Ag9 H8 N2 Na O34 P8 Averbuch-Pouchot M, Durif A Acta Crystallographica C48 (1992) 1173-1176 Structure of nonasilver sodium cyclooctaphosphate dinitrate tetrahydrate: Ag9NaP8O24(NO3)2 . 4H2O _cod_database_code 1007200 _database_code_amcsd 0010273 CELL PARAMETERS: 17.2540 7.5430 23.4650 90.000 90.000 90.000 SPACE GROUP: Cmcm X-RAY WAVELENGTH: 1.541838 Cell Volume: 3053.897 Density (g/cm3): 3.944 MAX. ABS. INTENSITY / VOLUME**2: 19.30827068 RIR: 1.594 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.54 17.44 11.7325 0 0 2 2 10.25 22.55 8.6270 2 0 0 2 12.74 44.55 6.9503 2 0 2 4 12.81 14.01 6.9114 1 1 0 4 13.36 36.42 6.6298 1 1 1 8 14.88 8.95 5.9550 1 1 2 8 17.12 25.21 5.1792 1 1 3 8 18.29 35.26 4.8510 2 0 4 4 19.78 2.14 4.4891 3 1 1 8 20.85 5.53 4.2612 3 1 2 8 21.95 3.46 4.0485 4 0 2 4 22.52 1.84 3.9481 3 1 3 8 23.59 3.47 3.7715 0 2 0 2 23.90 8.87 3.7237 0 2 1 4 24.68 9.86 3.6069 3 1 4 8 24.80 30.61 3.5905 0 2 2 4 25.00 19.14 3.5619 2 0 6 4 25.63 8.90 3.4752 4 0 4 4 25.78 18.84 3.4557 2 2 0 4 26.06 27.17 3.4188 2 2 1 8 26.18 15.07 3.4037 1 1 6 8 26.23 5.99 3.3972 0 2 3 4 26.90 16.00 3.3149 2 2 2 8 27.23 31.13 3.2754 3 1 5 8 28.23 2.70 3.1609 2 2 3 8 28.44 30.43 3.1380 5 1 0 4 28.70 100.00 3.1103 5 1 1 8 29.47 9.71 3.0315 5 1 2 8 29.62 57.32 3.0161 1 1 7 8 30.01 1.12 2.9775 2 2 4 8 30.06 27.68 2.9723 3 1 6 8 30.41 9.68 2.9398 0 2 5 4 30.48 10.86 2.9331 0 0 8 2 30.86 37.35 2.8973 4 0 6 4 31.75 32.49 2.8187 4 2 1 8 32.05 3.54 2.7930 6 0 2 4 32.17 62.32 2.7827 2 2 5 8 32.23 1.89 2.7770 2 0 8 4 32.44 21.33 2.7596 4 2 2 8 32.99 5.90 2.7148 0 2 6 4 33.13 3.30 2.7037 3 1 7 8 33.18 3.21 2.7000 1 1 8 8 33.58 15.97 2.6689 4 2 3 8 34.64 1.28 2.5896 2 2 6 8 34.74 13.27 2.5821 6 0 4 4 35.11 1.03 2.5557 4 2 4 8 35.84 2.34 2.5055 0 2 7 4 36.10 17.03 2.4881 1 3 0 4 36.31 5.80 2.4742 1 3 1 8 36.39 19.46 2.4690 3 1 8 8 36.72 18.68 2.4475 5 1 6 8 36.93 5.99 2.4339 1 3 2 8 37.37 1.93 2.4061 2 2 7 8 37.95 2.80 2.3710 1 3 3 8 38.36 16.75 2.3465 0 0 10 2 38.42 4.13 2.3429 7 1 0 4 38.62 5.34 2.3313 7 1 1 8 38.87 5.68 2.3168 6 0 6 4 38.90 4.09 2.3153 0 2 8 4 39.21 14.25 2.2976 4 2 6 8 39.21 1.45 2.2976 7 1 2 8 39.30 12.47 2.2928 3 3 1 8 39.40 1.84 2.2868 6 2 0 4 39.60 2.85 2.2760 6 2 1 8 39.80 2.11 2.2650 3 1 9 8 39.81 2.58 2.2642 2 0 10 4 39.88 11.25 2.2606 3 3 2 8 40.18 1.04 2.2445 6 2 2 8 40.18 6.97 2.2444 7 1 3 8 40.60 2.28 2.2219 1 1 10 8 40.83 1.37 2.2099 3 3 3 8 41.13 1.48 2.1949 6 2 3 8 41.50 5.14 2.1758 7 1 4 8 41.69 8.35 2.1665 4 2 7 8 41.89 2.54 2.1567 8 0 0 2 42.13 13.40 2.1447 0 2 9 4 42.14 16.41 2.1444 3 3 4 8 42.17 8.62 2.1428 5 1 8 8 42.43 