H26 O40 P6 Rb6 Te3 Averbuch-Pouchot M, Durif A Acta Crystallographica C47 (1991) 1576-1579 Crystal chemistry of cyclo-hexaphosphates. XVI. Structures of potassium cyclo-hexaphosphate ditellurate trihydrate and rubidium cyclo- hexaphosphate tritellurate tetrahydrate _cod_database_code 1007197 _database_code_amcsd 0010260 CELL PARAMETERS: 11.2220 8.0770 11.7310 111.110 104.660 83.250 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 959.238 Density (g/cm3): 3.025 MAX. ABS. INTENSITY / VOLUME**2: 13.23552894 RIR: 1.425 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.15 1.93 10.8520 1 0 0 2 10.23 7.88 8.6508 -1 0 1 2 11.75 2.04 7.5317 0 1 0 2 11.83 8.56 7.4819 0 -1 1 2 12.90 17.72 6.8630 1 0 1 2 13.04 1.59 6.7875 -1 -1 1 2 14.12 32.34 6.2740 1 1 0 2 14.51 12.79 6.1045 -1 1 0 2 15.60 1.73 5.6792 1 -1 1 2 16.34 9.22 5.4260 2 0 0 2 16.64 10.03 5.3284 0 0 2 2 16.73 30.64 5.2986 -1 -1 2 2 16.75 5.81 5.2918 0 -1 2 2 17.80 7.84 4.9828 -1 1 1 2 19.98 11.65 4.4438 2 0 1 2 20.17 14.20 4.4031 1 0 2 2 20.35 5.88 4.3640 -2 -1 2 2 20.40 100.00 4.3525 1 -1 2 2 20.45 2.06 4.3427 -2 1 0 2 20.53 30.74 4.3254 -2 0 2 2 21.98 6.27 4.0446 2 -1 1 2 22.17 1.93 4.0103 0 -2 1 2 22.23 15.96 3.9990 -2 1 1 2 22.72 32.22 3.9131 -1 -2 1 2 23.05 1.39 3.8593 -1 -1 3 2 23.54 5.23 3.7799 0 1 2 2 23.63 34.47 3.7659 0 2 0 2 23.65 2.79 3.7623 -1 -2 2 2 23.74 6.36 3.7485 0 -1 3 2 23.76 13.62 3.7443 -1 1 2 2 23.79 36.80 3.7409 0 -2 2 2 24.12 9.79 3.6904 -3 0 1 2 24.44 13.90 3.6416 2 1 1 2 24.53 5.27 3.6289 -1 0 3 2 24.61 6.70 3.6173 3 0 0 2 24.80 6.96 3.5904 1 2 0 2 25.07 25.31 3.5523 0 0 3 2 25.20 6.85 3.5334 -2 -1 3 2 25.24 17.98 3.5281 -3 -1 1 2 25.26 4.05 3.5260 -1 2 0 2 25.97 6.64 3.4315 2 0 2 2 26.08 27.65 3.4173 1 1 2 2 26.19 20.28 3.4024 -3 -1 2 2 26.26 1.52 3.3938 -2 -2 2 2 26.45 19.05 3.3703 -3 0 2 2 26.69 13.92 3.3406 -2 0 3 2 26.69 5.64 3.3399 -2 1 2 2 27.03 11.78 3.2986 3 1 0 2 27.07 1.63 3.2937 1 -1 3 2 27.28 1.89 3.2686 -1 -2 3 2 27.67 34.72 3.2242 -3 1 0 2 27.71 9.89 3.2198 0 2 1 2 27.98 1.46 3.1888 0 -2 3 2 28.15 1.24 3.1695 1 0 3 2 28.45 19.59 3.1370 2 2 0 2 28.47 22.26 3.1347 -3 1 1 2 28.57 15.09 3.1243 -1 2 1 2 29.05 11.57 3.0738 -2 -2 3 2 29.19 1.73 3.0589 2 -2 1 2 29.26 3.20 3.0522 -2 2 0 2 29.28 3.46 3.0506 1 2 1 2 29.38 2.12 3.0396 3 -1 1 2 30.48 6.22 2.9326 -1 -1 4 2 30.98 15.67 2.8870 -3 -2 2 2 30.98 5.47 2.8869 -1 1 3 2 30.99 2.12 2.8859 1 -2 3 2 31.32 6.01 2.8562 0 1 3 2 31.53 1.01 2.8371 0 -1 4 2 31.67 14.59 2.8251 -2 -1 4 2 32.30 1.03 2.7717 2 -1 3 2 32.74 4.14 2.7355 -1 0 4 2 32.80 1.09 2.7301 -1 -2 4 2 32.83 2.57 2.7280 -2 1 3 2 32.92 8.93 2.7210 -3 -2 3 2 32.93 3.40 2.7204 -4 -1 1 2 32.94 2.26 2.7192 3 0 2 2 32.96 6.58 2.7173 2 2 1 2 33.14 6.47 2.7035 2 0 3 2 33.19 9.23 2.6994 -4 -1 2 2 33.27 4.75 2.6930 3 -1 2 2 33.64 1.15 2.6642 0 0 4 2 33.65 3.53 2.6637 -1 -3 2 2 33.80 5.84 2.6522 1 1 3 2 33.83 1.75 2.6495 0 -3 2 2 33.83 8.91 2.6493 -2 -2 4 2 33.88 1.05 2.6459 0 -2 4 2 33.94 2.74 2.6409 -2 0 4 2 34.82 11.99 2.5766 4 1 0 2 34.89 4.34 2.5715 -3 2 0 2 34.90 7.56 2.5709 -3 -1 4 2 35.37 2.16 2.5374 -1 -3 3 2 35.49 1.16 2.5292 1 -3 1 2 35.50 1.15 2.5290 -4 1 0 2 35.78 4.08 2.5096 2 -2 3 2 35.97 3.15 2.4968 4 0 1 2 36.01 8.13 2.4940 0 -3 3 2 36.03 5.84 2.4925 1 -3 2 2 36.05 1.55 2.4914 -2 2 2 2 36.33 1.21 2.4727 -2 -3 1 2 36.51 1.22 2.4610 1 0 4 2 36.54 1.47 2.4591 -3 2 1 2 36.58 1.67 2.4563 -3 1 3 2 36.83 10.24 2.4407 3 1 2 2 36.90 6.70 2.4361 1 -2 4 2 36.99 6.58 2.4304 -1 3 0 2 37.08 2.76 2.4247 -3 0 4 2 37.08 4.58 2.4245 -4 -2 2 2 37.71 1.63 2.3852 3 -2 2 2 38.04 2.90 2.3654 2 1 3 2 38.51 1.35 2.3375 -1 -1 5 2 38.54 2.86 2.3362 1 -3 3 2 38.75 2.12 2.3241 3 -1 3 2 39.04 20.65 2.3071 2 -3 1 2 39.39 4.56 2.2877 3 0 3 2 39.52 1.11 2.2802 -1 -2 5 2 39.80 3.33 2.2651 -2 -3 4 2 39.80 2.16 2.2651 0 -1 5 2 39.96 2.58 2.2562 2 -3 2 2 39.99 1.26 2.2547 -2 -2 5 2 39.99 3.15 2.2547 -2 1 4 2 40.03 2.83 2.2523 -3 2 2 2 40.32 1.79 2.2368 -1 3 1 2 40.33 8.16 2.2364 -3 -3 1 2 40.60 6.25 2.2219 4 0 2 2 40.95 4.85 2.2038 4 -1 2 2 41.00 14.37 2.2015 2 0 4 2 41.06 1.08 2.1985 -5 -1 1 2 41.49 6.94 2.1763 2 -2 4 2 41.61 2.41 2.1704 5 0 0 2 41.77 1.34 2.1627 -4 0 4 2 41.80 2.97 2.1612 -4 1 3 2 41.83 6.36 2.1597 -2 2 3 2 41.83 1.00 2.1593 3 -2 3 2 41.86 2.63 2.1579 -2 0 5 2 42.34 5.71 2.1345 -3 -3 4 2 42.35 3.38 2.1344 4 -2 1 2 42.41 1.28 2.1314 0 0 5 2 42.71 1.61 2.1172 1 -3 4 2 42.78 6.16 2.1139 1 -1 5 2 42.81 5.91 2.1122 -3 1 4 2 43.03 2.45 2.1020 5 1 0 2 43.26 6.51 2.0913 3 3 0 2 43.47 2.13 2.0819 2 3 1 2 43.65 2.06 2.0738 -5 0 3 2 43.96 2.22 2.0596 3 2 2 2 44.08 1.40 2.0545 -1 -3 5 2 44.45 1.63 2.0380 5 0 1 2 44.53 1.95 2.0348 -3 3 0 2 44.61 5.57 2.0314 4 2 1 2 44.82 7.17 2.0223 