C6H9SI Marsh R E, Herbstein F H Acta Crystallographica B44 (1988) 77-88 More space-group changes _database_code_amcsd 0009822 CELL PARAMETERS: 18.0380 6.6110 7.4200 90.000 90.000 90.000 SPACE GROUP: Pnam X-RAY WAVELENGTH: 1.541838 Cell Volume: 884.829 Density (g/cm3): 1.734 MAX. ABS. INTENSITY / VOLUME**2: 12.95633108 RIR: 2.433 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.81 17.77 9.0190 2 0 0 2 14.27 10.16 6.2072 1 1 0 4 15.46 16.64 5.7300 2 0 1 4 16.63 34.33 5.3320 2 1 0 4 17.97 82.50 4.9360 0 1 1 4 18.64 50.26 4.7610 1 1 1 8 19.69 38.64 4.5095 4 0 0 2 19.96 2.91 4.4481 3 1 0 4 20.51 5.64 4.3300 2 1 1 8 23.08 64.99 3.8536 4 0 1 4 23.32 100.00 3.8151 3 1 1 8 23.89 57.52 3.7253 4 1 0 4 23.99 44.18 3.7100 0 0 2 2 25.97 14.55 3.4311 2 0 2 4 26.78 14.26 3.3293 4 1 1 8 26.97 1.04 3.3055 0 2 0 2 27.43 5.66 3.2514 1 2 0 4 28.02 11.83 3.1845 1 1 2 8 28.18 2.36 3.1668 5 1 0 4 29.33 57.89 3.0453 2 1 2 8 29.72 9.69 3.0063 6 0 0 2 30.01 64.27 2.9780 1 2 1 8 30.87 29.82 2.8966 3 2 0 4 31.22 11.54 2.8650 4 0 2 4 31.24 7.72 2.8632 2 2 1 8 34.11 19.92 2.6288 4 1 2 8 34.95 22.16 2.5676 6 1 1 8 35.79 1.31 2.5090 4 2 1 8 36.75 1.79 2.4452 1 2 2 8 36.88 2.42 2.4372 5 2 0 4 37.33 5.94 2.4086 5 1 2 8 37.46 13.00 2.4009 7 1 0 4 37.71 10.11 2.3853 2 0 3 4 37.79 2.10 2.3805 2 2 2 8 38.54 13.96 2.3357 6 0 2 4 38.88 2.56 2.3165 0 1 3 4 38.90 18.72 2.3155 5 2 1 8 39.21 4.38 2.2977 1 1 3 8 39.45 7.29 2.2843 7 1 1 8 39.47 17.92 2.2832 3 2 2 8 40.19 4.88 2.2437 2 1 3 8 41.27 7.27 2.1874 1 3 0 4 41.65 6.36 2.1686 4 0 3 4 41.79 13.74 2.1616 3 1 3 8 41.87 12.36 2.1573 8 0 1 4 42.22 2.94 2.1407 2 3 0 4 42.35 3.74 2.1340 8 1 0 4 42.43 2.17 2.1304 6 2 1 8 43.11 2.62 2.0981 1 3 1 8 43.94 1.94 2.0605 4 1 3 8 44.16 3.97 2.0509 8 1 1 8 44.48 7.04 2.0370 5 2 2 8 44.59 5.05 2.0323 7 2 0 4 44.97 9.00 2.0157 7 1 2 8 45.51 15.81 1.9930 3 3 1 8 46.11 21.89 1.9685 1 2 3 8 46.32 11.56 1.9601 7 2 1 8 46.98 4.39 1.9343 2 2 3 8 47.67 1.78 1.9076 6 2 2 8 48.30 11.73 1.8843 1 3 2 8 48.40 4.51 1.8806 5 3 0 4 48.90 1.30 1.8627 8 2 0 4 49.06 1.01 1.8570 9 1 1 8 49.11 6.40 1.8550 0 0 4 2 49.14 4.12 1.8542 2 3 2 8 49.26 5.75 1.8498 8 1 2 8 49.69 10.36 1.8350 6 1 3 8 50.04 4.81 1.8229 5 3 1 8 50.21 1.85 1.8170 2 0 4 4 50.60 1.13 1.8038 10 0 0 2 51.26 3.58 1.7824 7 2 2 8 51.41 1.57 1.7773 1 1 4 8 52.19 7.01 1.7528 10 0 1 4 52.21 7.73 1.7520 2 1 4 8 52.38 2.39 1.7467 4 3 2 8 52.59 2.08 1.7402 10 1 0 4 52.73 10.73 1.7360 5 2 3 8 52.98 2.27 1.7284 6 3 1 8 53.17 1.83 1.7227 7 1 3 8 53.41 3.04 1.7155 4 0 4 4 53.47 4.49 1.7138 9 2 0 4 54.13 4.33 1.6942 10 1 1 8 54.72 9.34 1.6774 5 3 2 8 54.81 2.76 