1.20 2.1306 6 2 4 8 43.16 20.10 2.0962 7 1 5 8 43.48 3.87 2.0813 2 2 9 8 43.93 2.88 2.0612 4 0 10 4 44.05 9.80 2.0557 6 2 5 8 44.10 1.06 2.0534 6 0 8 4 44.41 5.27 2.0400 4 2 8 8 44.45 1.16 2.0383 1 1 11 8 44.59 2.92 2.0321 5 3 0 4 44.77 1.54 2.0243 8 0 4 4 45.11 1.54 2.0099 7 1 6 8 45.22 31.30 2.0054 5 1 9 8 45.40 1.77 1.9979 1 3 7 8 45.53 4.59 1.9924 0 2 10 4 45.97 1.87 1.9741 6 2 6 8 46.15 7.21 1.9668 5 3 3 8 46.44 1.37 1.9554 0 0 12 2 47.00 1.34 1.9332 3 1 11 8 47.34 11.79 1.9204 4 2 9 8 47.34 1.20 1.9204 7 1 7 8 47.34 2.70 1.9202 5 3 4 8 47.69 2.34 1.9070 2 0 12 4 48.17 1.61 1.8891 6 2 7 8 48.18 1.80 1.8886 8 0 6 4 48.44 1.14 1.8792 5 1 10 8 48.63 3.86 1.8722 8 2 0 4 48.84 8.70 1.8648 5 3 5 8 49.03 2.76 1.8580 9 1 0 4 49.48 1.41 1.8423 2 4 0 4 49.68 1.56 1.8352 9 1 2 8 50.12 10.23 1.8200 2 4 2 8 50.26 9.60 1.8152 2 2 11 8 50.49 10.99 1.8077 9 1 3 8 50.61 2.53 1.8034 6 2 8 8 50.62 1.22 1.8032 5 3 6 8 50.72 3.00 1.8000 1 3 9 8 50.78 3.96 1.7980 3 1 12 8 50.86 9.03 1.7953 0 4 4 4 51.22 4.25 1.7836 8 2 4 8 51.30 2.85 1.7810 4 0 12 4 51.60 2.35 1.7713 9 1 4 8 52.03 10.30 1.7576 2 4 4 8 52.11 1.09 1.7552 7 3 1 8 52.28 1.70 1.7498 0 4 5 4 52.51 4.41 1.7427 7 1 9 8 52.58 3.74 1.7407 7 3 2 8 52.63 2.63 1.7390 8 2 5 8 52.67 4.04 1.7377 5 3 7 8 53.00 8.66 1.7279 4 4 0 4 53.01 4.83 1.7276 9 1 5 8 53.05 1.82 1.7264 3 3 9 8 53.08 7.18 1.7254 10 0 0 2 53.43 1.90 1.7149 2 4 5 8 53.69 3.16 1.7071 1 3 10 8 53.75 1.14 1.7055 4 2 11 8 53.98 5.90 1.6986 0 4 6 4 54.42 7.21 1.6859 7 3 4 8 54.67 4.13 1.6790 3 1 13 8 54.69 1.29 1.6783 9 1 6 8 55.11 1.28 1.6666 2 4 6 8 55.42 2.53 1.6580 7 1 10 8 55.78 9.26 1.6480 7 3 5 8 55.88 12.38 1.6453 2 0 14 4 55.93 2.94 1.6439 3 3 10 8 55.95 2.51 1.6435 0 4 7 4 56.64 7.08 1.6251 9 1 7 8 57.04 2.17 1.6145 2 4 7 8 57.20 3.03 1.6104 4 2 12 8 57.61 3.18 1.5999 2 2 13 8 58.09 5.12 1.5879 8 0 10 4 58.48 1.78 1.5781 8 2 8 8 58.52 7.54 1.5773 7 1 11 8 58.66 2.24 1.5737 3 1 14 8 58.86 1.35 1.5690 10 2 0 4 59.00 1.73 1.5655 10 2 1 8 59.01 1.59 1.5652 3 3 11 8 59.04 1.70 1.5646 5 1 13 8 59.23 1.61 1.5601 2 4 8 8 59.24 1.93 1.5599 6 2 11 8 59.83 1.72 1.5458 6 4 3 8 60.19 1.99 1.5374 1 3 12 8 60.25 8.24 1.5361 5 3 10 8 60.41 1.16 1.5324 11 1 1 8 60.44 4.97 1.5316 0 2 14 4 60.70 2.48 1.5257 1 1 15 8 60.75 6.48 1.5245 9 3 0 4 60.83 5.56 1.5227 11 1 2 8 60.89 2.63 1.5213 9 3 1 8 61.32 1.09 1.5118 9 3 2 8 61.43 1.13 1.5093 7 3 8 8 61.86 1.06 1.4998 1 5 1 8 62.09 1.22 1.4948 6 4 5 8 62.37 2.50 1.4887 4 4 8 8 62.45 2.53 1.4872 10 0 8 4 62.52 3.22 1.4856 11 1 4 8 62.78 1.73 1.4801 3 1 15 8 62.86 1.56 1.4784 5 1 14 8 63.26 2.20 1.4699 