4 -2 2 2 44.89 4.33 2.0191 0 3 2 2 45.12 1.29 2.0095 -5 -2 1 2 45.24 6.27 2.0043 3 -3 2 2 45.27 5.14 2.0031 -4 -1 5 2 45.36 5.81 1.9995 -4 2 2 2 45.75 10.42 1.9832 -5 -1 4 2 45.95 1.69 1.9749 -4 -2 5 2 46.15 1.38 1.9670 0 -4 3 2 46.25 6.57 1.9630 1 3 2 2 46.41 7.74 1.9566 -2 -4 2 2 46.59 2.49 1.9496 -2 -4 3 2 46.61 1.64 1.9485 5 1 1 2 46.69 3.92 1.9454 -3 3 1 2 46.98 4.05 1.9339 -1 -1 6 2 47.05 6.45 1.9312 -1 -2 6 2 47.10 2.82 1.9296 -2 -2 6 2 47.10 1.30 1.9296 -4 1 4 2 47.24 3.59 1.9240 -1 1 5 2 47.84 1.51 1.9012 -2 1 5 2 48.15 1.01 1.8900 0 2 4 2 48.34 7.48 1.8829 0 4 0 2 48.63 1.33 1.8722 -2 2 4 2 48.68 2.41 1.8705 0 -4 4 2 48.69 1.67 1.8701 4 3 0 2 48.76 1.11 1.8677 -3 -1 6 2 48.77 1.11 1.8671 5 0 2 2 49.37 1.57 1.8460 2 0 5 2 49.39 6.27 1.8452 -6 0 2 2 50.10 2.46 1.8208 4 2 2 2 50.20 3.98 1.8174 1 2 4 2 50.23 1.68 1.8164 -4 3 0 2 50.25 1.96 1.8157 -5 -3 3 2 50.29 3.68 1.8144 -2 0 6 2 50.32 1.64 1.8133 -1 -3 6 2 50.36 3.11 1.8121 -3 3 2 2 50.72 4.14 1.7998 3 2 3 2 51.09 1.41 1.7877 1 -4 4 2 51.36 1.15 1.7789 1 -1 6 2 51.45 1.27 1.7761 0 0 6 2 51.54 1.17 1.7732 5 1 2 2 51.67 3.47 1.7689 -5 -3 4 2 51.74 5.31 1.7667 -4 -2 6 2 51.82 2.08 1.7643 5 2 1 2 51.83 2.45 1.7640 -6 -2 2 2 51.86 1.58 1.7629 -4 -1 6 2 52.37 2.02 1.7471 -6 1 0 2 52.57 3.65 1.7409 -5 1 4 2 52.64 2.45 1.7387 0 -4 5 2 52.79 2.12 1.7341 -1 4 1 2 53.06 2.33 1.7260 -6 -2 1 2 53.33 2.03 1.7178 3 3 2 2 53.39 3.46 1.7159 -3 -4 5 2 53.40 1.54 1.7158 4 0 4 2 53.64 1.60 1.7086 2 2 4 2 53.89 4.72 1.7012 -6 -2 4 2 54.05 1.96 1.6967 4 -2 4 2 54.26 1.87 1.6906 3 4 0 2 54.31 1.27 1.6890 5 0 3 2 54.73 2.40 1.6770 3 0 5 2 54.85 1.30 1.6737 2 -4 4 2 54.97 3.68 1.6703 -4 0 6 2 55.25 1.01 1.6626 -6 1 3 2 55.73 2.23 1.6493 6 2 0 2 55.82 3.51 1.6469 2 -2 6 2 56.05 1.34 1.6406 -3 -2 7 2 56.06 1.20 1.6404 -1 1 6 2 56.29 2.21 1.6343 -2 -4 6 2 56.66 3.04 1.6246 3 -4 3 2 56.88 2.55 1.6187 -5 3 0 2 57.14 1.45 1.6121 -6 2 0 2 57.22 1.05 1.6099 0 4 2 2 57.33 2.04 1.6072 -6 2 1 2 57.41 1.84 1.6052 6 0 2 2 57.49 1.24 1.6031 0 -1 7 2 57.70 1.12 1.5978 -7 -1 2 2 58.31 4.66 1.5824 -1 -5 4 2 58.76 4.14 1.5715 -5 -3 6 2 58.91 1.22 1.5677 2 -3 6 2 58.93 2.05 1.5673 -6 2 2 2 58.95 3.08 1.5668 -5 -4 2 2 59.09 1.84 1.5633 -2 3 4 2 59.14 1.57 1.5622 -2 4 2 2 59.14 1.10 1.5621 2 -4 5 2 59.17 5.99 1.5614 1 -5 2 2 59.75 1.33 1.5478 1 1 6 2 59.85 3.04 