H23.5 O36.5 P8 Tl3.5 Chiadmi M, Vicat J, Tran Qui D, Boudjada A Acta Crystallographica C41 (1985) 811-814 Structure de l'orthophosphate acide de thallium a valence mixte, (Tl3 (Tl0.5 (H3 O)0.5) H14 (P O4)8) (H2 O)4 _cod_database_code 1008945 _database_code_amcsd 0016809 CELL PARAMETERS: 9.8200 9.9730 17.8700 90.140 90.010 119.460 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1523.801 Density (g/cm3): 3.371 MAX. ABS. INTENSITY / VOLUME**2: 88.83209769 RIR: 8.579 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.90 100.00 8.9350 0 0 2 2 10.19 1.29 8.6834 0 1 0 2 11.47 1.09 7.7176 -1 0 1 2 11.47 1.12 7.7135 1 -1 1 2 17.78 2.39 4.9882 1 1 0 2 17.79 2.28 4.9856 -1 2 0 2 18.07 1.58 4.9100 -2 1 0 2 18.46 1.00 4.8053 1 -2 1 2 18.74 2.11 4.7347 -2 1 1 2 18.74 2.19 4.7343 2 -1 1 2 19.87 3.95 4.4675 0 0 4 2 20.37 4.53 4.3602 -1 -1 2 2 20.38 4.56 4.3582 1 -2 2 2 20.41 3.33 4.3506 1 1 2 2 20.42 3.38 4.3493 -1 2 2 2 20.46 4.34 4.3417 0 2 0 2 20.64 1.17 4.3034 -2 1 2 2 20.64 1.25 4.3028 2 -1 2 2 20.78 4.67 4.2751 2 0 0 2 20.79 4.72 4.2730 -2 2 0 2 22.75 12.82 3.9096 0 -2 2 2 22.80 1.70 3.9006 0 2 2 2 23.08 15.10 3.8541 2 0 2 2 23.08 15.12 3.8529 -2 2 2 2 23.48 4.05 3.7891 -2 1 3 2 23.48 4.05 3.7884 2 -1 3 2 26.75 6.23 3.3322 -1 -1 4 2 26.76 6.20 3.3311 1 -2 4 2 26.82 3.60 3.3236 1 1 4 2 26.83 3.65 3.3232 -1 2 4 2 27.23 1.70 3.2752 1 2 0 2 27.24 1.76 3.2740 -1 3 0 2 27.73 1.51 3.2170 -3 1 0 2 27.74 1.51 3.2163 -3 2 0 2 27.88 1.79 3.1995 2 1 1 2 27.90 1.73 3.1979 -2 3 1 2 28.63 6.44 3.1181 0 -2 4 2 28.71 6.91 3.1091 0 2 4 2 28.88 5.23 3.0912 -2 0 4 2 28.90 5.18 3.0899 2 -2 4 2 28.93 9.10 3.0863 2 0 4 2 28.93 9.06 3.0860 -2 2 4 2 29.01 2.00 3.0779 -1 -2 2 2 29.02 1.97 3.0768 1 -3 2 2 29.52 1.19 3.0261 3 -1 2 2 29.52 1.17 3.0259 -3 2 2 2 30.00 1.21 2.9783 0 0 6 2 30.89 1.15 2.8945 0 3 0 2 30.94 2.04 2.8898 -2 1 5 2 30.95 2.04 2.8893 2 -1 5 2 31.36 1.04 2.8526 2 1 3 2 31.37 1.07 2.8516 -2 3 3 2 31.79 1.08 2.8152 -3 0 1 2 31.80 1.08 2.8137 3 -3 1 2 35.05 1.43 2.5601 -1 -1 6 2 35.06 1.51 2.5596 1 -2 6 2 36.01 1.82 2.4941 2 2 0 2 36.03 1.80 2.4928 -2 4 0 2 36.54 1.01 2.4593 0 -2 6 2 36.60 2.11 2.4550 -4 2 0 2 36.64 2.23 2.4527 0 2 6 2 36.75 1.50 2.4456 -2 0 6 2 36.76 1.54 2.4448 2 -2 6 2 36.81 2.28 2.4420 2 0 6 2 36.81 2.28 2.4419 -2 2 6 2 36.96 1.51 2.4324 0 -3 4 2 37.38 2.36 2.4057 1 3 0 2 37.39 2.33 2.4051 -1 4 0 2 37.75 1.89 2.3829 3 1 0 2 37.78 1.89 2.3815 -3 4 0 2 38.44 1.19 2.3421 4 -1 1 2 38.45 1.16 2.3415 -4 3 1 2 38.73 1.11 2.3247 -1 -3 2 2 38.75 1.13 2.3240 1 -4 2 2 39.10 1.05 2.3036 -3 -1 2 2 39.13 1.09 2.3022 3 -4 2 2 39.15 1.47 2.3012 3 1 2 2 39.17 1.45 2.3001 -3 4 2 2 40.38 2.34 2.2337 0 0 8 2 41.29 1.07 2.1863 -3 1 6 2 41.31 1.04 2.1857 3 -2 6 2 42.63 1.42 2.1207 -1 -3 4 2 42.64 1.34 2.1201 1 -4 4 2 43.06 1.52 2.1006 3 1 4 2 43.08 1.51 2.0999 -3 4 4 2 45.73 2.86 1.9839 0 2 8 2 45.80 1.43 1.9811 -2 0 8 2 45.81 1.42 1.9806 2 -2 8 2 49.67 1.27 1.8354 -3 1 8 2 49.68 1.25 1.8350 3 -2 8 2 51.11 1.91 1.7870 0 0 10 2 56.82 1.20 1.6203 0 -5 4 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.