0 4 10 4 63.62 1.18 1.4625 6 4 6 8 63.77 2.16 1.4595 11 1 5 8 63.80 1.16 1.4588 7 3 9 8 63.91 3.24 1.4567 9 1 10 8 63.93 1.51 1.4562 10 2 6 8 64.28 3.33 1.4490 2 4 10 8 64.49 2.16 1.4450 0 2 15 4 64.72 1.06 1.4403 4 4 9 8 65.02 1.24 1.4345 3 5 3 8 65.18 1.23 1.4313 1 5 5 8 65.39 1.43 1.4272 12 0 2 4 65.50 2.31 1.4251 2 2 15 8 65.71 1.36 1.4210 10 2 7 8 65.74 2.04 1.4204 9 3 6 8 65.97 1.20 1.4161 3 5 4 8 66.32 3.06 1.4094 8 4 2 8 66.34 1.26 1.4090 5 3 12 8 66.44 1.51 1.4071 8 2 11 8 67.03 1.67 1.3962 11 1 7 8 67.18 2.15 1.3934 3 5 5 8 67.30 3.94 1.3913 4 4 10 8 67.37 1.07 1.3901 10 0 10 4 67.45 3.65 1.3885 4 0 16 4 68.33 1.08 1.3728 5 5 2 8 68.88 3.30 1.3632 7 1 14 8 68.99 3.67 1.3612 5 5 3 8 69.21 2.14 1.3574 0 4 12 4 69.33 1.88 1.3553 3 3 14 8 69.51 1.04 1.3523 8 2 12 8 69.68 2.35 1.3495 5 3 13 8 69.92 4.45 1.3454 5 5 4 8 69.98 1.96 1.3443 10 2 9 8 70.16 1.56 1.3413 12 2 1 8 70.37 1.71 1.3380 3 5 7 8 70.56 1.26 1.3348 12 2 2 8 70.58 2.46 1.3344 8 4 6 8 71.72 4.44 1.3160 9 3 9 8 72.47 1.31 1.3043 10 2 10 8 72.61 3.00 1.3020 1 5 9 8 72.68 2.03 1.3010 7 1 15 8 73.29 3.52 1.2916 12 2 5 8 73.74 1.42 1.2848 7 5 1 8 74.18 2.16 1.2784 9 3 10 8 74.21 2.99 1.2779 5 5 7 8 74.88 1.08 1.2681 6 4 11 8 75.77 1.34 1.2554 0 6 1 4 76.16 1.66 1.2500 0 6 2 4 76.81 3.18 1.2409 7 5 5 8 76.86 1.27 1.2403 9 3 11 8 76.90 1.05 1.2398 2 4 14 8 76.91 3.52 1.2396 5 3 15 8 76.94 1.59 1.2392 3 5 10 8 77.29 1.47 1.2345 6 2 16 8 77.44 1.11 1.2324 14 0 0 2 77.47 1.29 1.2321 0 2 18 4 77.93 1.99 1.2260 12 0 10 4 78.21 1.11 1.2223 7 5 6 8 78.79 1.27 1.2146 8 4 10 8 78.86 1.15 1.2138 7 3 14 8 79.39 1.16 1.2070 4 6 0 4 79.46 2.28 1.2061 14 0 4 4 79.60 1.01 1.2044 3 5 11 8 79.75 1.66 1.2025 2 6 5 8 80.20 1.22 1.1968 0 6 6 4 80.21 2.66 1.1967 9 1 15 8 80.82 2.72 1.1892 5 3 16 8 81.25 2.65 1.1840 9 5 1 8 82.11 1.91 1.1737 13 3 0 4 82.12 1.75 1.1737 0 2 19 4 82.16 1.82 1.1732 0 0 20 2 82.43 1.30 1.1700 14 2 1 8 82.49 1.06 1.1693 7 3 15 8 82.53 1.69 1.1689 4 6 5 8 82.56 2.20 1.1685 13 1 9 8 83.08 1.10 1.1625 2 0 20 4 83.24 1.02 1.1607 13 3 3 8 83.51 3.50 1.1577 0 4 16 4 83.75 1.09 1.1549 1 5 13 8 84.08 1.39 1.1512 9 1 16 8 84.26 2.97 1.1492 5 1 19 8 84.32 1.72 1.1485 6 4 14 8 85.80 1.15 1.1325 4 2 19 8 86.20 1.77 1.1282 7 5 10 8 86.78 2.31 1.1223 12 4 4 8 86.78 2.23 1.1222 14 2 6 8 88.68 1.51 1.1031 1 1 21 8 88.80 1.56 1.1018 7 5 11 8 88.97 1.36 1.1002 11 3 12 8 89.25 1.78 1.0974 12 4 6 8 89.27 2.87 1.0972 5 3 18 8 89.47 1.09 1.0953 4 6 9 8 89.76 1.05 1.0925 7 1 19 8 89.89 1.49 1.0913 12 0 14 4 89.91 1.53 1.0911 14 0 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.