K Li O6 P2 El Horr N, Bagieu M Acta Crystallographica C41 (1985) 1157-1159 Structure de la forme de haute temperature du polyphosphate de lithium et de potassium: Li K (P O3)2 _cod_database_code 1008946 _database_code_amcsd 0016814 CELL PARAMETERS: 13.7530 13.8180 11.8650 90.000 90.340 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2254.772 Density (g/cm3): 2.403 MAX. ABS. INTENSITY / VOLUME**2: 4.398031803 RIR: 0.596 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.07 1.24 9.7477 1 1 0 4 11.73 13.43 7.5474 -1 1 1 4 11.77 15.29 7.5163 1 1 1 4 12.81 1.93 6.9090 0 2 0 2 14.84 71.39 5.9705 0 2 1 4 14.93 15.53 5.9324 0 0 2 2 17.53 6.88 5.0582 1 1 2 4 18.20 84.21 4.8738 2 2 0 4 19.66 1.13 4.5150 -2 2 1 4 19.71 37.69 4.5050 -2 0 2 2 19.72 2.06 4.5016 2 2 1 4 19.72 3.84 4.5009 0 2 2 4 19.82 31.55 4.4787 2 0 2 2 20.41 4.04 4.3511 3 1 0 4 21.67 10.87 4.1012 -1 3 1 4 21.70 5.44 4.0962 1 3 1 4 21.72 1.18 4.0925 -3 1 1 4 21.80 9.39 4.0776 3 1 1 4 23.58 63.71 3.7737 -2 2 2 4 23.67 100.00 3.7581 2 2 2 4 24.32 1.99 3.6594 1 1 3 4 25.30 4.44 3.5203 -1 3 2 4 25.32 1.61 3.5180 -3 1 2 4 25.35 7.96 3.5140 1 3 2 4 25.46 27.84 3.4991 3 1 2 4 25.79 21.42 3.4545 0 4 0 2 25.91 4.01 3.4382 4 0 0 2 25.96 6.33 3.4324 0 2 3 4 26.88 2.69 3.3168 0 4 1 4 28.45 27.79 3.1372 -3 3 1 4 28.51 74.95 3.1305 3 3 1 4 29.02 98.41 3.0774 -2 2 3 4 29.14 5.18 3.0647 2 2 3 4 29.89 7.50 2.9894 -2 4 1 4 29.93 3.74 2.9855 2 4 1 4 29.93 56.34 2.9853 0 4 2 4 29.95 38.38 2.9833 -4 2 1 4 29.96 9.97 2.9824 -4 0 2 2 30.12 14.74 2.9671 4 0 2 2 30.13 5.98 2.9662 0 0 4 2 30.46 5.73 2.9348 -3 1 3 4 30.52 8.85 2.9289 1 3 3 4 30.63 17.48 2.9184 3 1 3 4 31.33 2.53 2.8548 -3 3 2 4 31.45 1.12 2.8447 3 3 2 4 31.49 12.13 2.8411 -1 1 4 4 31.56 10.79 2.8344 1 1 4 4 32.67 11.52 2.7413 -2 4 2 4 32.70 5.45 2.7382 -4 2 2 4 32.74 16.49 2.7354 2 4 2 4 32.85 1.38 2.7263 4 2 2 4 34.04 1.17 2.6338 -5 1 1 4 34.13 12.47 2.6272 5 1 1 4 34.47 10.09 2.6018 0 4 3 4 35.36 5.83 2.5386 -2 2 4 4 35.49 3.49 2.5291 2 2 4 4 35.84 1.04 2.5054 3 3 3 4 36.51 1.45 2.4611 -5 1 2 4 36.59 8.49 2.4560 -1 3 4 4 36.65 2.20 2.4517 1 3 4 4 36.68 4.52 2.4503 5 1 2 4 36.77 6.96 2.4445 3 1 4 4 36.88 55.97 2.4369 4 4 0 4 36.91 2.24 2.4354 -4 2 3 4 36.99 3.03 2.4303 2 4 3 4 37.65 2.97 2.3891 -4 4 1 4 37.72 5.66 2.3851 4 4 1 4 38.02 3.86 2.3668 3 5 0 4 38.11 1.08 2.3615 5 3 0 4 39.03 3.70 2.3079 -1 1 5 4 39.11 1.03 2.3030 0 6 0 2 39.31 3.94 2.2921 6 0 0 2 39.87 1.16 2.2608 0 6 1 4 39.94 1.29 2.2575 -4 4 2 4 