Jamesonite Niizeki N, Buerger M J Zeitschrift fur Kristallographie 109 (1957) 161-183 The crystal structure of jamesonite, FePb4Sb6S14 _database_code_amcsd 0010581 CELL PARAMETERS: 15.5700 18.9800 4.0300 90.000 91.800 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 1190.352 Density (g/cm3): 5.758 MAX. ABS. INTENSITY / VOLUME**2: 61.60222590 RIR: 3.484 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.32 7.37 9.4900 0 2 0 2 10.92 16.33 8.1023 1 2 0 4 11.37 1.16 7.7812 2 0 0 2 14.72 8.98 6.0171 2 2 0 4 15.12 3.67 5.8609 1 3 0 4 17.72 7.72 5.0039 3 1 0 4 19.56 1.79 4.5387 1 4 0 4 21.94 30.13 4.0512 2 4 0 4 22.07 7.42 4.0280 0 0 1 2 22.16 2.70 4.0114 3 3 0 4 22.86 15.11 3.8906 4 0 0 2 23.34 40.15 3.8113 4 1 0 4 23.46 9.26 3.7921 1 1 1 4 24.00 28.12 3.7078 0 2 1 4 24.13 2.83 3.6879 1 5 0 4 24.52 4.51 3.6306 -1 2 1 4 24.85 36.43 3.5836 1 2 1 4 25.02 1.24 3.5596 -2 1 1 4 25.21 2.25 3.5321 2 0 1 2 25.44 7.74 3.5012 3 4 0 4 25.65 2.54 3.4725 2 1 1 4 26.12 100.00 3.4117 2 5 0 4 26.23 1.54 3.3978 0 3 1 4 26.33 3.46 3.3855 -2 2 1 4 26.71 13.01 3.3381 -1 3 1 4 26.90 5.78 3.3141 4 3 0 4 26.93 5.60 3.3103 2 2 1 4 27.01 1.05 3.3014 1 3 1 4 28.01 3.68 3.1852 -3 1 1 4 28.38 43.64 3.1446 -2 3 1 4 28.80 2.63 3.0999 1 6 0 4 28.95 13.08 3.0840 2 3 1 4 29.07 16.79 3.0714 5 1 0 4 29.15 14.43 3.0634 3 5 0 4 29.20 2.74 3.0586 -3 2 1 4 29.51 3.33 3.0265 -1 4 1 4 30.03 16.56 2.9761 3 2 1 4 30.51 12.32 2.9304 2 6 0 4 31.05 1.52 2.8800 -2 4 1 4 31.08 11.60 2.8775 -3 3 1 4 31.46 3.29 2.8434 -4 0 1 2 31.58 4.69 2.8333 2 4 1 4 31.82 53.74 2.8120 -4 1 1 4 31.86 43.35 2.8084 3 3 1 4 32.05 1.68 2.7928 5 3 0 4 32.41 1.25 2.7626 0 5 1 4 32.49 5.04 2.7555 4 0 1 2 32.84 24.41 2.7269 4 1 1 4 32.88 22.68 2.7237 -4 2 1 4 32.97 1.62 2.7170 4 5 0 4 33.17 25.61 2.7008 3 6 0 4 33.55 1.55 2.6712 1 7 0 4 33.56 7.96 2.6707 -3 4 1 4 34.21 1.53 2.6212 -2 5 1 4 34.29 11.25 2.6152 3 4 1 4 34.69 2.60 2.5858 2 5 1 4 35.05 2.18 2.5604 2 7 0 4 35.54 1.86 2.5263 4 3 1 4 35.89 3.86 2.5020 6 2 0 4 36.46 3.93 2.4641 -1 6 1 4 36.52 1.06 2.4604 -3 5 1 4 36.69 2.06 2.4493 1 6 1 4 37.17 5.44 2.4186 -5 2 1 4 37.75 4.72 2.3831 -2 6 1 4 37.92 1.35 2.3725 0 8 0 2 38.19 6.74 2.3564 2 6 1 4 38.29 5.81 2.3507 5 2 1 4 38.38 2.05 2.3454 1 8 0 4 39.60 18.54 2.2759 6 4 0 4 39.72 1.61 2.2694 2 8 0 4 39.79 8.31 2.2654 5 3 1 4 40.09 3.16 2.2493 0 7 1 4 40.42 19.33 2.2317 -1 7 1 4 40.55 4.82 2.2245 4 7 0 4 40.67 3.17 2.2186 5 6 0 4 41.07 1.58 2.1977 -6 1 1 4 41.60 6.42 2.1710 -2 7 1 4 41.73 1.69 2.1646 7 