H10 K3 O17 P3 Te Boudjada N, Averbuch-Pouchot M, Durif A Acta Crystallographica B37 (1981) 647-649 Structure d'un Trimetaphosphate-Tellurate de Potassium Dihydrate Te(OH)6K3P3O9(H2O)2 _cod_database_code 1007063 _database_code_amcsd 0009733 CELL PARAMETERS: 15.6100 7.4560 14.8400 90.000 108.010 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1642.572 Density (g/cm3): 2.466 MAX. ABS. INTENSITY / VOLUME**2: 10.56374864 RIR: 1.395 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.95 36.98 14.8451 1 0 0 2 11.92 22.20 7.4226 2 0 0 2 12.11 14.02 7.3093 -1 0 2 2 12.54 9.37 7.0564 0 0 2 2 13.29 19.94 6.6628 1 1 0 4 14.40 38.77 6.1514 -2 0 2 2 15.47 3.63 5.7262 1 1 1 4 15.48 9.62 5.7238 1 0 2 2 16.65 2.33 5.3257 -2 1 1 4 16.85 44.68 5.2603 2 1 0 4 17.30 70.18 5.1251 0 1 2 4 17.93 5.53 4.9484 3 0 0 2 18.70 100.00 4.7449 -2 1 2 4 19.55 4.74 4.5402 1 1 2 4 19.86 28.75 4.4704 2 0 2 2 21.55 4.97 4.1230 3 1 0 4 21.99 20.69 4.0422 -3 1 2 4 23.20 12.91 3.8340 2 1 2 4 23.38 13.99 3.8049 -4 0 2 2 23.87 28.07 3.7280 0 2 0 2 23.98 3.24 3.7113 4 0 0 2 23.99 2.35 3.7087 3 1 1 4 24.36 4.94 3.6546 -2 0 4 2 24.62 2.97 3.6157 1 2 0 4 24.78 3.82 3.5933 -3 1 3 4 24.96 2.01 3.5678 -1 2 1 4 24.97 3.02 3.5662 3 0 2 2 25.24 14.77 3.5282 0 0 4 2 25.79 2.28 3.4543 -4 1 1 4 25.89 10.86 3.4409 1 2 1 4 26.09 6.14 3.4149 -3 0 4 2 26.30 4.80 3.3891 -4 1 2 4 26.76 15.23 3.3314 2 2 0 4 26.83 30.37 3.3224 4 1 0 4 26.85 3.47 3.3210 -1 2 2 4 26.90 9.75 3.3140 -1 1 4 4 27.05 13.05 3.2963 0 2 2 4 27.17 4.22 3.2816 -2 1 4 4 27.73 18.55 3.2171 3 1 2 4 27.74 38.79 3.2162 1 0 4 2 27.99 3.96 3.1882 -2 2 2 4 28.08 4.02 3.1777 2 1 3 4 28.27 18.99 3.1566 -4 1 3 4 28.37 9.46 3.1462 2 2 1 4 28.57 26.53 3.1238 1 2 2 4 28.75 14.55 3.1047 -3 1 4 4 29.03 8.55 3.0757 -4 0 4 2 29.27 2.40 3.0511 4 1 1 4 29.48 1.31 3.0295 -3 2 1 4 30.01 2.68 2.9776 3 2 0 4 30.10 16.05 2.9690 5 0 0 2 30.33 3.53 2.9467 -3 2 2 4 30.60 1.07 2.9218 0 2 3 4 31.20 6.41 2.8666 -5 1 1 4 31.24 1.16 2.8631 2 2 2 4 31.24 3.71 2.8630 -5 1 2 4 31.25 2.34 2.8619 2 0 4 2 31.46 1.47 2.8433 -4 1 4 4 31.85 4.75 2.8098 3 2 1 4 32.46 1.34 2.7585 -3 2 3 4 32.46 5.39 2.7584 5 1 0 4 33.54 3.18 2.6719 -3 1 5 4 33.54 2.06 2.6718 2 1 4 4 33.66 1.74 2.6629 -4 2 2 4 34.36 1.00 2.6098 -2 2 4 4 34.51 6.25 2.5992 -6 0 2 2 35.07 2.66 2.5588 -5 1 4 4 35.26 2.16 2.5456 -4 2 3 4 35.65 4.60 2.5181 -3 2 4 4 36.27 8.76 