 4 39.37 17.07 2.2885 1 2 2 4 40.45 4.26 2.2300 0 3 0 2 41.81 11.08 2.1606 3 1 1 4 42.16 4.40 2.1435 1 3 0 4 42.20 1.08 2.1416 0 3 1 4 43.00 1.66 2.1036 -1 3 1 4 43.35 1.57 2.0872 -3 2 1 4 43.65 7.03 2.0736 -1 2 3 4 44.23 1.18 2.0478 3 2 0 4 44.69 2.99 2.0277 1 3 1 4 45.00 1.45 2.0147 -3 1 3 4 45.78 18.33 1.9821 -3 2 2 4 46.09 14.42 1.9693 2 2 2 4 46.66 4.13 1.9467 -4 0 2 2 46.77 11.62 1.9424 4 0 0 2 46.98 3.21 1.9340 2 3 0 4 47.06 6.39 1.9310 -1 3 2 4 47.08 5.22 1.9302 -2 0 4 2 47.09 1.32 1.9297 3 0 2 2 47.12 3.77 1.9286 0 3 2 4 47.74 1.08 1.9051 -1 1 4 4 48.72 1.20 1.8691 -4 1 2 4 48.82 2.10 1.8654 4 1 0 4 49.14 4.34 1.8541 3 1 2 4 49.31 3.32 1.8481 2 1 3 4 49.37 7.76 1.8461 0 1 4 4 50.01 5.49 1.8237 -2 3 2 4 50.09 10.55 1.8211 2 3 1 4 51.43 14.14 1.7767 -3 0 4 2 51.89 1.32 1.7620 1 0 4 2 53.35 2.67 1.7172 -3 1 4 4 53.53 4.83 1.7118 -3 3 1 4 53.80 3.14 1.7039 1 1 4 4 54.54 3.30 1.6825 -4 2 2 4 54.57 1.39 1.6818 0 3 3 4 54.90 5.01 1.6725 0 4 0 2 54.92 1.30 1.6718 -2 2 4 4 55.09 1.95 1.6671 2 2 3 4 55.90 5.59 1.6449 2 3 2 4 56.26 1.99 1.6350 1 4 0 4 56.94 1.76 1.6171 -1 4 1 4 58.86 5.27 1.5689 2 0 4 2 59.49 5.79 1.5539 5 0 0 2 59.90 3.41 1.5442 -1 1 5 4 60.00 1.23 1.5419 -4 1 4 4 60.27 2.94 1.5356 4 1 2 4 60.35 1.03 1.5337 -3 3 3 4 60.36 1.34 1.5335 0 4 2 4 62.61 1.35 1.4837 -1 3 4 4 63.03 1.06 1.4749 -5 1 3 4 63.78 1.18 1.4592 3 3 2 4 64.95 2.15 1.4357 -5 2 2 4 65.14 1.69 1.4320 -4 2 4 4 65.40 1.28 1.4270 4 2 2 4 65.89 2.17 1.4175 -3 4 1 4 68.67 1.07 1.3669 -5 1 4 4 72.13 1.28 1.3096 -6 1 2 4 73.11 2.57 1.2944 -5 3 2 4 73.20 3.79 1.2930 -1 3 5 4 73.29 1.34 1.2917 -4 3 4 4 74.25 1.09 1.2773 3 2 4 4 74.47 1.65 1.2740 -6 1 3 4 75.09 2.50 1.2651 2 5 0 4 75.15 1.04 1.2642 -1 5 2 4 75.17 1.44 1.2640 -2 4 4 4 77.38 2.92 1.2333 5 2 2 4 77.85 2.10 1.2270 -1 2 6 4 80.08 1.13 1.1984 4 1 4 4 80.37 1.25 1.1948 1 1 6 4 84.71 1.81 1.1443 2 4 4 4 85.25 2.41 1.1384 5 4 0 4 86.08 1.65 1.1295 -6 1 5 4 87.78 1.15 1.1120 -1 1 7 4 88.64 1.02 1.1034 0 6 1 4 89.51 1.05 1.0950 7 1 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.