Boulangerite Skowron A, Brown I D Acta Crystallographica C46 (1990) 531-534 Refinement of the structure of boulangerite, Pb5Sb4S11 Locality: synthetic _database_code_amcsd 0010118 CELL PARAMETERS: 23.4900 21.2450 4.0200 90.000 90.000 90.000 SPACE GROUP: Pnam X-RAY WAVELENGTH: 1.541838 Cell Volume: 2006.161 Density (g/cm3): 6.111 MAX. ABS. INTENSITY / VOLUME**2: 49.06965581 RIR: 2.615 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.23 4.20 7.8783 2 2 0 4 13.06 6.66 6.7802 1 3 0 4 14.61 8.65 6.0646 2 3 0 4 17.12 1.19 5.1805 1 4 0 4 18.33 3.81 4.8394 2 4 0 4 19.35 5.75 4.5872 5 1 0 4 20.20 8.39 4.3954 3 4 0 4 21.25 1.46 4.1811 1 5 0 4 22.25 7.86 3.9956 2 5 0 4 22.51 8.18 3.9499 0 1 1 4 22.57 7.58 3.9391 4 4 0 4 22.71 4.82 3.9150 6 0 0 2 22.71 23.83 3.9149 5 3 0 4 22.83 23.24 3.8952 1 1 1 8 23.10 21.22 3.8502 6 1 0 4 23.77 11.43 3.7439 2 1 1 8 23.83 100.00 3.7346 3 5 0 4 23.97 78.06 3.7125 1 2 1 8 24.23 34.01 3.6735 6 2 0 4 24.87 1.40 3.5808 2 2 1 8 25.15 1.48 3.5408 0 6 0 2 25.48 7.49 3.4960 0 3 1 4 25.76 10.00 3.4579 1 3 1 8 25.88 12.11 3.4424 4 5 0 4 26.60 9.13 3.3507 2 3 1 8 26.90 33.50 3.3146 7 1 0 4 27.65 39.77 3.2263 3 6 0 4 27.88 3.80 3.1998 7 2 0 4 27.95 20.24 3.1923 3 3 1 8 28.10 5.79 3.1759 1 4 1 8 29.46 28.76 3.0323 4 6 0 4 29.55 8.48 3.0233 5 1 1 8 29.74 64.49 3.0040 4 3 1 8 30.13 24.82 2.9664 3 4 1 8 30.45 10.90 2.9355 5 2 1 8 30.86 2.34 2.8979 1 5 1 8 31.57 14.96 2.8339 2 5 1 8 31.61 6.28 2.8301 8 2 0 4 31.62 32.32 2.8299 3 7 0 4 31.81 53.24 2.8135 4 4 1 8 31.91 40.71 2.8047 6 0 1 4 31.91 2.22 2.8047 5 3 1 8 32.19 83.36 2.7806 6 1 1 8 32.73 1.44 2.7361 3 5 1 8 33.03 17.10 2.7118 6 2 1 8 33.23 21.57 2.6962 4 7 0 4 33.85 14.61 2.6478 5 4 1 8 34.61 2.59 2.5916 2 6 1 8 34.63 7.24 2.5902 2 8 0 4 34.92 1.19 2.5697 8 4 0 4 35.68 9.16 2.5162 3 6 1 8 35.70 1.72 2.5149 3 8 0 4 36.22 1.19 2.4801 5 5 1 8 36.70 4.66 2.4490 9 3 0 4 37.14 18.22 2.4209 7 3 1 8 37.32 1.80 2.4094 1 7 1 8 37.93 39.10 2.3723 2 7 1 8 38.32 4.87 2.3487 1 9 0 4 38.43 12.60 2.3424 9 4 0 4 38.46 4.90 2.3407 6 5 1 8 38.85 4.70 2.3179 7 4 1 8 38.92 1.81 2.3143 2 9 0 4 38.92 12.96 2.3142 8 2 1 8 38.92 1.01 2.3140 3 7 1 8 38.96 2.05 2.3118 5 8 0 4 40.10 22.01 2.2484 8 3 1 8 40.28 