1.6748 7 3 0 4 55.12 5.54 1.6663 8 0 3 4 55.32 4.59 1.6605 4 1 4 8 55.61 1.98 1.6528 0 4 0 2 56.31 1.67 1.6337 7 3 1 8 56.62 1.21 1.6257 2 4 0 4 57.00 1.27 1.6157 8 1 3 8 57.50 1.29 1.6029 6 3 2 8 57.59 1.27 1.6006 5 1 4 8 57.86 1.41 1.5936 3 4 0 4 57.94 3.86 1.5916 11 1 0 4 58.09 5.32 1.5880 2 4 1 8 58.13 5.11 1.5870 3 3 3 8 58.46 3.49 1.5787 6 0 4 4 58.59 1.81 1.5755 10 1 2 8 58.81 2.96 1.5702 7 2 3 8 59.14 5.88 1.5621 3 2 4 8 59.41 10.54 1.5558 9 2 2 8 59.58 1.02 1.5518 4 4 0 4 60.67 2.01 1.5265 7 3 2 8 61.00 3.50 1.5189 4 4 1 8 61.15 1.19 1.5157 9 1 3 8 61.41 2.52 1.5097 0 4 2 4 61.65 1.32 1.5045 1 4 2 8 61.99 3.21 1.4970 5 3 3 8 62.97 1.64 1.4761 5 2 4 8 63.36 3.35 1.4679 7 1 4 8 63.54 1.61 1.4643 3 4 2 8 63.61 3.85 1.4627 11 1 2 8 63.87 2.68 1.4574 10 0 3 4 64.04 5.02 1.4540 9 3 1 8 64.32 2.41 1.4483 6 4 0 4 64.34 2.19 1.4480 0 1 5 4 64.57 1.44 1.4433 1 1 5 8 64.69 3.72 1.4410 11 2 1 8 64.84 3.66 1.4380 12 1 1 8 65.60 1.24 1.4232 10 1 3 8 66.04 3.66 1.4148 1 3 4 8 66.31 2.56 1.4096 4 0 5 4 66.41 4.00 1.4077 3 1 5 8 66.72 1.17 1.4019 2 3 4 8 66.82 2.18 1.4000 8 1 4 8 67.20 1.67 1.3932 12 0 2 4 68.48 1.59 1.3701 7 2 4 8 68.64 1.68 1.3674 7 4 1 8 68.73 1.26 1.3658 11 2 2 8 69.15 3.46 1.3585 2 4 3 8 69.65 3.86 1.3500 1 2 5 8 69.70 3.41 1.3492 6 4 2 8 70.91 1.54 1.3291 8 3 3 8 71.43 3.41 1.3206 5 3 4 8 71.75 1.58 1.3156 11 3 0 4 71.81 2.98 1.3145 4 4 3 8 71.97 2.73 1.3120 8 4 1 8 72.45 2.10 1.3045 6 1 5 8 72.63 2.59 1.3017 0 5 1 4 74.63 4.38 1.2717 9 3 3 8 74.79 3.20 1.2694 14 0 1 4 74.81 1.03 1.2691 10 1 4 8 74.83 1.23 1.2688 4 5 0 4 74.92 2.08 1.2675 5 2 5 8 75.12 1.42 1.2646 14 1 0 4 75.23 1.32 1.2630 11 2 3 8 75.38 3.82 1.2610 12 1 3 8 75.39 1.33 1.2608 13 2 1 8 75.53 4.03 1.2588 9 2 4 8 75.84 1.62 1.2545 8 4 2 8 76.11 2.40 1.2506 4 5 1 8 76.66 1.15 1.2431 7 3 4 8 76.89 1.53 1.2399 11 3 2 8 76.91 1.68 1.2396 8 0 5 4 77.13 2.09 1.2367 0 0 6 2 77.32 1.40 1.2340 0 4 4 4 77.34 1.48 1.2338 2 5 2 8 79.19 2.04 1.2095 13 2 2 8 79.32 2.14 1.2079 11 1 4 8 79.48 2.61 1.2059 3 3 5 8 79.57 1.07 1.2047 2 1 6 8 79.75 1.37 1.2025 10 4 1 8 79.91 2.74 1.2005 4 5 2 8 80.07 2.11 1.1985 7 2 5 8 80.39 2.43 1.1945 6 5 1 8 82.12 2.07 1.1737 4 1 6 8 82.14 1.28 1.1734 8 4 3 8 82.77 1.81 1.1660 0 5 3 4 83.32 1.12 1.1597 13 3 1 8 83.50 1.14 1.1577 10 4 2 8 84.55 1.60 1.1460 10 0 5 4 84.86 1.16 1.1427 14 0 3 4 84.96 1.77 1.1416 6 4 4 8 85.05 1.18 1.1406 8 5 0 4 85.35 2.18 1.1373 3 2 6 8 86.03 1.22 1.1301 15 2 0 4 86.14 1.03 1.1289 4 5 3 8 87.05 1.18 1.1194 13 3 2 8 89.05 1.42 1.0994 7 1 6 8 89.40 1.14 1.0960 2 4 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.