40.06 2.00 2.2508 4 4 2 4 40.07 1.07 2.2504 0 4 4 4 40.27 2.88 2.2393 4 0 4 2 40.36 1.78 2.2346 -5 1 3 4 40.37 7.79 2.2340 1 5 3 4 40.59 1.03 2.2226 5 1 3 4 41.01 2.07 2.2006 -3 5 2 4 41.07 5.82 2.1979 -5 3 2 4 41.10 1.32 2.1960 3 5 2 4 41.22 9.10 2.1902 5 3 2 4 41.34 1.24 2.1838 2 6 0 4 41.51 1.69 2.1755 6 2 0 4 42.06 7.12 2.1484 -2 6 1 4 42.09 1.39 2.1470 2 6 1 4 42.19 6.86 2.1420 -6 2 1 4 42.20 2.72 2.1417 -2 4 4 4 42.20 1.56 2.1416 -4 2 4 4 42.28 1.81 2.1377 6 2 1 4 42.29 1.67 2.1371 -2 2 5 4 42.31 5.10 2.1360 2 4 4 4 42.44 4.21 2.1300 2 2 5 4 43.36 4.27 2.0867 -1 3 5 4 43.43 6.12 2.0834 1 3 5 4 43.55 1.03 2.0784 3 1 5 4 44.80 2.77 2.0230 5 3 3 4 45.31 4.17 2.0017 -1 5 4 4 45.31 1.05 2.0015 -5 1 4 4 45.36 5.33 1.9993 1 5 4 4 45.59 7.96 1.9900 5 1 4 4 45.89 3.27 1.9775 0 0 6 2 46.42 8.97 1.9559 0 4 5 4 46.84 2.02 1.9396 -1 1 6 4 46.92 9.15 1.9364 1 1 6 4 47.22 12.40 1.9250 -5 5 1 4 47.28 6.11 1.9224 5 5 1 4 47.41 4.17 1.9177 7 1 1 4 47.52 3.36 1.9132 -2 6 3 4 47.59 13.26 1.9107 -6 2 3 4 47.60 7.39 1.9102 2 6 3 4 48.15 2.82 1.8900 -4 6 1 4 48.20 1.69 1.8880 4 6 1 4 48.23 1.77 1.8868 -4 4 4 4 48.30 2.21 1.8842 -4 2 5 4 48.44 3.39 1.8791 4 4 4 4 49.10 2.06 1.8554 1 7 2 4 49.13 1.45 1.8544 -5 5 2 4 49.18 1.27 1.8528 -3 5 4 4 49.33 1.50 1.8473 3 5 4 4 49.68 2.48 1.8351 -2 2 6 4 50.15 1.86 1.8189 -6 0 4 2 50.26 1.17 1.8154 6 4 2 4 50.71 3.34 1.8002 1 3 6 4 51.08 2.81 1.7880 -7 3 1 4 51.95 1.01 1.7602 -2 6 4 4 52.20 2.37 1.7524 -1 7 3 4 52.23 2.66 1.7515 -5 5 3 4 52.29 1.11 1.7495 -7 1 3 4 52.41 3.31 1.7457 5 5 3 4 53.02 1.06 1.7272 0 8 0 2 53.10 3.29 1.7247 -4 6 3 4 53.15 1.25 1.7232 -6 4 3 4 53.25 2.27 1.7202 4 6 3 4 53.31 2.24 1.7186 -4 0 6 2 53.39 1.66 1.7162 0 4 6 4 53.81 1.01 1.7037 -4 4 5 4 54.20 1.60 1.6924 -3 3 6 4 54.69 2.92 1.6783 -3 5 5 4 54.87 4.94 1.6732 3 5 5 4 55.03 1.00 1.6687 1 1 7 4 55.05 2.99 1.6682 8 2 0 4 55.40 2.35 1.6584 0 8 2 4 55.68 1.28 1.6507 8 2 1 4 55.83 1.82 1.6467 3 7 3 4 56.07 3.70 1.6403 7 3 3 4 56.37 4.22 1.6323 -5 5 4 4 56.41 1.32 1.6311 1 7 4 4 56.60 2.92 1.6260 5 5 4 4 56.66 2.21 1.6246 6 6 0 4 57.28 6.08 1.6084 -2 6 5 4 57.47 1.83 1.6035 8 2 2 4 57.56 4.71 1.6013 7 5 0 4 57.64 1.12 1.5991 6 2 5 4 57.75 3.42 1.5964 1 5 6 4 57.99 2.73 1.5905 5 1 6 4 58.06 1.56 1.5886 5 7 1 4 58.17 1.24 1.5859 7 5 1 4 58.31 2.55 1.5824 -3 1 7 4 58.56 1.63 1.5764 3 1 7 4 59.01 1.60 1.5652 6 6 2 4 59.71 1.07 1.5486 -3 7 4 4 59.90 1.49 1.5441 7 5 2 4 59.93 2.21 1.5434 4 8 0 4 60.07 1.10 1.5403 -8 2 3 