Na9[P2W15Nb3O62].2C2H3N.23H2O Finke R G, Lyon D K, Nomiya K, Weakley T J R Acta Crystallographica C46 (1990) 1592-1596 Structure of nonasodium alpha-triniobatopentadecawolframatodiphosphate- acetonitrile-water(1/2/23), Na9[P2W15Nb3O62].2CH3CN.23H2O _database_code_amcsd 0010175 CELL PARAMETERS: 13.3410 15.8900 21.3950 87.850 77.180 71.870 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 4200.438 Density (g/cm3): 3.686 MAX. ABS. INTENSITY / VOLUME**2: 91.04431285 RIR: 8.042 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 4.24 3.29 20.8496 0 0 1 2 5.86 4.20 15.0924 0 1 0 2 7.11 33.25 12.4280 0 -1 1 2 7.15 20.86 12.3642 1 0 0 2 7.35 29.09 12.0326 0 1 1 2 7.46 100.00 11.8474 1 0 1 2 7.71 29.02 11.4705 1 1 0 2 8.48 37.87 10.4248 0 0 2 2 9.09 10.85 9.7316 -1 0 1 2 11.73 1.77 7.5462 0 2 0 2 12.02 2.55 7.3610 1 2 1 2 12.39 2.23 7.1433 1 -1 2 2 12.84 2.54 6.8966 -1 -2 1 2 13.16 1.17 6.7278 1 0 3 2 13.42 1.93 6.5973 2 1 1 2 13.69 1.27 6.4694 2 1 0 2 13.85 3.45 6.3959 0 -1 3 2 14.01 1.05 6.3206 2 0 1 2 14.21 3.09 6.2327 0 1 3 2 14.25 1.61 6.2140 0 -2 2 2 14.33 1.62 6.1821 2 0 0 2 14.46 1.15 6.1247 2 1 2 2 14.64 2.60 6.0488 -1 1 2 2 14.72 1.86 6.0163 0 2 2 2 14.96 4.15 5.9237 2 0 2 2 15.19 3.57 5.8309 -2 -1 1 2 15.45 1.49 5.7352 2 2 0 2 15.83 3.00 5.5989 -2 0 1 2 15.95 1.59 5.5558 -1 0 3 2 16.57 3.60 5.3497 2 1 3 2 16.84 3.42 5.2661 1 3 0 2 16.95 3.27 5.2296 2 0 3 2 17.01 7.51 5.2124 0 0 4 2 17.11 2.44 5.1835 -2 1 0 2 17.38 2.93 5.1029 1 1 4 2 17.54 2.27 5.0560 2 -1 2 2 18.23 2.51 4.8658 -2 0 2 2 19.32 1.14 4.5932 -1 -3 2 2 20.01 1.89 4.4378 -2 -3 1 2 21.02 1.44 4.2265 1 -3 1 2 21.41 2.14 4.1510 2 3 3 2 21.45 1.75 4.1427 0 -3 3 2 21.90 1.73 4.0584 -1 3 1 2 21.92 1.30 4.0549 0 -1 5 2 22.16 1.73 4.0109 0 3 3 2 22.40 1.62 3.9696 1 4 0 2 22.51 1.15 3.9491 3 0 3 2 22.65 11.25 3.9251 1 4 1 2 22.95 6.20 3.8746 -1 -4 1 2 23.30 1.89 3.8182 1 3 4 2 23.50 1.54 3.7862 2 4 0 2 23.57 1.51 3.7746 3 -1 1 2 23.58 1.99 3.7731 0 4 0 2 23.98 1.50 3.7104 -1 0 5 2 24.14 1.11 3.6867 -2 -1 4 2 24.39 2.08 3.6497 3 0 4 2 24.66 3.01 3.6105 -2 0 4 2 24.93 1.71 3.5719 -3 0 2 2 25.42 1.70 3.5041 -1 1 5 2 25.64 1.45 3.4749 0 0 6 2 26.24 1.51 3.3958 -1 -4 3 2 26.35 2.31 3.3826 2 1 6 2 26.50 6.59 3.3639 2 0 6 2 26.54 2.03 3.3590 -2 1 4 2 26.95 1.08 3.3082 4 1 1 2 26.99 3.23 3.3037 4 1 2 2 27.37 1.43 3.2591 1 -4 2 2 27.60 2.54 3.2321 4 1 0 2 27.60 1.73 3.2321 -3 -4 1 2 27.78 1.64 3.2111 3 4 3 2 27.86 4.09 3.2026 -2 -1 5 2 27.95 4.22 3.1923 2 -1 6 2 28.17 9.89 3.1680 1 5 0 2 28.23 6.70 3.1608 4 0 1 2 28.26 2.05 3.1579 4 3 1 2 28.32 1.04 3.1516 1 -2 6 2 28.41 2.50 3.1418 1 5 1 2 28.47 2.41 3.1353 1 -3 5 2 28.59 6.29 3.1226 2 5 1 2 28.59 1.59 3.1223 -1 -5 1 2 28.64 1.13 3.1171 -2 -2 5 2 28.71 1.27 3.1099 3 3 5 2 29.25 1.11 3.0533 -2 -5 1 2 29.29 1.51 3.0490 1 5 2 2 29.45 2.48 3.0334 -1 1 6 2 30.04 1.14 2.9750 -2 1 5 2 30.19 1.33 2.9606 2 1 7 2 30.60 1.53 2.9219 -2 -3 5 2 30.63 2.57 2.9184 4 -1 2 2 31.29 2.18 2.8586 -4 1 0 2 31.53 1.59 2.8375 3 3 6 2 31.55 1.75 2.8354 2 -1 7 2 31.62 3.58 2.8300 3 -3 1 2 31.68 3.96 2.8240 -1 3 5 2 31.77 1.41 2.8170 -2 -1 6 2 32.22 3.83 2.7779 -2 0 6 2 32.46 1.95 2.7583 3 1 7 2 33.77 2.34 2.6543 -2 1 6 2 34.02 2.23 2.6354 2 -3 6 2 34.17 2.40 2.6243 5 1 1 2 34.44 2.00 2.6043 5 3 1 2 34.56 1.40 2.5956 -3 -3 5 2 34.70 1.85 2.5854 3 3 7 2 35.01 1.44 2.5632 1 -3 7 2 35.62 2.23 2.5203 1 -4 6 2 36.03 1.45 2.4929 5 4 2 2 36.12 1.00 2.4866 5 4 1 2 36.64 1.33 2.4525 3 -4 2 2 36.85 2.27 2.4391 -3 -4 5 2 36.96 1.56 2.4319 -3 4 0 2 37.28 2.02 2.4122 3 4 7 2 38.00 1.14 2.3681 4 -3 2 2 38.71 1.14 2.3262 5 5 1 2 38.77 1.09 2.3229 -1 3 7 2 39.10 1.33 2.3038 -1 4 6 2 47.79 1.65 1.9032 6 0 7 2 51.87 1.06 1.7628 2 9 0 2 52.56 1.39 1.7412 0 -8 5 2 52.66 1.06 1.7381 4 8 6 2 52.68 2.46 1.7375 0 0 12 2 53.12 1.30 1.7241 -4 -8 4 2 53.81 1.66 1.7037 -6 0 5 2 54.03 1.31 1.6973 0 8 5 2 54.15 1.43 1.6937 6 8 2 2 54.90 1.43 1.6723 2 -8 1 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.