2 0 4 41.87 1.95 2.1576 3 8 0 4 41.93 1.17 2.1548 -6 2 1 4 42.01 1.22 2.1508 2 7 1 4 42.76 1.49 2.1147 -4 6 1 4 43.13 1.76 2.0975 7 3 0 4 43.14 7.18 2.0970 6 2 1 4 43.56 1.76 2.0777 4 6 1 4 43.58 5.03 2.0770 -3 7 1 4 44.17 6.14 2.0506 3 7 1 4 44.31 24.21 2.0443 0 8 1 4 44.50 9.18 2.0358 6 3 1 4 44.81 6.29 2.0227 1 8 1 4 45.01 12.98 2.0140 0 0 2 2 45.03 13.10 2.0132 7 4 0 4 45.21 6.25 2.0057 6 6 0 4 45.22 10.09 2.0053 -6 4 1 4 45.28 10.41 2.0028 0 1 2 4 45.48 6.09 1.9943 -1 1 2 4 46.27 6.65 1.9621 -1 2 2 4 46.27 1.32 1.9620 -5 6 1 4 46.69 3.15 1.9453 8 0 0 2 46.95 2.61 1.9352 8 1 0 4 47.02 6.72 1.9327 4 7 1 4 47.05 2.78 1.9315 -7 2 1 4 47.39 2.03 1.9184 7 5 0 4 47.57 6.13 1.9116 -6 5 1 4 47.72 1.96 1.9057 8 2 0 4 47.93 9.11 1.8980 0 10 0 2 48.10 2.87 1.8916 3 8 1 4 48.31 4.96 1.8840 1 10 0 4 48.34 6.16 1.8829 7 2 1 4 48.52 1.05 1.8764 -2 3 2 4 48.67 3.54 1.8709 6 5 1 4 48.95 1.16 1.8608 -3 2 2 4 49.14 7.50 1.8540 4 9 0 4 49.20 3.39 1.8518 1 9 1 4 49.28 1.43 1.8490 3 1 2 4 49.69 1.76 1.8347 1 4 2 4 50.07 5.71 1.8217 -4 8 1 4 50.07 4.65 1.8216 -7 4 1 4 50.15 8.50 1.8189 7 6 0 4 50.19 3.38 1.8177 -3 3 2 4 50.33 10.23 1.8131 -6 6 1 4 50.36 3.82 1.8120 -4 0 2 2 50.48 6.10 1.8081 5 7 1 4 50.97 10.38 1.7918 2 4 2 4 51.25 1.08 1.7824 3 10 0 4 51.53 2.96 1.7737 -8 0 1 2 51.76 2.42 1.7661 4 0 2 2 51.77 3.68 1.7660 -8 1 1 4 52.00 6.68 1.7585 4 1 2 4 52.26 2.59 1.7505 -7 5 1 4 52.41 2.32 1.7459 5 9 0 4 52.44 11.39 1.7449 -2 5 2 4 52.49 1.04 1.7435 -8 2 1 4 53.19 4.01 1.7220 9 1 0 4 53.46 2.36 1.7141 7 5 1 4 53.74 6.56 1.7058 4 10 0 4 53.85 4.43 1.7025 8 2 1 4 53.90 2.43 1.7011 9 2 0 4 54.02 1.78 1.6974 -3 5 2 4 54.06 1.78 1.6963 5 8 1 4 54.15 4.08 1.6938 -4 9 1 4 54.34 1.61 1.6883 -5 2 2 4 54.46 1.88 1.6847 6 7 1 4 54.49 2.84 1.6841 1 6 2 4 54.82 3.02 1.6747 4 9 1 4 55.45 1.90 1.6570 8 6 0 4 55.49 1.51 1.6558 -5 3 2 4 55.68 5.34 1.6507 2 6 2 4 56.18 1.72 1.6373 3 11 0 4 56.66 2.00 1.6246 9 4 0 4 57.13 1.17 1.6123 -5 9 1 4 57.45 1.52 1.6040 1 7 2 4 57.53 4.55 1.6020 3 6 2 4 57.90 2.60 1.5926 -6 2 2 4 57.97 1.12 1.5910 -2 7 2 4 58.72 1.46 1.5723 -4 6 2 4 59.39 1.46 1.5562 10 0 0 2 59.45 2.50 1.5547 -3 7 2 4 59.61 2.00 1.5510 10 1 0 4 60.26 1.58 1.5357 10 2 0 4 60.28 1.99 1.5354 0 8 2 4 60.44 1.01 1.5316 -1 8 2 4 60.51 1.17 1.5300 7 9 0 4 60.54 1.76 1.5293 -6 4 2 4 60.86 2.21 1.5220 -3 11 1 4 61.44 4.47 1.5091 5 11 0 4 61.56 3.20 1.5065 -4 7 2 4 61.66 1.40 1.5043 8 8 0 4 61.97 1.37 1.4975 -7 2 2 4 62.41 2.64 1.4880 6 4 2 4 62.48 2.17 1.4865 -6 5 2 4 