Wolfeite Kolitsch U Acta Crystallographica E59 (2003) i125-i128 Mg-rich wolfeite, (Fe,Mg)2(PO4)(OH): structure refinement and Raman spectroscopic data Locality: Big Fish River area, Yukon Territory, Canada _database_code_amcsd 0010412 CELL PARAMETERS: 12.2740 13.1690 9.7540 90.000 108.640 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 1493.901 Density (g/cm3): 3.887 MAX. ABS. INTENSITY / VOLUME**2: 11.97455339 RIR: 1.003 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 19.21 1.06 4.6212 0 0 2 2 20.34 14.50 4.3664 -2 2 1 4 20.37 7.86 4.3597 -2 0 2 2 22.74 2.17 3.9106 -1 2 2 4 23.93 2.38 3.7189 3 1 0 4 24.58 43.36 3.6217 2 2 1 4 25.42 2.28 3.5035 2 3 0 4 26.62 33.54 3.3486 1 2 2 4 26.68 1.39 3.3407 3 2 0 4 27.08 7.39 3.2922 0 4 0 2 28.04 1.11 3.1827 0 3 2 4 28.25 70.75 3.1593 2 0 2 2 28.33 5.57 3.1505 -3 2 2 4 28.94 1.14 3.0850 2 3 1 4 28.99 88.44 3.0800 -1 4 1 4 30.65 100.00 2.9168 -4 0 2 2 30.71 1.33 2.9110 1 3 2 4 30.75 9.65 2.9075 4 0 0 2 30.77 2.41 2.9058 3 3 0 4 31.22 25.09 2.8650 2 4 0 4 31.28 1.75 2.8593 -2 2 3 4 31.51 1.81 2.8392 4 1 0 4 32.08 64.12 2.7905 0 2 3 4 32.18 27.46 2.7813 -4 2 1 4 33.42 16.72 2.6814 0 4 2 4 34.13 17.94 2.6273 -2 4 2 4 34.50 1.04 2.5995 3 3 1 4 35.06 41.02 2.5594 -3 4 1 4 36.99 22.40 2.4303 -2 0 4 2 37.30 1.78 2.4104 3 2 2 4 37.67 5.29 2.3881 -4 2 3 4 37.83 7.58 2.3779 4 2 1 4 38.98 12.25 2.3106 0 0 4 2 39.09 2.20 2.3042 3 4 1 4 39.53 6.94 2.2795 2 4 2 4 39.67 7.28 2.2723 2 2 3 4 39.70 15.57 2.2705 -1 2 4 4 39.83 5.62 2.2631 -5 2 2 4 40.92 3.26 2.2057 -3 2 4 4 41.36 5.78 2.1832 -4 4 2 4 41.65 1.73 2.1683 4 0 2 2 42.32 18.77 2.1354 0 6 1 4 42.68 10.21 2.1183 1 4 3 4 42.82 1.24 2.1117 1 1 4 4 44.08 13.35 2.0542 -2 6 1 4 44.54 12.16 2.0344 -6 0 2 2 45.09 1.44 2.0106 -6 1 2 4 45.15 1.43 2.0083 -6 1 1 4 45.34 5.75 2.0004 -1 6 2 4 46.37 3.97 1.9583 2 6 1 4 46.44 7.85 1.9553 -2 4 4 4 46.71 13.53 1.9446 2 0 4 2 46.79 21.09 1.9417 -6 2 1 4 46.87 2.37 1.9384 6 0 0 2 47.25 2.17 1.9237 2 1 4 4 47.57 1.38 1.9115 1 6 2 4 47.61 2.81 1.9100 3 6 0 4 48.11 2.99 1.8913 0 4 4 4 48.83 4.01 1.8649 -6 2 3 4 49.35 3.85 1.8467 -5 4 3 4 49.44 1.02 1.8435 0 7 1 4 49.57 1.60 1.8390 -1 7 1 4 50.19 10.44 1.8176 -4 4 4 4 50.56 1.45 1.8053 -2 6 3 4 50.90 1.12 1.7939 -6 0 4 2 51.10 4.39 1.7876 0 6 3 4 51.17 19.63 1.7852 -4 6 1 4 51.26 1.35 1.7824 