Sborgite Merlino S, Sartori F Acta Crystallographica B28 (1972) 3559-3567 The crystal structure of sborgite, NaB5O6(OH)4*3H2O Locality: synthetic _database_code_amcsd 0009465 CELL PARAMETERS: 11.1190 16.4740 13.5760 90.000 112.830 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2291.962 Density (g/cm3): 1.710 MAX. ABS. INTENSITY / VOLUME**2: 2.388467935 RIR: 0.455 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.17 9.18 8.7017 1 1 0 4 10.29 17.59 8.5932 -1 1 1 4 10.74 18.77 8.2370 0 2 0 2 12.87 16.30 6.8800 0 2 1 4 14.16 5.32 6.2562 0 0 2 2 14.18 5.91 6.2444 1 1 1 4 14.46 10.85 6.1254 -1 1 2 4 17.31 11.46 5.1240 2 0 0 2 18.40 7.54 4.8213 -1 3 1 4 19.26 100.00 4.6072 -2 2 1 4 20.02 2.38 4.4342 1 1 2 4 20.36 12.76 4.3628 -1 1 3 4 20.41 3.55 4.3508 2 2 0 4 20.67 31.98 4.2966 -2 2 2 4 20.86 2.75 4.2592 1 3 1 4 21.58 7.92 4.1185 0 4 0 2 22.73 1.64 3.9120 0 4 1 4 23.76 42.09 3.7446 2 2 1 4 23.91 8.08 3.7210 0 2 3 4 24.21 1.66 3.6760 -2 2 3 4 24.97 28.87 3.5664 -3 1 2 4 25.24 28.44 3.5281 1 3 2 4 25.51 2.57 3.4918 -1 3 3 4 26.42 2.92 3.3740 2 0 2 2 26.57 12.01 3.3549 1 1 3 4 26.65 1.69 3.3448 3 1 0 4 26.92 4.38 3.3114 -1 1 4 4 26.94 77.38 3.3090 -2 4 1 4 27.03 3.14 3.2992 -2 0 4 2 27.11 1.52 3.2897 -3 1 3 4 27.79 70.97 3.2101 2 4 0 4 27.99 38.74 3.1881 -2 4 2 4 28.46 1.82 3.1367 1 5 0 4 28.50 4.70 3.1315 -1 5 1 4 28.53 3.26 3.1281 0 0 4 2 29.16 1.79 3.0627 -2 2 4 4 29.23 2.27 3.0558 -3 3 1 4 29.37 24.61 3.0415 -3 3 2 4 30.16 17.29 2.9627 3 1 1 4 30.38 10.84 2.9420 2 4 1 4 30.50 10.65 2.9305 0 4 3 4 30.57 3.40 2.9243 0 2 4 4 30.74 7.34 2.9084 -2 4 3 4 30.83 1.35 2.9006 3 3 0 4 31.07 3.99 2.8787 -1 3 4 4 31.23 13.20 2.8644 -3 3 3 4 33.48 8.82 2.6763 1 1 4 4 33.65 3.22 2.6634 -1 5 3 4 33.85 7.00 2.6479 -1 1 5 4 33.95 1.62 2.6407 3 3 1 4 34.05 3.14 2.6332 -4 2 2 4 34.34 3.36 2.6116 2 2 3 4 34.56 1.43 2.5956 -3 3 4 4 34.66 5.20 2.5883 -4 2 1 4 34.84 20.55 2.5749 -2 4 4 4 35.02 2.65 2.5620 4 0 0 2 35.66 4.48 2.5180 -4 0 4 2 36.06 1.87 2.4911 0 4 4 4 36.62 1.39 2.4541 -3 5 1 4 36.96 2.10 2.4319 1 3 4 4 37.15 3.55 2.4201 2 6 0 4 37.30 8.80 2.4107 -2 6 2 4 37.88 1.42 2.3750 1 5 3 4 37.94 3.68 2.3715 3 5 0 4 38.14 3.68 2.3595 -1 5 4 4 38.27 2.79 2.3516 -3 5 3 4 39.19 1.70 2.2988 2 6 1 4 39.48 3.78 2.2827 -2 6 3 4 39.85 1.53 2.2622 -2 0 6 2 39.93 6.25 2.2578 -4 4 3 4 39.93 6.27 2.2576 -2 4 5 4 40.09 4.76 2.2491 4 2 1 4 40.58 2.13 2.2230 3 5 1 4 40.70 11.02 2.2171 2 2 4 4 40.70 3.26 2.2167 -1 7 2 4 41.04 1.10 2.1992 -5 1 2 4 41.39 1.64 2.1814 -2 2 6 4 41.42 4.23 2.1801 -3 1 6 4 41.51 12.22 2.1754 4 4 0 4 42.06 12.70 2.1483 -4 4 4 4 42.18 4.76 2.1424 -5 1 1 4 42.45 2.47 2.1296 2 6 2 4 42.85 1.58 2.1104 -2 6 4 4 43.03 4.30 2.1021 4 0 2 2 43.17 1.08 2.0955 1 7 2 4 43.20 7.00 2.0941 1 5 4 4 43.39 1.38 2.0854 0 0 6 2 43.66 3.30 2.0733 1 3 5 4 43.97 1.50 2.0593 0 8 0 2 44.02 1.58 2.0571 -1 3 6 4 44.37 7.81 2.0418 -3 3 6 4 44.56 2.27 2.0332 4 4 1 4 44.83 2.53 2.0216 0 2 6 4 45.12 3.61 2.0095 2 4 4 4 45.52 3.23 1.9929 -4 2 6 4 45.57 1.20 1.9906 -5 3 4 4 45.76 1.15 1.9828 -2 4 6 4 46.42 7.32 1.9560 0 8 2 4 46.50 1.58 1.9532 -4 6 2 4 46.69 2.43 1.9455 3 1 4 4 46.72 4.78 1.9443 2 6 3 4 46.83 1.90 1.9400 1 7 3 4 46.88 1.88 1.9380 3 7 0 4 47.06 1.63 1.9310 -2 8 1 4 47.16 4.44 1.9271 -3 7 3 4 47.22 2.61 1.9250 -4 6 3 4 47.22 7.39 1.9249 -2 6 5 4 47.51 2.55 1.9138 2 2 5 4 47.59 1.47 1.9107 2 8 0 4 47.71 1.61 1.9061 -2 8 2 4 48.00 1.74 1.8953 5 1 1 4 48.25 5.20 1.8862 -2 2 7 4 48.50 2.39 1.8771 -1 1 7 4 48.63 3.26 1.8723 4 4 2 4 49.13 2.42 1.8544 3 7 1 4 49.20 2.76 1.8519 1 5 5 4 49.27 2.32 1.8495 0 6 5 4 49.39 2.73 1.8453 3 3 4 4 49.52 1.75 1.8405 -5 5 2 4 49.53 1.82 1.8403 -1 5 6 4 49.57 4.91 1.8389 -6 0 2 2 49.67 6.34 1.8353 -5 5 3 4 50.49 1.18 1.8075 -6 2 3 4 50.51 1.06 1.8069 -5 5 1 4 50.66 1.10 1.8019 1 9 0 4 50.89 1.52 1.7943 -4 2 7 4 51.13 1.32 1.7866 -1 3 7 4 51.68 1.97 1.7689 -5 3 6 4 51.83 1.32 1.7641 2 6 4 4 51.83 1.26 1.7638 -1 9 2 4 52.17 1.04 1.7533 -2 4 7 4 52.38 1.14 1.7466 5 1 2 4 53.06 1.42 1.7260 -6 2 5 4 53.26 1.06 1.7200 0 8 4 4 53.41 1.81 1.7154 3 1 5 4 53.55 1.43 1.7114 4 4 3 4 54.67 1.11 1.6788 -4 4 7 4 54.68 2.13 1.6787 -6 0 6 2 55.54 2.62 1.6545 -4 8 2 4 55.67 1.52 1.6511 5 5 1 4 55.72 2.17 1.6496 -4 0 8 2 55.80 1.98 1.6474 0 10 0 2 55.96 6.02 1.6432 -4 8 1 4 56.18 1.00 1.6372 -2 8 5 4 56.74 1.12 1.6225 -6 4 5 4 57.05 1.42 1.6144 -1 7 6 4 57.41 2.12 1.6050 4 8 0 4 58.42 1.58 1.5798 -7 1 3 4 59.56 1.26 1.5521 4 6 3 4 60.61 1.75 1.5279 -6 6 2 4 61.98 1.15 1.4973 -7 1 6 4 62.72 1.33 1.4814 -1 11 1 4 63.13 1.70 1.4727 -6 0 8 2 63.86 1.93 1.4576 0 10 4 4 69.28 1.02 1.3562 2 0 8 2 72.48 1.00 1.3040 0 12 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.