Rinneite Figgis B N, Sobolev A N, Kucharski E S, Broughton V Acta Crystallographica C56 (2000) e228-e229 Rinneite, K3Na[FeCl6], at 293, 84 and 9.5 K Locality: synthetic Sample: T = 84 _database_code_amcsd 0010320 CELL PARAMETERS: 11.9220 11.9220 13.7610 90.000 90.000 120.000 SPACE GROUP: R-3c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1693.865 Density (g/cm3): 2.404 MAX. ABS. INTENSITY / VOLUME**2: 15.79988551 RIR: 2.140 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.86 33.02 5.9610 1 1 0 6 15.48 52.33 5.7256 0 1 2 6 21.52 3.00 4.1293 2 0 2 6 23.70 4.84 3.7543 2 1 1 12 24.49 11.15 3.6353 1 1 3 12 25.89 24.99 3.4416 3 0 0 6 27.32 8.32 3.2638 1 0 4 6 29.98 4.75 2.9805 2 2 0 6 31.24 18.84 2.8628 0 2 4 6 31.92 60.83 2.8035 1 3 1 12 33.91 30.80 2.6437 3 1 2 12 34.76 55.98 2.5806 2 1 4 12 35.93 100.00 2.4992 2 2 3 12 38.57 4.90 2.3343 3 2 1 12 39.28 10.77 2.2935 0 0 6 2 40.02 7.78 2.2530 4 1 0 12 40.09 7.43 2.2491 1 2 5 12 40.27 2.97 2.2397 2 3 2 12 41.01 8.67 2.2009 1 3 4 12 42.22 6.09 2.1405 1 1 6 12 43.85 3.46 2.0647 4 0 4 6 44.82 1.12 2.0223 1 4 3 12 45.66 5.02 1.9870 3 3 0 6 45.72 2.70 1.9843 3 1 5 12 46.55 30.97 1.9510 3 2 4 12 47.65 1.81 1.9085 3 0 6 6 48.50 3.10 1.8772 4 2 2 12 49.60 8.32 1.8378 5 1 1 12 50.19 10.94 1.8176 2 2 6 12 50.86 1.09 1.7953 2 3 5 12 51.01 3.64 1.7905 1 5 2 12 51.62 1.65 1.7705 0 5 4 6 52.09 2.79 1.7557 2 1 7 12 53.23 19.66 1.7208 6 0 0 6 54.05 6.52 1.6967 0 1 8 6 55.59 7.62 1.6533 5 2 0 12 55.78 4.50 1.6480 3 4 2 12 56.38 2.04 1.6319 2 0 8 6 56.81 11.30 1.6207 1 3 7 12 57.32 2.74 1.6073 1 4 6 12 58.65 1.49 1.5740 1 2 8 12 59.05 7.03 1.5643 1 6 1 12 59.43 2.05 1.5553 2 5 3 12 60.17 4.37 1.5379 1 5 5 12 60.30 2.60 1.5348 6 1 2 12 60.86 1.21 1.5222 4 3 4 12 61.28 4.66 1.5127 3 2 7 12 62.73 2.01 1.4811 1 1 9 12 64.63 5.81 1.4422 5 3 2 12 65.17 1.04 1.4314 0 4 8 6 65.55 1.74 1.4241 6 2 1 12 65.90 2.50 1.4173 4 4 3 12 66.73 1.23 1.4018 2 6 2 12 67.27 3.28 1.3918 2 3 8 12 67.65 1.84 1.3849 2 4 7 12 68.12 1.01 1.3764 0 6 6 6 68.63 1.14 1.3675 7 1 0 12 68.68 6.76 1.3667 6 1 5 12 68.83 3.35 1.3640 1 0 10 6 69.04 2.29 1.3604 2 2 9 12 69.32 13.38 1.3556 3 5 4 12 71.35 1.56 1.3219 6 2 4 12 71.37 5.17 1.3216 5 0 8 6 71.73 1.12 1.3159 5 4 1 12 72.74 1.09 1.3000 5 3 5 12 72.86 2.53 1.2982 4 5 2 12 75.08 1.51 1.2652 1 4 9 12 75.37 3.35 1.2611 1 5 8 12 76.18 2.17 1.2496 4 4 6 12 79.28 2.38 1.2084 0 8 4 6 80.65 2.72 1.1913 1 2 11 12 81.23 1.01 1.1843 2 7 4 12 81.60 1.19 1.1798 3 5 7 12 83.18 1.54 1.1614 6 1 8 12 84.49 1.00 1.1467 7 2 5 12 85.09 3.46 1.1401 8 1 4 12 85.90 2.93 1.1315 6 3 6 12 86.55 1.14 1.1246 2 4 10 12 86.75 1.78 1.1225 5 2 9 12 87.02 1.10 1.1197 0 7 8 6 87.02 4.59 1.1197 5 3 8 12 88.47 1.85 1.1051 5 1 10 12 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.