4 60.41 1.59 1.5324 4 4 6 4 60.47 1.05 1.5311 -4 8 1 4 60.88 1.81 1.5217 0 4 7 4 61.30 1.46 1.5123 5 3 6 4 61.61 1.49 1.5054 9 1 1 4 61.63 7.77 1.5050 -6 6 3 4 61.71 1.87 1.5033 5 5 5 4 61.78 1.32 1.5017 -6 0 6 2 61.83 1.07 1.5005 6 6 3 4 61.84 1.03 1.5003 0 6 6 4 62.10 1.29 1.4947 -4 8 2 4 62.19 4.87 1.4927 4 8 2 4 62.23 1.88 1.4919 -4 6 5 4 62.47 1.43 1.4867 -7 5 3 4 62.58 1.76 1.4844 5 7 3 4 62.64 2.01 1.4831 0 0 8 2 62.70 4.07 1.4817 7 5 3 4 62.72 1.49 1.4814 4 2 7 4 63.09 1.42 1.4735 -9 1 2 4 63.40 1.02 1.4672 -2 6 6 4 63.85 1.09 1.4578 2 8 4 4 64.47 1.89 1.4453 -3 9 1 4 64.78 2.60 1.4391 -4 8 3 4 64.85 1.69 1.4377 -1 5 7 4 65.38 1.55 1.4274 -6 6 4 4 65.64 1.77 1.4224 6 6 4 4 65.74 4.28 1.4205 -2 2 8 4 67.62 3.97 1.3854 5 5 6 4 67.79 5.09 1.3824 7 7 1 4 68.08 1.46 1.3772 -6 4 6 4 68.44 1.47 1.3708 -6 8 1 4 68.46 1.35 1.3704 6 4 6 4 68.51 1.03 1.3697 6 8 1 4 68.53 1.21 1.3692 -8 6 1 4 68.62 1.04 1.3676 2 8 5 4 68.66 1.17 1.3671 -3 9 3 4 68.90 1.82 1.3628 0 4 8 4 69.11 1.46 1.3592 9 3 3 4 69.13 2.72 1.3589 4 0 8 2 69.22 1.56 1.3572 -1 9 4 4 69.24 1.46 1.3569 -7 7 2 4 69.90 1.10 1.3458 2 10 1 4 70.04 1.87 1.3433 -8 6 2 4 70.15 2.17 1.3415 -10 0 2 2 70.23 1.10 1.3402 -2 6 7 4 70.28 1.45 1.3393 10 2 1 4 70.36 1.62 1.3380 10 0 2 2 70.38 1.31 1.3378 2 6 7 4 72.66 1.82 1.3012 -8 0 6 2 72.81 2.11 1.2990 8 6 3 4 73.04 1.90 1.2954 -4 8 5 4 73.25 2.78 1.2923 4 8 5 4 73.93 2.71 1.2821 -2 10 3 4 73.95 1.56 1.2818 -5 5 7 4 74.08 1.58 1.2798 1 7 7 4 74.22 2.26 1.2777 10 4 0 4 74.31 1.14 1.2765 5 5 7 4 74.67 1.19 1.2711 -10 4 1 4 74.70 1.36 1.2708 -5 9 3 4 74.80 2.07 1.2693 -4 4 8 4 75.25 1.36 1.2627 -1 3 9 4 75.53 1.04 1.2588 -5 3 8 4 75.59 1.10 1.2579 -6 6 6 4 76.32 1.68 1.2477 10 4 2 4 76.53 1.10 1.2449 10 0 4 2 76.84 1.36 1.2406 -9 3 5 4 76.91 2.26 1.2397 -7 3 7 4 76.91 1.26 1.2396 -3 7 7 4 77.12 1.71 1.2367 3 7 7 4 77.40 1.01 1.2329 7 3 7 4 77.94 1.02 1.2258 2 6 8 4 78.36 3.47 1.2203 5 9 4 4 78.40 2.44 1.2198 3 3 9 4 78.51 1.25 1.2183 -4 8 6 4 78.56 1.53 1.2177 -8 4 6 4 79.03 1.19 1.2116 8 8 1 4 80.99 2.06 1.1872 -5 1 9 4 81.05 1.99 1.1865 0 0 10 2 81.09 1.12 1.1860 -1 5 9 4 81.12 2.53 1.1855 8 2 7 4 81.76 3.62 1.1779 -6 10 1 4 81.93 1.14 1.1759 2 10 5 4 81.93 2.38 1.1759 -10 4 4 4 82.46 1.13 1.1697 10 2 5 4 83.84 1.45 1.1539 -2 2 10 4 85.78 1.45 1.1327 0 10 6 4 85.83 1.35 1.1322 -10 0 6 2 85.98 1.43 1.1306 12 2 0 4 86.00 1.34 1.1304 0 12 2 4 87.80 1.35 1.1118 -12 2 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.