(NH3OH)6P6O18.4H2O Durif A, Averbuch-Pouchot M T Acta Crystallographica C46 (1990) 2026-2028 Crystal chemistry of cyclo-hexaphosphates. VIII. structure of hydroxylammonium cyclo-hexaphosphate tetrahydrate _database_code_amcsd 0010206 CELL PARAMETERS: 10.3650 9.2780 7.2800 108.390 100.300 96.020 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 643.806 Density (g/cm3): 1.894 MAX. ABS. INTENSITY / VOLUME**2: 4.162777056 RIR: 0.715 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.80 73.85 10.0447 1 0 0 2 10.20 3.23 8.6718 0 1 0 2 13.15 20.25 6.7318 0 0 1 2 13.62 100.00 6.5010 0 -1 1 2 14.10 45.06 6.2824 -1 0 1 2 15.58 49.81 5.6890 -1 -1 1 2 16.88 12.69 5.2525 1 -1 1 2 17.43 2.75 5.0886 1 0 1 2 17.66 10.80 5.0223 2 0 0 2 18.83 2.98 4.7135 -2 1 0 2 19.11 2.87 4.6438 -1 1 1 2 19.26 9.98 4.6094 0 1 1 2 20.48 7.27 4.3359 0 2 0 2 20.86 35.16 4.2575 -1 2 0 2 21.39 7.05 4.1538 -2 -1 1 2 21.86 1.47 4.0665 1 -2 1 2 21.93 1.69 4.0530 2 1 0 2 22.32 1.41 3.9824 -1 -2 1 2 23.12 2.39 3.8466 1 1 1 2 23.31 9.77 3.8165 2 -1 1 2 23.71 1.20 3.7520 1 2 0 2 24.38 5.95 3.6516 2 0 1 2 24.70 13.50 3.6044 -2 2 0 2 24.99 23.57 3.5634 -1 -1 2 2 26.48 28.71 3.3659 0 0 2 2 26.58 16.69 3.3536 2 -2 1 2 26.62 2.65 3.3482 3 0 0 2 26.84 24.04 3.3223 -3 1 0 2 26.95 31.94 3.3087 -3 0 1 2 27.34 21.72 3.2616 -1 2 1 2 27.36 1.31 3.2602 -2 -2 1 2 27.44 41.42 3.2505 0 -2 2 2 27.84 3.43 3.2045 1 -1 2 2 28.03 9.58 3.1836 0 2 1 2 28.10 1.08 3.1755 -2 -1 2 2 28.11 5.42 3.1749 -1 -2 2 2 28.41 11.48 3.1412 -2 0 2 2 28.85 2.03 3.0942 -3 1 1 2 28.91 22.13 3.0884 -3 -1 1 2 29.45 5.87 3.0331 2 2 0 2 29.51 2.75 3.0267 -2 2 1 2 29.81 13.57 2.9976 1 -3 1 2 29.83 12.02 2.9953 1 0 2 2 30.23 12.93 2.9566 3 1 0 2 30.79 2.99 2.9038 -3 2 0 2 30.94 52.78 2.8906 0 3 0 2 31.10 19.61 2.8761 3 -1 1 2 31.22 1.36 2.8653 -1 -3 1 2 31.63 10.18 2.8288 0 1 2 2 32.29 4.12 2.7722 -2 1 2 2 32.43 7.53 2.7609 3 0 1 2 32.97 1.45 2.7164 -2 3 0 2 33.18 3.19 2.7000 3 -2 1 2 33.46 6.13 2.6782 -3 -1 2 2 33.71 3.42 2.6585 1 3 0 2 34.04 9.28 2.6339 -3 2 1 2 34.13 3.39 2.6268 -3 -2 1 2 34.14 4.56 2.6262 2 -2 2 2 34.29 1.54 2.6148 -1 -3 2 2 34.63 1.46 2.5904 1 -3 2 2 35.00 9.40 2.5639 1 1 2 2 35.23 8.14 2.5475 -4 0 1 2 35.55 1.94 2.5254 -2 -3 1 2 35.76 3.58 2.5112 4 0 0 2 36.20 1.97 2.4813 -3 1 2 2 36.63 3.11 2.4530 3 2 0 2 36.78 7.94 2.4437 2 2 1 2 36.82 6.17 2.4412 -3 -2 2 2 36.85 22.83 2.4391 3 1 1 2 36.87 1.11 2.4381 -1 3 1 2 37.15 4.11 2.4201 -1 -1 3 2 37.24 2.21 2.4144 -4 -1 1 2 37.83 2.10 2.3783 0 -1 3 2 37.85 6.72 2.3771 -1 2 2 2 38.68 1.51 2.3280 -2 -1 3 2 38.78 2.21 2.3219 -2 2 2 2 39.13 2.64 2.3020 1 -4 1 2 39.67 10.32 2.2720 -4 0 2 2 40.24 2.08 2.2410 2 1 2 2 41.08 3.32 2.1971 -1 -4 1 2 41.09 2.89 2.1968 4 0 1 2 41.11 2.79 2.1958 0 -4 2 2 41.86 8.34 2.1580 1 -4 2 2 41.87 1.84 2.1575 -1 -3 3 2 42.12 1.52 2.1451 3 0 2 2 43.55 2.50 2.0780 3 2 1 2 43.58 1.74 2.0769 -4 -2 2 2 43.87 5.17 2.0637 -3 -2 3 2 44.24 4.07 2.0475 1 4 0 2 44.27 2.14 2.0461 -2 1 3 2 44.50 1.36 2.0360 -5 1 0 2 45.13 1.74 2.0089 5 0 0 2 45.16 3.10 2.0077 4 1 1 2 45.76 3.53 1.9827 -3 4 0 2 46.41 1.16 1.9564 -4 3 1 2 46.42 2.55 1.9562 -5 2 0 2 46.48 1.39 1.9537 -4 2 2 2 46.57 2.74 1.9503 -1 3 2 2 46.99 1.51 1.9337 -2 3 2 2 47.10 1.72 1.9293 2 -3 3 2 47.14 2.52 1.9279 -1 4 1 2 47.37 1.91 1.9190 -4 -1 3 2 47.66 1.35 1.9082 4 -2 2 2 47.81 2.37 1.9025 -2 4 1 2 47.97 1.07 1.8963 -3 -3 3 2 47.98 1.67 1.8963 2 0 3 2 47.98 2.38 1.8960 0 3 2 2 48.95 2.08 1.8606 3 -4 2 2 49.22 1.24 1.8511 -3 3 2 2 49.26 1.56 1.8500 -4 -2 3 2 49.95 3.22 1.8258 4 0 2 2 50.28 1.33 1.8146 0 -5 2 2 50.81 1.46 1.7969 4 -4 1 2 51.07 2.42 1.7885 0 -2 4 2 51.18 4.44 1.7850 3 -1 3 2 51.93 1.09 1.7608 -1 5 0 2 52.25 1.66 1.7508 3 -3 3 2 52.78 2.50 1.7344 -2 5 0 2 52.95 1.43 1.7292 2 1 3 2 53.12 1.34 1.7241 -1 0 4 2 53.34 3.05 1.7174 -6 0 1 2 53.93 1.47 1.7002 -3 -2 4 2 54.00 3.00 1.6982 -5 0 3 2 54.10 1.86 1.6953 -3 -4 3 2 54.73 1.41 1.6772 0 -5 3 2 55.47 1.12 1.6565 -6 -1 1 2 55.55 1.04 1.6544 -6 0 2 2 55.56 1.47 1.6541 1 -5 3 2 56.67 1.27 1.6242 -6 -1 2 2 57.87 1.84 1.5933 6 1 0 2 58.50 1.01 1.5778 -1 3 3 2 59.41 1.08 1.5557 0 1 4 2 59.85 2.83 1.5454 6 0 1 2 60.14 1.45 1.5386 -6 3 1 2 60.17 1.12 1.5379 -3 5 1 2 60.21 4.07 1.5370 1 -6 1 2 60.77 1.21 1.5241 -5 2 3 2 60.88 1.47 1.5216 6 -3 1 2 61.02 1.98 1.5184 1 4 2 2 61.34 1.36 1.5112 -6 -1 3 2 61.74 1.43 1.5026 3 3 2 2 61.85 1.43 1.5000 -3 -5 3 2 62.25 1.48 1.4913 -4 1 4 2 62.39 1.53 1.4883 0 -5 4 2 63.87 1.02 1.4575 -2 6 0 2 64.39 1.26 1.4470 -2 -5 4 2 64.60 1.03 1.4427 -1 -6 3 2 65.38 1.18 1.4273 6 -1 2 2 65.68 2.98 1.4217 3 2 3 2 66.98 1.31 1.3972 -5 3 3 2 67.14 1.24 1.3942 4 -5 3 2 68.04 1.70 1.3779 7 1 0 2 69.17 1.11 1.3582 -4 6 0 2 71.01 1.29 1.3274 -3 -4 5 2 71.29 1.24 1.3229 1 -7 2 2 76.50 1.09 1.2452 6 3 1 2 76.78 1.03 1.2414 3 -3 5 2 78.50 1.02 1.2184 -2 -7 1 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.