Aikinite Ohmasa M, Nowacki W Zeitschrift fur Kristallographie 132 (1970) 71-86 A redetermination of the crystal structure of aikinite [BiS2|S|CuIVPbVII] Locality: Beresowsk, Ural _database_code_amcsd 0010716 CELL PARAMETERS: 11.6380 4.0390 11.3190 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 532.060 Density (g/cm3): 7.189 MAX. ABS. INTENSITY / VOLUME**2: 77.62666628 RIR: 3.516 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.90 3.47 8.1142 1 0 1 4 15.23 1.67 5.8190 2 0 0 2 17.13 10.19 5.1752 2 0 1 4 17.42 4.26 5.0896 1 0 2 4 21.91 45.95 4.0571 2 0 2 4 23.38 17.25 3.8041 0 1 1 4 24.25 98.74 3.6698 3 0 1 4 24.62 46.07 3.6158 1 1 1 8 24.81 82.09 3.5891 1 0 3 4 26.87 14.61 3.3180 2 1 0 4 27.88 6.98 3.1998 3 0 2 4 28.02 82.97 3.1841 2 1 1 8 28.19 1.81 3.1658 2 0 3 4 28.21 66.96 3.1638 1 1 2 8 30.73 8.79 2.9095 4 0 0 2 31.25 100.00 2.8624 2 1 2 8 31.62 12.69 2.8298 0 0 4 2 31.75 1.97 2.8179 4 0 1 4 32.47 9.54 2.7572 0 1 3 4 32.56 3.82 2.7496 1 0 4 4 33.40 59.45 2.6829 1 1 3 8 34.67 56.41 2.5876 4 0 2 4 35.27 18.83 2.5448 2 0 4 4 35.80 24.74 2.5081 3 1 2 8 36.05 6.80 2.4916 2 1 3 8 38.12 25.18 2.3608 4 1 0 4 38.97 14.95 2.3110 4 1 1 8 39.10 2.41 2.3040 4 0 3 4 39.53 2.04 2.2799 5 0 1 4 39.65 33.02 2.2729 1 1 4 8 40.12 11.20 2.2474 3 1 3 8 40.60 1.89 2.2222 1 0 5 4 41.44 13.13 2.1788 4 1 2 8 41.96 20.51 2.1531 2 1 4 8 41.97 6.48 2.1527 5 0 2 4 42.86 1.60 2.1098 2 0 5 4 44.67 2.36 2.0285 4 0 4 4 44.88 38.92 2.0195 0 2 0 2 45.60 25.13 1.9896 3 1 4 8 45.70 9.21 1.9854 5 1 1 8 45.80 11.77 1.9810 5 0 3 4 45.96 8.15 1.9748 0 1 5 4 46.44 34.86 1.9552 3 0 5 4 46.65 4.13 1.9469 1 1 5 8 46.84 8.55 1.9397 6 0 0 2 47.56 1.41 1.9118 6 0 1 4 47.88 9.84 1.8997 5 1 2 8 48.24 12.60 1.8865 0 0 6 2 48.38 1.08 1.8813 2 2 1 8 49.69 3.36 1.8349 6 0 2 4 50.34 3.77 1.8128 4 1 4 8 50.48 8.37 1.8079 2 2 2 8 50.79 2.84 1.7976 5 0 4 4 51.37 10.75 1.7786 5 1 3 8 51.66 19.05 1.7693 3 2 1 8 51.96 17.44 1.7600 1 2 3 8 51.96 6.85 1.7599 3 1 5 8 52.32 9.57 1.7485 6 1 0 4 52.99 8.27 1.7280 6 1 1 8 53.67 1.65 1.7078 3 2 2 8 54.24 2.99 1.6911 1 1 6 8 