63.02 2.42 1.4751 -4 11 1 4 63.39 1.47 1.4673 -1 12 1 4 63.54 3.39 1.4641 1 12 1 4 63.63 1.22 1.4624 4 11 1 4 63.81 1.19 1.4588 8 7 1 4 63.92 2.76 1.4565 0 9 2 4 64.31 7.37 1.4485 6 5 2 4 64.51 1.09 1.4445 -7 4 2 4 64.56 3.66 1.4435 2 12 1 4 64.74 1.99 1.4399 10 5 0 4 65.16 1.48 1.4317 7 3 2 4 65.25 1.13 1.4299 8 9 0 4 65.28 1.88 1.4293 -10 3 1 4 65.75 1.07 1.4203 -5 11 1 4 66.24 1.62 1.4108 11 1 0 4 66.60 2.83 1.4042 6 6 2 4 66.78 2.84 1.4009 10 3 1 4 66.93 3.57 1.3981 8 8 1 4 66.97 1.08 1.3974 9 8 0 4 67.36 1.27 1.3902 -5 8 2 4 67.53 2.23 1.3871 -8 3 2 4 67.78 1.20 1.3827 -9 7 1 4 67.85 1.10 1.3813 0 10 2 4 68.05 3.34 1.3777 8 0 2 2 68.21 1.36 1.3749 10 4 1 4 68.57 4.23 1.3686 -10 5 1 4 68.63 2.08 1.3675 -7 6 2 4 69.10 1.02 1.3594 9 7 1 4 69.15 1.63 1.3585 8 10 0 4 69.21 1.12 1.3574 -8 9 1 4 69.40 5.48 1.3542 -2 13 1 4 69.41 3.23 1.3540 4 9 2 4 69.69 1.45 1.3493 2 13 1 4 70.03 1.56 1.3436 10 5 1 4 70.08 1.86 1.3427 0 0 3 2 70.12 1.08 1.3420 -3 10 2 4 70.51 2.06 1.3356 2 14 0 4 70.88 2.26 1.3295 -9 1 2 4 71.36 1.12 1.3218 5 13 0 4 72.06 3.44 1.3106 -4 10 2 4 72.23 1.65 1.3080 10 6 1 4 72.90 1.05 1.2976 -3 2 3 4 73.01 2.14 1.2959 -8 10 1 4 74.05 1.04 1.2802 9 2 2 4 74.15 1.23 1.2788 8 10 1 4 74.15 1.36 1.2788 -4 1 3 4 74.18 1.31 1.2784 -9 9 1 4 74.18 2.23 1.2783 3 2 3 4 74.22 1.04 1.2778 -7 8 2 4 74.47 1.66 1.2741 6 12 1 4 74.74 2.74 1.2702 -4 2 3 4 74.79 1.50 1.2694 10 7 1 4 74.87 1.32 1.2683 2 4 3 4 75.14 2.35 1.2643 3 11 2 4 75.16 1.27 1.2640 3 3 3 4 75.36 1.31 1.2612 1 15 0 4 75.51 2.26 1.2591 -8 7 2 4 75.78 2.27 1.2553 -2 5 3 4 76.15 1.04 1.2501 -3 14 1 4 76.23 2.00 1.2489 2 15 0 4 76.43 1.33 1.2462 4 2 3 4 76.45 1.36 1.2459 -12 0 1 2 76.62 1.48 1.2436 2 5 3 4 76.74 1.33 1.2419 -1 12 2 4 77.12 1.07 1.2368 -8 11 1 4 77.23 1.08 1.2353 -12 2 1 4 77.71 1.07 1.2288 10 8 1 4 78.30 1.06 1.2211 7 12 1 4 78.32 3.14 1.2208 12 1 1 4 79.38 1.54 1.2071 -11 7 1 4 79.68 1.90 1.2033 10 2 2 4 79.77 1.94 1.2023 -1 7 3 4 79.83 2.23 1.2015 6 14 0 4 81.04 1.08 1.1865 -6 3 3 4 81.68 1.12 1.1788 -8 9 2 4 82.38 1.77 1.1706 -6 4 3 4 83.05 1.23 1.1629 1 8 3 4 83.09 1.63 1.1624 7 13 1 4 83.52 2.71 1.1575 6 3 3 4 83.69 1.20 1.1556 10 5 2 4 85.04 1.10 1.1407 -11 4 2 4 86.18 1.74 1.1285 -6 6 3 4 86.29 1.00 1.1274 -9 12 1 4 87.03 1.61 1.1197 -8 1 3 4 87.26 1.87 1.1173 -7 14 1 4 87.49 2.96 1.1150 8 10 2 4 87.79 1.13 1.1119 -5 13 2 4 87.90 1.67 1.1108 4 8 3 4 87.95 2.09 1.1103 2 14 2 4 88.68 1.06 1.1031 -12 8 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.