1.69 2.2392 4 7 1 8 40.56 4.01 2.2239 9 5 0 4 40.91 4.19 2.2060 1 8 1 8 41.47 15.02 2.1774 2 8 1 8 41.97 7.40 2.1529 5 7 1 8 42.06 19.42 2.1483 10 4 0 4 42.39 5.07 2.1321 3 8 1 8 42.55 2.40 2.1245 0 10 0 2 42.88 1.33 2.1093 5 9 0 4 43.05 1.48 2.1009 9 6 0 4 43.66 2.96 2.0731 4 8 1 8 44.05 9.78 2.0558 10 5 0 4 44.30 2.84 2.0445 11 3 0 4 44.51 10.86 2.0356 0 9 1 4 44.78 2.21 2.0239 9 4 1 8 45.11 45.33 2.0100 0 0 2 2 45.21 2.14 2.0057 2 9 1 8 45.25 8.37 2.0041 5 8 1 8 45.53 5.00 1.9922 10 2 1 8 45.86 1.80 1.9789 9 7 0 4 46.07 1.24 1.9702 8 6 1 8 46.09 3.62 1.9696 8 8 0 4 46.39 1.62 1.9575 12 0 0 2 46.94 1.51 1.9358 5 10 0 4 47.13 2.72 1.9284 6 8 1 8 47.21 2.17 1.9251 12 2 0 4 47.22 3.90 1.9249 1 11 0 4 47.26 14.28 1.9233 4 9 1 8 48.55 1.23 1.8752 3 11 0 4 48.63 8.03 1.8724 1 10 1 8 48.74 1.11 1.8685 8 7 1 8 48.76 2.60 1.8678 5 9 1 8 48.77 9.70 1.8673 6 10 0 4 48.92 45.18 1.8620 9 6 1 8 49.04 1.93 1.8576 10 7 0 4 49.06 7.20 1.8569 11 2 1 8 49.28 2.43 1.8491 7 8 1 8 49.63 1.17 1.8367 12 4 0 4 49.82 2.65 1.8303 10 5 1 8 49.89 1.09 1.8279 3 4 2 8 49.93 1.35 1.8265 3 10 1 8 50.05 1.38 1.8224 11 3 1 8 50.85 1.43 1.7956 2 5 2 8 51.01 1.35 1.7904 4 4 2 8 51.08 1.10 1.7881 6 0 2 4 51.08 4.58 1.7881 5 3 2 8 51.27 3.90 1.7818 6 1 2 8 51.29 3.60 1.7813 13 2 0 4 51.63 7.15 1.7704 0 12 0 2 51.64 20.26 1.7699 3 5 2 8 51.78 1.97 1.7654 1 12 0 4 51.85 6.96 1.7633 6 2 2 8 51.96 4.83 1.7599 12 0 1 4 51.96 5.94 1.7599 10 6 1 8 51.97 6.40 1.7595 10 8 0 4 52.15 8.01 1.7539 12 1 1 8 52.25 6.76 1.7508 13 3 0 4 52.39 3.65 1.7465 11 7 0 4 52.47 1.79 1.7441 5 10 1 8 52.59 2.31 1.7404 7 9 1 8 52.73 5.28 1.7361 1 11 1 8 52.74 2.35 1.7358 4 5 2 8 52.86 7.46 1.7321 6 11 0 4 53.13 1.08 1.7237 11 5 1 8 53.30 7.94 1.7187 7 1 2 8 53.73 9.43 1.7060 3 6 2 8 54.79 7.22 1.6754 4 6 2 8 54.84 1.40 1.6739 7 11 0 4 54.88 1.20 1.6729 8 9 1 8 54.89 2.65 1.6726 14 1 0 4 55.44 4.88 1.6573 14 2 0 4 55.46 1.02 1.6567 5 12 0 4 56.12 2.06 1.6388 8 2 2 8 56.13 9.75 1.6387 3 7 2 8 56.36 1.22 1.6324 5 11 1 8 57.16 6.49 1.6115 4 7 2 8 57.98 7.77 1.5907 6 11 1 8 58.09 2.67 1.5880 2 8 2 8 59.50 1.92 1.5537 9 3 2 8 59.85 1.69 1.5453 7 11 1 8 60.44 3.82 1.5317 5 12 1 8 60.64 1.91 1.5271 1 9 2 8 60.71 4.99 