Cattiite Catti M, Franchini-Angela M, Ivaldi G Zeitschrift fur Kristallographie 155 (1981) 53-64 A case of polytypism in hydrated oxysalts: the crystal structure of Mg3(PO4)2*22H2O-II Locality: synthetic _database_code_amcsd 0010835 CELL PARAMETERS: 6.9370 6.9320 16.1320 82.150 89.720 119.490 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 666.568 Density (g/cm3): 1.642 MAX. ABS. INTENSITY / VOLUME**2: 1.850961765 RIR: 0.367 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.11 100.00 7.9624 0 0 2 2 14.72 48.42 6.0171 1 0 0 2 14.87 12.89 5.9565 0 1 0 2 15.02 28.86 5.8965 0 1 1 2 15.30 64.11 5.7911 1 0 1 2 15.44 10.16 5.7392 -1 1 1 2 16.25 14.96 5.4553 1 -1 1 2 16.70 49.02 5.3083 0 0 3 2 16.70 1.18 5.3078 0 -1 1 2 17.11 9.89 5.1830 0 1 2 2 17.72 30.34 5.0062 1 0 2 2 17.87 57.97 4.9648 -1 1 2 2 19.22 1.41 4.6183 -1 0 2 2 19.25 5.55 4.6101 1 -1 2 2 19.99 94.98 4.4415 0 -1 2 2 20.56 11.52 4.3204 0 1 3 2 21.52 42.49 4.1287 -1 1 3 2 22.33 12.27 3.9812 0 0 4 2 23.26 3.73 3.8239 1 -1 3 2 24.84 3.66 3.5849 0 1 4 2 25.69 5.26 3.4683 -2 1 0 2 25.75 2.59 3.4591 1 1 0 2 25.78 10.53 3.4559 1 0 4 2 25.92 3.24 3.4372 -1 1 4 2 25.95 18.08 3.4335 -1 2 0 2 26.28 22.03 3.3913 2 -1 1 2 26.32 5.44 3.3865 -2 1 1 2 26.61 28.64 3.3497 1 1 2 2 26.84 7.19 3.3219 -1 2 2 2 27.14 7.54 3.2857 -1 -1 1 2 27.31 4.62 3.2659 1 -2 1 2 27.87 8.97 3.2007 1 -1 4 2 27.89 5.55 3.1994 -1 0 4 2 28.02 23.26 3.1850 0 0 5 2 28.03 14.39 3.1838 2 -1 2 2 28.10 13.55 3.1758 -2 1 2 2 28.98 5.18 3.0809 -1 2 3 2 29.57 2.46 3.0210 -1 -1 2 2 29.62 4.55 3.0160 0 1 5 2 29.62 2.36 3.0158 0 2 1 2 29.69 3.60 3.0085 2 0 0 2 29.76 5.08 3.0024 2 0 1 2 29.92 1.07 2.9861 -2 2 0 2 30.00 4.62 2.9782 0 2 0 2 30.02 6.03 2.9768 -2 2 1 2 30.32 5.51 2.9482 0 2 2 2 30.70 10.71 2.9122 -2 0 1 2 30.78 6.15 2.9048 -1 1 5 2 30.84 9.20 2.8989 -2 1 3 2 30.88 68.61 2.8956 2 0 2 2 30.89 6.71 2.8948 2 -2 1 2 31.17 67.86 2.8696 -2 2 2 2 31.43 60.92 2.8465 0 -2 1 2 31.79 3.32 2.8148 1 1 4 2 32.02 3.50 2.7955 -1 2 4 2 32.02 6.09 2.7948 0 2 3 2 32.69 9.39 2.7396 -2 0 2 2 32.83 4.27 2.7277 -1 -1 3 2 32.87 26.34 2.7245 1 -1 5 2 32.90 6.93 2.7224 -1 0 5 2 32.94 1.08 2.7189 1 -2 3 2 32.97 8.89 2.7167 2 0 3 2 33.27 1.02 2.6928 -2 2 3 2 33.77 24.58 2.6541 0 0 6 2 33.77 16.59 