54.96 3.93 1.6706 6 1 2 8 55.38 2.43 1.6590 4 2 0 4 55.94 3.46 1.6438 0 2 4 4 55.99 3.21 1.6423 5 1 4 8 56.08 1.57 1.6400 2 1 6 8 56.54 1.06 1.6277 1 2 4 8 57.55 2.52 1.6016 1 0 7 4 57.61 2.12 1.5999 6 0 4 4 57.93 18.05 1.5920 4 2 2 8 58.15 2.22 1.5864 6 1 3 8 58.33 6.03 1.5819 2 2 4 8 59.32 1.97 1.5580 2 0 7 4 60.80 9.87 1.5234 7 1 1 8 60.89 6.26 1.5214 7 0 3 4 61.59 1.97 1.5058 5 1 5 8 62.37 7.71 1.4888 1 1 7 8 62.61 1.18 1.4836 7 1 2 8 63.08 7.98 1.4738 4 1 6 8 63.12 2.75 1.4728 5 2 2 8 64.06 7.47 1.4536 2 1 7 8 64.59 1.52 1.4429 8 0 1 4 65.07 2.36 1.4335 7 0 4 4 65.18 1.16 1.4312 4 2 4 8 66.07 5.93 1.4142 5 2 3 8 66.34 1.82 1.4089 8 0 2 4 66.57 17.15 1.4047 3 2 5 8 66.88 4.45 1.3989 6 2 0 4 67.71 1.86 1.3838 6 1 5 8 68.00 6.58 1.3786 0 2 6 4 68.05 2.40 1.3777 5 1 6 8 68.21 2.24 1.3748 2 0 8 4 69.18 1.56 1.3581 6 2 2 8 69.51 4.21 1.3524 6 0 6 4 69.59 1.58 1.3509 7 1 4 8 70.08 1.53 1.3427 5 2 4 8 70.60 5.32 1.3341 4 1 7 8 70.83 4.00 1.3303 8 1 2 8 70.96 1.32 1.3282 1 3 1 8 71.06 1.02 1.3266 1 1 8 8 72.55 2.91 1.3030 2 3 1 8 72.64 2.56 1.3016 1 3 2 8 72.65 2.07 1.3015 2 1 8 8 73.75 2.30 1.2848 9 0 1 4 73.91 1.07 1.2824 6 1 6 8 74.21 4.16 1.2778 2 3 2 8 74.58 2.43 1.2724 4 0 8 4 74.62 7.73 1.2718 7 1 5 8 75.34 1.66 1.2616 5 1 7 8 75.40 1.18 1.2606 9 0 2 4 75.41 2.57 1.2606 1 3 3 8 75.81 1.65 1.2549 1 2 7 8 75.87 1.35 1.2540 6 2 4 8 76.13 1.73 1.2504 1 0 9 4 76.81 1.60 1.2410 3 3 2 8 77.36 1.34 1.2336 2 2 7 8 77.46 3.00 1.2321 8 1 4 8 78.24 1.69 1.2219 4 3 0 4 78.75 4.33 1.2152 7 2 3 8 78.78 1.33 1.2148 4 3 1 8 79.22 2.52 1.2092 1 3 4 8 79.88 2.37 1.2008 0 1 9 4 80.75 1.55 1.1901 2 3 4 8 81.91 1.02 1.1761 9 0 4 4 82.09 1.09 1.1740 8 2 1 8 82.37 1.29 1.1707 9 1 3 8 82.52 1.92 1.1689 7 2 4 8 83.29 2.55 1.1601 3 3 4 8 83.70 1.34 1.1555 8 2 2 8 84.97 1.03 1.1415 5 3 2 8 85.43 1.85 1.1365 2 2 8 8 86.11 1.11 1.1292 9 1 4 8 86.64 3.46 1.1237 6 2 6 8 87.16 3.10 1.1183 10 1 0 4 87.63 1.31 1.1135 5 3 3 8 88.38 1.23 1.1060 6 3 0 4 88.91 1.00 1.1008 6 3 1 8 89.00 1.22 1.0999 6 1 8 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.