1.5254 9 4 2 8 61.54 1.64 1.5068 12 9 0 4 61.79 2.45 1.5015 2 13 1 8 62.26 1.96 1.4912 9 5 2 8 62.48 2.72 1.4865 14 4 1 8 63.10 1.08 1.4734 11 9 1 8 63.30 3.61 1.4693 7 13 0 4 63.37 8.40 1.4677 10 4 2 8 63.74 1.22 1.4601 0 10 2 4 64.00 1.52 1.4548 14 5 1 8 64.02 1.26 1.4543 16 2 0 4 64.32 2.15 1.4483 13 7 1 8 64.69 2.39 1.4409 5 13 1 8 64.86 1.19 1.4376 16 3 0 4 64.88 4.53 1.4372 10 5 2 8 65.00 1.26 1.4348 13 9 0 4 65.07 1.42 1.4333 11 3 2 8 65.35 1.86 1.4280 8 13 0 4 65.91 5.59 1.4171 1 14 1 8 66.18 2.04 1.4120 6 13 1 8 66.27 2.59 1.4104 11 10 1 8 66.28 1.04 1.4102 9 7 2 8 66.32 2.16 1.4095 2 14 1 8 66.45 5.28 1.4071 15 4 1 8 66.46 1.95 1.4068 8 8 2 8 66.99 1.05 1.3969 3 14 1 8 67.35 1.27 1.3903 12 2 2 8 67.36 1.98 1.3902 1 11 2 8 67.77 1.37 1.3827 7 14 0 4 67.92 2.84 1.3801 15 5 1 8 67.96 1.84 1.3793 14 7 1 8 68.60 5.43 1.3680 6 10 2 8 69.69 1.86 1.3493 11 11 1 8 70.39 2.75 1.3376 14 8 1 8 70.66 2.01 1.3331 13 2 2 8 70.94 4.18 1.3285 0 12 2 4 71.01 2.29 1.3273 1 2 3 8 71.07 1.15 1.3264 1 12 2 8 71.23 3.73 1.3239 10 8 2 8 71.46 3.98 1.3202 13 3 2 8 71.57 2.19 1.3183 11 7 2 8 71.91 1.56 1.3130 12 12 0 4 71.97 4.40 1.3121 6 11 2 8 71.99 2.37 1.3117 16 5 1 8 72.26 1.02 1.3075 7 14 1 8 72.47 1.64 1.3043 17 1 1 8 72.69 5.18 1.3009 12 11 1 8 73.68 1.70 1.2857 14 1 2 8 73.75 2.83 1.2847 4 3 3 8 73.95 1.39 1.2818 3 4 3 8 74.15 3.16 1.2787 14 2 2 8 74.85 2.38 1.2686 4 4 3 8 74.90 1.63 1.2678 6 0 3 4 75.06 4.68 1.2655 6 1 3 8 75.76 2.28 1.2555 16 7 1 8 76.29 2.81 1.2482 12 12 1 8 76.53 1.45 1.2448 3 16 1 8 76.69 1.83 1.2427 2 17 0 4 76.95 2.17 1.2391 18 1 1 8 77.32 1.59 1.2341 3 17 0 4 77.41 1.74 1.2328 18 2 1 8 77.42 1.51 1.2327 4 16 1 8 77.95 1.12 1.2257 7 3 3 8 78.44 2.56 1.2192 2 7 3 8 78.69 3.50 1.2159 8 15 1 8 79.45 1.10 1.2063 13 12 1 8 79.50 1.25 1.2056 12 9 2 8 79.84 1.68 1.2014 8 3 3 8 80.55 1.95 1.1925 17 9 0 4 80.74 1.34 1.1902 2 8 3 8 81.07 2.69 1.1862 7 13 2 8 82.05 1.84 1.1745 19 2 1 8 82.84 1.13 1.1653 0 9 3 4 82.94 1.49 1.1641 8 13 2 8 84.48 1.11 1.1468 20 4 0 4 84.82 1.60 1.1430 4 9 3 8 85.18 1.12 1.1392 7 14 2 8 86.06 5.31 1.1298 9 6 3 8 88.56 1.09 1.1042 12 1 3 8 89.06 1.51 1.0993 12 12 2 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.