1.5453 5 -1 4 2 60.09 2.03 1.5398 -7 -2 3 2 60.21 1.19 1.5369 -4 -4 6 2 60.30 2.17 1.5349 1 3 4 2 60.34 2.12 1.5339 -6 -3 5 2 60.36 1.53 1.5335 4 -2 5 2 60.54 1.30 1.5294 4 -4 2 2 60.63 2.37 1.5273 7 1 0 2 60.68 2.92 1.5261 -4 4 0 2 60.91 1.24 1.5209 -3 -5 2 2 60.93 2.32 1.5204 3 -1 6 2 60.96 1.37 1.5198 6 -2 2 2 61.36 1.49 1.5109 -3 3 4 2 61.41 2.01 1.5098 -7 1 0 2 61.73 2.42 1.5028 5 -3 3 2 62.40 1.86 1.4883 6 3 0 2 63.06 1.02 1.4742 -5 -1 7 2 63.49 1.76 1.4652 2 1 6 2 64.01 1.68 1.4547 -6 1 5 2 64.04 3.58 1.4540 4 2 4 2 64.07 1.34 1.4534 4 -3 5 2 64.08 1.13 1.4531 0 -4 7 2 64.08 1.76 1.4531 7 1 1 2 64.19 1.07 1.4508 3 -3 6 2 64.44 1.04 1.4459 1 -5 5 2 64.49 1.82 1.4448 -5 3 3 2 64.56 2.97 1.4434 -2 2 6 2 64.58 1.63 1.4431 5 1 4 2 64.59 1.41 1.4430 2 -4 6 2 65.20 1.13 1.4309 -7 -3 2 2 65.24 1.79 1.4302 -1 -1 8 2 65.28 1.00 1.4293 -4 -5 5 2 65.32 2.05 1.4285 -6 -4 2 2 65.42 1.35 1.4265 -1 -3 8 2 65.48 1.19 1.4255 -3 -3 8 2 65.50 1.65 1.4250 -3 -1 8 2 65.77 1.34 1.4198 4 -4 4 2 65.84 1.79 1.4186 0 -2 8 2 65.95 1.08 1.4165 5 -3 4 2 66.05 2.60 1.4145 -6 2 4 2 66.15 1.43 1.4125 -4 -2 8 2 66.54 1.83 1.4053 3 5 0 2 66.71 1.00 1.4021 -5 4 0 2 67.29 1.44 1.3914 0 -3 8 2 67.39 1.39 1.3895 -4 -3 8 2 67.59 1.08 1.3861 2 0 7 2 67.98 1.40 1.3789 -5 -5 4 2 68.13 1.74 1.3764 -3 5 0 2 68.21 1.06 1.3749 -7 -1 6 2 68.83 1.10 1.3640 -4 2 6 2 69.14 2.92 1.3587 4 4 2 2 69.35 1.32 1.3550 -7 2 3 2 69.50 1.20 1.3525 -5 3 4 2 69.67 1.12 1.3497 -8 -2 4 2 69.93 1.03 1.3452 7 -2 2 2 70.35 1.16 1.3382 -8 0 4 2 70.74 1.28 1.3319 -2 -6 4 2 71.18 1.00 1.3247 -4 -4 8 2 71.50 2.86 1.3194 1 5 2 2 73.41 1.44 1.2898 7 2 2 2 74.17 1.01 1.2784 1 -5 7 2 74.43 1.55 1.2747 -2 -1 9 2 74.53 1.41 1.2732 -1 3 6 2 74.73 1.25 1.2702 2 4 4 2 75.27 2.83 1.2624 -1 1 8 2 75.60 1.08 1.2578 -8 -1 6 2 75.91 1.02 1.2534 -8 -3 1 2 76.43 1.42 1.2463 2 -6 4 2 77.46 1.16 1.2322 3 -5 6 2 77.59 1.36 1.2305 2 0 8 2 77.66 1.10 1.2295 -6 4 2 2 77.72 1.39 1.2287 5 -3 6 2 78.07 1.37 1.2241 -4 -6 6 2 78.53 1.07 1.2181 2 -4 8 2 78.59 1.04 1.2173 1 -2 9 2 78.98 1.87 1.2122 -8 -4 4 2 79.13 1.22 1.2104 5 3 4 2 79.13 1.26 1.2103 -7 -2 8 2 79.44 1.43 1.2064 -3 -6 7 2 79.88 1.76 1.2009 -9 1 2 2 79.90 1.12 1.2006 3 -3 8 2 81.21 1.88 1.1845 5 1 6 2 81.87 1.10 1.1766 -8 3 1 2 82.15 1.11 1.1733 -7 -5 6 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.