2 5 3 4 51.28 4.87 1.7815 -4 2 5 4 51.34 4.11 1.7797 0 2 5 4 51.51 3.32 1.7742 3 4 3 4 51.54 1.52 1.7731 4 2 3 4 51.58 6.72 1.7718 5 4 1 4 53.05 1.24 1.7263 1 1 5 4 54.12 8.45 1.6945 3 2 4 4 54.82 2.33 1.6745 3 6 2 4 54.97 2.90 1.6704 6 4 0 4 55.22 1.15 1.6635 4 6 1 4 55.29 1.29 1.6615 -3 4 5 4 55.32 3.48 1.6607 -1 4 5 4 55.90 1.09 1.6449 3 5 3 4 56.60 19.23 1.6261 2 6 3 4 56.93 1.96 1.6176 -1 8 1 4 57.10 14.09 1.6130 6 0 2 2 57.18 3.64 1.6110 7 2 0 4 57.56 8.23 1.6011 -3 6 4 4 57.57 1.10 1.6011 6 1 2 4 58.12 8.31 1.5871 -4 0 6 2 58.25 9.88 1.5839 2 8 0 4 58.64 9.75 1.5743 -6 2 5 4 58.74 12.77 1.5718 2 2 5 4 58.85 1.66 1.5692 -7 2 4 4 59.62 6.46 1.5507 0 8 2 4 59.65 1.92 1.5500 -1 2 6 4 60.03 4.57 1.5411 -5 4 5 4 60.08 6.05 1.5400 -2 8 2 4 60.31 3.81 1.5347 -7 4 1 4 60.33 5.11 1.5342 -8 0 2 2 61.12 11.14 1.5162 -7 4 3 4 62.35 4.62 1.4892 -5 2 6 4 62.96 3.96 1.4763 -8 2 3 4 63.35 1.95 1.4681 -1 8 3 4 63.44 7.68 1.4663 3 8 1 4 63.75 1.13 1.4598 2 8 2 4 63.82 1.91 1.4584 -8 0 4 2 63.84 6.49 1.4581 -2 6 5 4 63.94 2.65 1.4561 5 4 3 4 63.96 1.48 1.4557 -2 4 6 4 63.97 8.41 1.4555 -6 6 3 4 64.05 4.60 1.4538 8 0 0 2 64.08 4.53 1.4532 -6 0 6 2 64.31 1.75 1.4485 6 4 2 4 65.06 2.32 1.4336 -4 8 2 4 65.14 2.64 1.4321 1 2 6 4 65.26 3.67 1.4296 -4 4 6 4 65.54 5.17 1.4242 4 4 4 4 66.04 6.19 1.4148 -4 6 5 4 66.08 11.90 1.4139 0 6 5 4 66.19 1.76 1.4119 6 2 3 4 66.26 6.21 1.4106 4 6 3 4 67.12 1.30 1.3946 5 2 4 4 67.21 2.20 1.3929 7 2 2 4 67.33 2.47 1.3906 -8 4 2 4 67.63 4.08 1.3853 6 6 1 4 69.23 4.86 1.3571 -2 2 7 4 69.82 1.77 1.3472 -8 2 5 4 70.25 4.10 1.3399 -7 2 6 4 70.88 1.63 1.3295 -6 4 6 4 71.19 2.98 1.3245 -5 8 3 4 71.87 3.08 1.3136 -4 8 4 4 72.57 2.27 1.3027 2 6 5 4 74.37 1.07 1.2755 2 4 6 4 75.82 5.45 1.2547 6 8 0 4 76.81 3.09 1.2410 -9 4 1 4 77.16 1.72 1.2363 -3 10 2 4 79.37 2.01 1.2072 6 6 3 4 79.55 1.22 1.2050 -10 0 4 2 80.24 1.96 1.1964 5 6 4 4 80.43 1.36 1.1941 -7 8 1 4 80.84 1.89 1.1890 8 4 2 4 81.66 3.20 1.1791 -5 2 8 4 82.39 1.10 1.1705 -6 0 8 2 82.60 5.10 1.1680 -4 6 7 4 83.04 1.14 1.1630 10 0 0 2 83.38 2.29 1.1591 8 2 3 4 83.60 1.86 1.1566 -1 10 4 4 84.20 1.53 1.1499 9 4 1 4 84.42 2.25 1.1475 -10 4 2 4 85.12 1.83 1.1398 4 8 4 4 85.53 1.32 1.1354 9 2 2 4 87.71 1.32 1.1127 5 2 6 4 89.25 1.72 1.0974 0 12 0 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.