2.6539 0 -2 2 2 33.97 2.85 2.6389 0 -1 5 2 34.23 2.33 2.6196 2 -1 4 2 34.61 31.82 2.5915 0 2 4 2 34.74 2.32 2.5825 0 1 6 2 35.61 9.40 2.5208 2 -2 3 2 35.74 1.53 2.5121 -1 2 5 2 35.82 2.41 2.5071 1 0 6 2 35.88 7.47 2.5031 2 0 4 2 36.83 5.57 2.4407 1 -2 4 2 36.89 8.69 2.4366 0 -2 3 2 37.92 10.13 2.3725 0 2 5 2 38.15 2.50 2.3589 1 -1 6 2 38.19 2.84 2.3567 -1 0 6 2 39.01 25.56 2.3092 -2 0 4 2 39.08 11.62 2.3050 2 -2 4 2 39.31 1.53 2.2921 0 -1 6 2 39.42 2.14 2.2860 1 2 1 2 39.44 9.96 2.2845 2 0 5 2 39.62 1.32 2.2750 0 0 7 2 39.72 1.78 2.2692 2 1 0 2 39.76 3.67 2.2673 -2 2 5 2 39.78 4.57 2.2662 -3 2 0 2 39.79 1.38 2.2653 -2 3 1 2 40.02 1.07 2.2528 -1 3 2 2 40.08 3.99 2.2499 -2 3 0 2 40.35 6.40 2.2355 -2 3 2 2 40.35 2.47 2.2352 3 -2 1 2 40.96 2.59 2.2035 1 2 3 2 41.12 1.19 2.1953 -3 2 2 2 41.20 1.90 2.1910 -1 -2 1 2 41.21 4.52 2.1908 1 -2 5 2 41.37 15.98 2.1827 -1 1 7 2 41.68 6.29 2.1669 -3 1 2 2 41.73 1.75 2.1643 3 -2 2 2 42.77 1.04 2.1143 -2 -1 2 2 43.09 7.82 2.0992 2 -2 5 2 43.16 3.05 2.0958 -1 3 4 2 43.26 1.42 2.0914 -1 -2 2 2 43.65 1.00 2.0735 1 -1 7 2 43.81 1.23 2.0664 -2 3 4 2 43.85 1.62 2.0648 -3 1 3 2 44.48 2.49 2.0370 1 1 7 2 44.86 4.89 2.0204 0 -1 7 2 45.08 2.80 2.0109 3 0 1 2 45.11 2.15 2.0100 0 3 1 2 45.21 1.97 2.0057 3 0 0 2 45.27 4.03 2.0031 0 3 2 2 45.48 1.46 1.9944 -3 3 1 2 45.52 6.14 1.9927 -3 2 4 2 45.54 1.86 1.9917 1 2 5 2 45.62 1.98 1.9887 2 -3 3 2 45.69 1.34 1.9855 0 3 0 2 45.94 2.28 1.9756 -1 -1 6 2 45.99 3.51 1.9733 -1 -2 3 2 46.08 1.03 1.9697 -3 0 1 2 46.14 2.36 1.9673 -3 3 2 2 46.16 3.49 1.9667 1 -3 3 2 46.18 10.69 1.9656 0 2 7 2 46.19 1.14 1.9655 0 3 3 2 46.40 2.37 1.9569 3 -3 1 2 46.65 1.57 1.9470 3 -2 4 2 46.67 4.17 1.9461 -3 1 4 2 46.99 1.53 1.9337 -1 1 8 2 47.02 1.49 1.9327 0 -3 1 2 47.08 1.81 1.9304 3 0 3 2 47.54 7.61 1.9125 -2 0 6 2 47.56 10.54 1.9119 2 -2 6 2 47.90 1.08 1.8993 -2 1 7 2 48.39 5.58 1.8809 -2 2 7 2 48.40 3.89 1.8808 3 -1 5 2 48.78 1.24 1.8667 1 2 6 2 49.04 1.18 1.8576 -1 3 6 2 49.12 2.84 1.8546 3 0 4 2 49.32 2.13 1.8477 -1 -2 4 2 49.36 1.69 1.8463 1 -1 8 2 49.41 1.78 1.8444 -1 0 8 2 49.51 4.67 1.8411 2 1 6 2 49.52 4.58 1.8408 0 -2 6 2 49.59 1.22 1.8381 -3 3 4 2 49.93 3.28 1.8264 -3 0 3 2 49.94 7.35 1.8262 -2 3 6 2 50.08 1.60 1.8215 -3 1 5 2 50.11 13.90 