2.4766 5 0 2 2 36.32 1.02 2.4733 -2 0 6 2 36.66 8.65 2.4512 1 3 0 4 36.79 11.06 2.4428 -1 0 6 2 36.89 6.90 2.4364 -3 0 6 2 36.90 1.20 2.4361 -1 3 1 4 36.91 1.31 2.4352 1 2 4 4 37.39 1.26 2.4053 -6 0 4 2 37.45 4.52 2.4014 -6 1 3 4 37.58 1.26 2.3933 3 1 4 4 37.74 1.14 2.3839 -5 2 2 4 37.92 4.30 2.3725 -4 2 4 4 38.09 5.76 2.3625 -2 3 1 4 38.19 2.35 2.3567 2 3 0 4 38.30 1.90 2.3503 5 1 2 4 38.33 4.25 2.3483 6 1 0 4 38.34 9.29 2.3475 -2 1 6 4 38.40 7.37 2.3442 0 3 2 4 38.77 4.62 2.3225 5 2 0 4 38.79 9.05 2.3214 -1 1 6 4 39.09 3.00 2.3044 -2 3 2 4 39.53 2.53 2.2797 1 3 2 4 40.07 2.14 2.2503 0 2 5 4 40.20 2.99 2.2432 0 1 6 4 40.39 1.36 2.2333 -4 1 6 4 40.45 2.82 2.2299 -7 0 2 2 40.62 2.22 2.2208 -1 3 3 4 40.87 11.86 2.2081 -3 3 2 4 41.07 1.01 2.1975 0 3 3 4 41.12 1.71 2.1952 -2 3 3 4 41.57 2.78 2.1722 2 3 2 4 42.21 2.03 2.1410 4 1 4 4 42.28 4.12 2.1376 6 0 2 2 42.39 1.84 2.1321 -6 2 2 4 42.40 2.04 2.1318 -7 0 4 2 42.66 1.32 2.1194 -6 2 1 4 42.76 4.26 2.1146 -5 1 6 4 43.25 2.23 2.0918 3 2 4 4 43.49 2.27 2.0808 -4 3 2 4 43.84 5.04 2.0651 4 3 0 4 43.89 6.27 2.0630 -1 3 4 4 43.89 1.04 2.0629 5 2 2 4 43.92 2.17 2.0615 6 2 0 4 44.07 4.09 2.0548 6 1 2 4 44.17 3.49 2.0505 -6 0 6 2 44.33 5.39 2.0432 -1 2 6 4 44.41 3.55 2.0398 7 1 0 4 44.42 3.15 2.0395 -3 2 6 4 44.43 1.38 2.0390 3 3 2 4 44.46 2.47 2.0377 -2 1 7 4 44.66 2.93 2.0292 -3 1 7 4 45.12 1.04 2.0095 -3 3 4 4 46.11 1.20 1.9686 6 2 1 4 46.86 2.80 1.9389 7 1 1 4 47.30 3.36 1.9217 5 1 4 4 47.51 1.13 1.9137 -7 2 2 4 47.64 1.01 1.9087 3 3 3 4 47.72 1.26 1.9058 5 3 0 4 47.79 1.33 1.9033 -2 3 5 4 47.81 1.46 1.9025 -8 0 4 2 47.92 1.02 1.8983 -7 2 3 4 48.07 1.20 1.8928 -7 0 6 2 48.26 2.47 1.8856 -8 1 2 4 48.49 7.58 1.8773 7 0 2 2 48.86 3.62 1.8640 0 4 0 2 49.09 2.78 1.8556 8 0 0 2 49.13 5.07 1.8544 6 2 2 4 49.26 1.17 1.8498 -2 0 8 2 49.27 1.32 1.8495 1 4 0 4 49.30 3.62 1.8484 3 1 6 4 49.31 1.31 1.8480 0 4 1 4 49.44 1.73 1.8434 -8 1 4 4 49.44 2.00 1.8433 7 2 0 4 49.67 2.23 1.8355 -3 2 7 4 49.70 2.80 1.8346 -7 1 6 4 49.91 1.31 1.8273 -4 0 8 2 50.15 2.24 1.8189 -1 0 8 2 50.48 1.66 1.8079 2 4 0 4 50.51 3.70 1.8070 2 2 6 4 50.53 3.96 1.8062 -1 4 2 4 50.78 3.70 1.7980 -3 1 8 4 50.82 1.52 1.7966 -6 2 6 4 50.83 1.81 1.7963 -6 3 2 4 51.06 1.22 1.7887 -6 3 1 4 51.42 2.84 1.7769 -5 0 8 2 51.49 5.88 1.7748 -4 1 8 4 51.57 2.52 1.7724 1 4 2 4 51.73 3.90 1.7671 -1 1 8 4 51.83 1.75 1.7641 0 0 