1.8205 0 3 5 2 50.17 2.72 1.8184 3 -3 3 2 51.06 5.27 1.7886 -1 -1 7 2 51.66 1.16 1.7694 0 0 9 2 52.07 2.07 1.7563 3 -1 6 2 52.37 1.47 1.7469 -3 2 6 2 52.40 9.21 1.7460 2 2 1 2 52.41 1.54 1.7459 2 -2 7 2 52.41 1.30 1.7457 -2 0 7 2 52.54 5.83 1.7418 2 2 2 2 52.69 1.46 1.7373 1 0 9 2 52.79 12.65 1.7342 -4 2 0 2 52.80 2.40 1.7339 -3 0 4 2 52.81 1.69 1.7336 -1 3 7 2 52.85 12.74 1.7322 -2 4 1 2 52.94 4.97 1.7296 2 2 0 2 52.99 2.74 1.7280 3 -3 4 2 52.99 8.64 1.7280 2 0 8 2 53.10 3.82 1.7246 4 -2 1 2 53.28 1.47 1.7192 1 -3 5 2 53.31 4.75 1.7186 -2 2 8 2 54.53 2.47 1.6829 0 -2 7 2 54.54 1.23 1.6826 2 -4 1 2 54.72 1.38 1.6774 3 1 1 2 54.81 2.24 1.6749 2 2 4 2 54.85 4.25 1.6737 1 1 9 2 55.05 2.06 1.6682 -1 2 9 2 55.31 2.06 1.6609 -2 4 4 2 55.48 1.07 1.6563 1 3 3 2 55.63 2.22 1.6522 -3 4 0 2 55.70 4.00 1.6501 4 -2 3 2 55.75 1.10 1.6488 -1 4 3 2 55.83 1.69 1.6468 -4 2 3 2 56.34 1.15 1.6329 2 -4 2 2 56.49 1.79 1.6290 -1 -1 8 2 56.51 2.01 1.6285 1 -2 8 2 56.53 2.22 1.6280 -2 -1 6 2 56.68 1.81 1.6240 2 -3 6 2 56.78 1.46 1.6214 -1 -3 1 2 56.91 1.84 1.6179 -4 1 2 2 57.10 5.78 1.6129 4 -3 2 2 57.80 1.99 1.5951 -3 -1 2 2 58.55 1.06 1.5765 -2 2 9 2 58.96 1.11 1.5665 -1 4 5 2 59.87 2.17 1.5449 0 -2 8 2 61.66 1.06 1.5043 4 0 0 2 62.20 1.47 1.4924 -1 -1 9 2 62.98 1.15 1.4759 3 0 8 2 64.28 1.29 1.4491 2 -1 10 2 64.35 2.45 1.4478 4 0 4 2 64.35 1.33 1.4477 0 0 11 2 65.00 1.10 1.4348 -4 4 4 2 65.12 2.16 1.4325 -1 1 11 2 65.55 1.08 1.4241 3 1 7 2 66.40 1.40 1.4079 1 1 11 2 67.61 1.63 1.3856 3 0 9 2 68.05 2.78 1.3777 0 -4 3 2 68.10 2.08 1.3768 3 2 3 2 68.13 2.48 1.3762 -3 3 9 2 68.21 2.54 1.3749 -1 -1 10 2 68.56 1.43 1.3687 -4 3 7 2 68.82 2.88 1.3642 5 -2 2 2 68.82 1.34 1.3641 -3 5 3 2 68.83 1.64 1.3641 -2 5 0 2 69.62 1.27 1.3505 -2 -3 1 2 70.08 3.42 1.3427 2 -5 1 2 70.40 1.19 1.3375 -5 3 3 2 71.12 1.06 1.3256 3 -1 10 2 71.45 1.35 1.3202 -2 -3 2 2 71.64 2.68 1.3173 4 1 2 2 71.73 1.08 1.3158 -1 -3 6 2 72.29 1.03 1.3071 -5 4 1 2 72.35 2.59 1.3060 4 0 7 2 72.39 2.00 1.3054 0 -3 8 2 72.82 1.03 1.2988 -1 2 12 2 73.04 1.30 1.2954 2 1 11 2 73.47 2.25 1.2889 -2 3 11 2 74.16 1.80 1.2786 -3 4 9 2 78.66 1.04 1.2164 1 -3 10 2 78.67 1.49 1.2163 -3 3 11 2 82.50 1.24 1.1692 2 0 13 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.