8 2 52.07 1.09 1.7563 4 0 6 2 52.14 1.16 1.7543 5 3 2 4 52.16 4.25 1.7534 6 3 0 4 52.18 6.04 1.7531 -2 3 6 4 52.32 1.28 1.7486 -5 3 5 4 52.46 2.99 1.7443 3 4 0 4 52.53 1.69 1.7421 -8 0 6 2 52.96 2.81 1.7290 -9 0 2 2 53.24 2.10 1.7204 2 4 2 4 53.61 1.33 1.7095 4 1 6 4 54.12 2.66 1.6946 -8 2 4 4 54.23 2.50 1.6916 1 0 8 2 54.75 2.05 1.6767 7 2 2 4 54.84 3.90 1.6739 -4 4 2 4 55.07 2.15 1.6676 -9 1 4 4 55.19 1.10 1.6644 -6 1 8 4 55.27 1.95 1.6619 4 3 4 4 55.30 1.05 1.6612 8 2 0 4 55.33 1.65 1.6605 -2 4 4 4 55.45 2.14 1.6570 -2 2 8 4 55.73 1.92 1.6495 -5 3 6 4 55.73 2.08 1.6495 9 0 0 2 55.81 1.00 1.6471 -7 3 1 4 55.84 1.13 1.6465 2 4 3 4 56.05 1.63 1.6408 -4 2 8 4 56.22 1.42 1.6361 -3 4 4 4 56.81 1.54 1.6206 6 3 2 4 57.11 1.74 1.6127 1 4 4 4 57.20 4.73 1.6105 9 1 0 4 57.27 1.73 1.6086 6 2 4 4 58.42 2.05 1.5797 5 1 6 4 58.46 1.35 1.5787 5 4 0 4 58.48 1.11 1.5782 7 2 3 4 58.63 1.39 1.5746 7 1 4 4 58.69 1.50 1.5731 4 4 2 4 58.88 2.28 1.5685 -9 2 2 4 60.35 1.75 1.5336 -8 3 2 4 60.95 1.14 1.5200 -10 1 2 4 61.19 1.39 1.5147 -6 4 2 4 61.47 1.45 1.5084 9 2 0 4 61.59 2.70 1.5058 -7 3 6 4 61.85 1.40 1.5001 3 4 4 4 62.31 3.01 1.4901 -7 2 8 4 62.35 1.26 1.4893 5 4 2 4 62.37 1.54 1.4888 6 4 0 4 62.53 1.07 1.4854 -3 3 8 4 62.61 2.64 1.4837 1 5 0 4 62.70 1.84 1.4819 -1 4 6 4 62.76 2.09 1.4804 -3 4 6 4 63.12 1.28 1.4730 -9 2 6 4 63.15 1.86 1.4722 -4 3 8 4 63.84 1.16 1.4581 -4 4 6 4 64.16 2.57 1.4516 -4 1 10 4 64.22 2.39 1.4503 -10 1 6 4 64.81 1.98 1.4386 0 3 8 4 65.19 2.01 1.4310 -6 0 10 2 65.64 1.55 1.4223 -9 1 8 4 65.70 1.22 1.4212 -1 1 10 4 66.43 1.18 1.4073 -6 3 8 4 66.91 1.11 1.3984 1 3 8 4 67.52 1.42 1.3873 8 3 2 4 67.70 1.02 1.3839 2 4 6 4 67.72 1.04 1.3837 4 5 0 4 68.07 1.20 1.3774 7 0 6 2 68.24 1.71 1.3743 9 3 0 4 68.81 1.17 1.3644 8 2 4 4 70.01 1.15 1.3439 -5 5 2 4 70.04 1.29 1.3434 1 1 10 4 70.49 1.17 1.3359 4 2 8 4 71.25 2.47 1.3236 5 1 8 4 71.78 1.53 1.3151 8 4 0 4 71.91 1.65 1.3130 -2 4 8 4 74.20 1.03 1.2780 6 3 6 4 74.64 1.03 1.2715 -4 3 10 4 74.70 1.37 1.2707 -10 3 6 4 74.91 1.60 1.2676 -9 4 2 4 75.36 1.50 1.2612 -11 1 8 4 76.03 1.03 1.2517 -9 3 8 4 77.99 1.17 1.2252 -7 4 8 4 78.64 1.61 1.2167 -3 1 12 4 78.72 1.11 1.2156 -9 4 6 4 78.85 1.50 1.2139 -10 1 10 4 81.35 2.40 1.1829 5 3 8 4 83.64 1.47 1.1562 -8 1 12 4 84.52 1.01 1.1463 5 6 0 4 85.31 1.09 1.1377 -11 3 8 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.